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European inter-comparison studies as a tool for perfecting irradiated food detection methods

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EN
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EN
In this paper, we present the results of inter-comparison studies on identification of irradiated food carried out by the leading European laboratories from 1991 to 2018. In 1990s, the Federal Institute for Health Protection of Consumers and Veterinary Medicine in Germany played the leading role in the organization of the inter-laboratory tests on this subject. At the beginning of the present century, the Spanish Agency for Food Safety and Nutrition and Food National Spanish Centre took over this role. In total, 47 international tests were carried out in which nearly 500 samples of alimentary products were analysed in 37 laboratories from 14 European countries. The tests were aimed at proving the reliability of analytical methods – thermoluminescence (TL), photostimulated luminescence (PSL), and electron paramagnetic resonance (EPR) spectroscopy – for identification of specific irradiated food products and to control the analytical skills and experience of participating laboratories. The results made possible a discussion on why some irradiated food samples are more difficult for identification. In general, the tests showed that TL measurements of products such as herbs, nuts, peppers, and raisins, and EPR studies of fish and chicken bones, fresh strawberries, and dried fruits could be used as reliable control methods. The challenge that control laboratories are facing now, is related to the identifi cation of complex food products such as diet supplements or biopharmaceuticals, in which only some additives are irradiated.
Słowa kluczowe
Czasopismo
Rocznik
Strony
91--97
Opis fizyczny
Bibliogr. 30 poz., rys.
Twórcy
  • Institute of Nuclear Chemistry and Technology Dorodna 16 Str., 03-195 Warsaw, Poland
  • Institute of Nuclear Chemistry and Technology Dorodna 16 Str., 03-195 Warsaw, Poland
Bibliografia
  • 1. FAO/WHO. (2003). General Standard for Irradiated Foods. Codex Alimentarius 106-1983. Rev. 1-2003.
  • 2. International Atomic Energy Agency. (1989). Conference on Acceptance, Control of and Trade in Irradiated Food. Conference proceedings, Geneva, 12–16 December 1988. Vienna: IAEA.
  • 3. European Committee for Standardization. (2002). Foodstuffs – Thermoluminescence detection of irradiated food from which silicate minerals can be isolated. EN 1788:2002. Brussels: European Committee for Standardization.
  • 4. European Committee for Standardization. (2009). Foodstuffs – Detection of irradiated food using photostimulated luminescence. EN 13751:2009. Brussels: European Committee for Standardization.
  • 5. European Committee for Standardization. (2003). Foodstuffs – Detection of irradiated food containing crystalline sugar by ESR spectroscopy. EN 13708:2003. Brussels: European Committee for Standardization.
  • 6. European Committee for Standardization. (2001). Foodstuffs – Detection of irradiated food containing cellulose by ESR spectroscopy. EN 1787:2001.Brussels: European Committee for Standardization.
  • 7. European Committee for Standardization. (2000). Foodstuffs – Detection of irradiated food containing bone – Method by ESR spectroscopy. EN 1786:2000. Brussels: European Committee for Standardization.
  • 8. Sanderson, D. C. W., Schreiber, G. A., Wagner, U., Leffke, A., Helle, N., Ammon, J., & Carmichael, L. (1991). A European trial of TL detection of irradiated herbs and spices. Scottish Universities Research Reactor Center Report to BCR.
  • 9. Schreiber, G. A., Helle, N., & Bogl, K. W. (1995). An inter-laboratory trial on the identification of irradiatedspices, herbs and spice-herbs mixtures by thermoluminescence analysis. Journal of AOAC International, 78(1), 88–93.
  • 10. Schreiber, G. A., Helle, N., Schulzki, G., Linke, B., Spiegelberg, A., Mager, M., & Bogl, K.W. (1996).Interlaboratory tests to identify irradiation treatment of various foodstuffs via gas chromatographic detection of hydrocarbons, ESR spectroscopy and TL analysis. In C. H. McMurray, E. M. Stewart, R. Gray & J. Pearce (Eds.), Detection methods for irradiated foods – current status (pp. 98–107). Cambridge: Royal Society of Chemistry.
  • 11. Sanderson, D. C. W., Carmichael, L., Naylor, J. D., & Fisk, S. (1997). An international collaborative blind trial of thermoluminescence detection of irradiated shellfish. Scottish Universities Research Reactor Center Report to MAFF.
  • 12. Schreiber, G. A., Wagner, U., Ammon, J., Sanderson, D. C. W., Zoost, C., & Bogl, K. W. (1997). An interlaboratory on the identification of irradiated potatoes and on the estimation of applied doses by thermoluminescence analysis. Report of the Federal Institute for Health Protection of Consumers and Veterinary Medicine. Berlin: Bundesinstitut fur gesundheitlichen Verbraucherschutz und Veterinarmedizin. (BgVVHefte 13/1997).
