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Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders

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Warianty tytułu
PL
Wpływ obróbki cieplnej na mikrostrukturę i właściwości magnetyczne nanokrystalicznych proszków ferrytu Mn-Zn
Języki publikacji
EN
Abstrakty
EN
The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.
Twórcy
autor
  • Department of Advanced Materials Engineering, Sejong University, Seoul 143-747, Korea
autor
  • Department of Materials Engineering, Korea Aerospace University, Gyeonggi-Do, 412-791, Korea
autor
  • Department of Materials Engineering, Korea Aerospace University, Gyeonggi-Do, 412-791, Korea
Bibliografia
  • [1] J. Zhang, Liming Yu, S. Yuan, S. Zhang, X. Zhao, J. Magn. Magn. Mater. 321, 3585-3588 (2009).
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  • [3] M. M. Hessien, M.M. Rashad, K. El-Barawy, I.A. Ibrahim, J. Magn. Magn. Mater. 320, 1615-1621 (2008).
  • [4] D. J. Kim et al., Korean Powder Metallurgy Inst, Powder metallugy & Particulate Materials Processing, Seoul 2010.
  • [5] S. K. Pradhan, S. Bid, M. Gateshki, V. Petkov, J. Mater. Chem. Phys. 93, 224-230 (2005).
  • [6] S. Dasgupta, J. Das, J. Eckert, I. Manna, J. Magn. Magn. Mater. 306, 9-15 (2006).
  • [7] S. J. Park, Y. S. Song, K. S. Nam, S. Y. Chang, J. Kor. Powd. Met. Inst. 19, 122-126 (2012).
  • [8] S. M. Hong, E. K. Park, K. Y. Kim, J. J. Park, M. K. Lee, C. K. Rhee, J. K. Lee, Y. S. Kwon, J. Kor. Powd. Met. Inst. 19, 32-39 (2012).
  • [9] H. P. Klug, L. E. Alexander, Joohn Wiley and Sons, X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials, New York 1997.
  • [10] L. Zhao, H. Yang, L. Yu, Y. Cui, X. Zhao, B. Zou, S. Feng, J. Magn. Magn. Mater. 301, 445-451 (2006).
Uwagi
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-6846cdc5-c50a-480e-9d1b-e6eae63c1a79
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