  • 13. Raffi , J. (1992). Electron spin resonance intercomparison studies on irradiated foodstuffs. BSR-Information. Luxembourg: Commission of the European Communities. (Report EUR/13630/en).
  • 14. Sanderson, D. C. W., Carmichael, L., & Fisk, S. (1998). Establishing luminescence methods to detect irradiated foods. Food Sci. Techn. Today, 12(2), 97–102.
  • 15. Raffi , J., Stevenson, M. H., Kent, M., Thiery, J. M., & Belliardo, J. -J. (1992). European intercomparison on electron spin resonance identification of irradiated foodstuffs. Int. J. Food Sci. Technol., 27, 111–124.
  • 16. Raffi , J., Fakirian, A., & Lesgards, G. (1994). Comparison between electron spin resonance and thermoluminescence in view of identification of irradiated aromatic herbs. Annual Flamand Experimental Chemistry, 87, 125–133.
  • 17. Linke, B., Helle, N., Ammon, J., Ballin, U., Delincee, H., Stewart, E., Vater, N., Vreden, N., Bogl, K. W., & Schreiber, G. A. (1995). Elektronenspinresonanzspectroskopische Untersuchungen zur Idetifi zierung bestrahlter Krustentiere und Gewurze: Durchfuhrung eines Ringversuches an Nordseekrabben, Kaisergranat und Paprikapulover. Berlin: Federal Institute for Health Protection of Consumers and Veterinary Medicine. (BgVV-Heft 09).
  • 18. Helle, N., Linke, B., Schroeiber, G. A., & Bogl, K. W. (1996). Nachweis der gamma Bestrahlung von Trockenfruechten. Bundesgesundheitsblatt, 35, 179.
  • 19. Rafi i, J., Stachowicz, W., Migdał, W., Barabassy, S., Kalman, B., Yordanov, N., Andrade, E., Prost, M., & Callens, F. (1998). Establishment of an eastern network of laboratories for identification of irradiated food-stuffs. Final report of Copernicus Concerted Action. (CIPA-CT94-0134, CCE).
  • 20. Barea Sanchez, M. (2015). Final report of the intercomparison exercise for quality assurance on TL, PSL and EPR irradiated food detection methods (6th round). Spain: Servicio de Toxicologia Alimentaria et Centro Nacional de Alimentacion.
  • 21. Spanish Agency for Consumer Affairs, Food Safety and Nutrition, & National Food Center. (2018). Intercomparison exercises for quality assurance on physical methods for irradiated food detection (8th round). Spain: AECOSAN/CNA.
  • 22. Raffi , J. (1992). Electron spin resonance intercomparison studies on irradiated foodstuffs. Final report of Contract No 5348/1/5/340/90/4/BCR-F (10). Commission of the European Communities.
  • 23. Desrosiers, M. F. (1992). Coordinated research program on analytical detection methods for irradiation treatment of foods ADMIT. In Second Research Coordination Meeting. Budapest, Hungary 1992.
  • 24. Desrosiers, M. F. (1994). Report on activities for the coordinated research program on analytical detection methods for irradiation treatment of foods ADMIT. In Third Research Coordination Meeting, Belfast, Northern Ireland 1994.
  • 25. Stewart, E. M., & Kilpatrick, D. J. (1994). An international collaborative blind trial using ESR spectroscopy to detect irradiated crustacea. Ministry of Agriculture, Fisheries and Food MAFF. (UK 1994/5).
  • 26. Guzik, G. P., Stachowicz, W., Cutrubinis, M., & Sulea, C. (2009). Polish-Romanian intercomparison study on the EPR and PSL detections of irradiated foodstuffs. In Annual Report INCT 2008 (pp. 110–112). Warsaw: Institute of Nuclear Chemistry and Technology.
  • 27. Stachowicz, W., Burlińska, G., Michalik, J., Dziedzic-Goclawska, A., & Ostrowski, K. (1996). EPR spectroscopy for the detection of foods treated with ionising radiation. In C. H. McMurray, E. M. Steward, R. Grey & J. Pearce (Eds.), Detection methods for irradiated foods. Current status (pp. 23–44). Cambridge: The Royal Society of Chemistry.
  • 28. Council of the European Union, European Parliament. (1999). Directive 1999/2/EC of the European Parliament and of the Council on the approximation of the laws of the Member States concerning foods and food ingredients treated with ionizing radiation. Publications Office of the European Union.
  • 29. Council of the European Union, European Parliament. (1999). Directive 1999/3/EC of the European Parliament and of the Council on the establishment of a Community list of foods and food ingredients treated with ionizing radiation. Publications Office of the European Union.
  • 30. European Commission. (2020). Evaluation of the EU’s regulatory framework for irradiation of food. A questionaire. European Food Safety Authority.
Uwagi
Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-691d4fb9-07e6-4e3c-a7b9-cdac949ff862
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