Sorption in an ammonioalunite-ammoniojarosite solid solution: results for the 1, 2, 4, 7, 11, 12 and 13 group elements and LREEs

Kruszewski, Łukasz; Marciniak-Maliszewska, Beata; Kotowski, Jakub

doi:10.7306/gq.1716

Artykuł - szczegóły

Tytuł artykułu

Sorption in an ammonioalunite-ammoniojarosite solid solution: results for the 1, 2, 4, 7, 11, 12 and 13 group elements and LREEs

Autorzy

Kruszewski Łukasz , Marciniak-Maliszewska Beata , Kotowski Jakub

Treść / Zawartość

Pełne teksty:

Kruszewski_L_Sorption_GQ_Vol. 67_No. 4_2023.pdf

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Identyfikatory

DOI

10.7306/gq.1716

Warianty tytułu

Języki publikacji

Abstrakty

This paper collates selected analytical results from a 1-year sorption experiments conducted on natural samples of an ammonioalunite-ammoniojarosite solid solution (AAJ) of known initial composition. These include Electron Microprobe (EPMA) and Powder X-Ray Diffraction (PXRD) results for baths subjected to Li₂SO₄·H₂O, KI, Rb₂CO₃ (0.33-0.62 wt.% Rb₂O in the AAJ, CsCl (0.24-1.07 wt.% Cs₂O), Ca(OH)₂ (ettringite formation), Sr(NO₃)₂ (0.31–10.25 wt.% SrO), ZrO(NO₃)₂·2H₂O, MnSO₄₂O, CuSO₄·5H₂O (up to 1.05 wt.% CuO), ZnCl₂, Ga(NO₃)₃·9H₂O (5.86-21.44 wt.% Ga₂O₃), ZrCl₄ (up to 17.56 wt.% ZrO₂ in AAJ, i.e., up to 0.27 apfu Zr, InCl₃ (0.85–17.04 wt.% In₂O₃, i.e., possibly up to 0.42 apfu), KH₂AsO₄ (up to 45.93 wt.% As₂O5, recast to 1.64 apfu As), K₂SeO₃ (up to 44.86 wt.% SeO₂, recast to 1.55 apfu Se), LaCl₃·7H2O (0.17–0.22 wt.% La₂O₃), CeCl₃·7H₂O (0.38–1.74 wt.% Ce₂O₃), and PrCl₃·6H-2O (1.66–4.10 wt.% Pr₂O₃). Zn, Mn, and I only rarely show accumulation. (NH₄)Fe₃(AsO₄)₂[(OH)₄(H₂O)₂] and (NH₄)Fe₃[(AsO₄)(SO₄)][(OH)₅(H₂O)] are occasionally the dominant hypothetical end-members in the As experiment. In the KI case the resulting material is 1.6 times more enriched in K than the base used. Special attention is paid to Zr, with PXRD and EPMA results not ideally coincident with a trial Scanning Electron Microscopy-Electron Backscatter Diffraction study suggesting deposition of tetragonal ZrSiO₄ (synthetic zircon).

Słowa kluczowe

alunite group sorption gallium indium zirconium strontium hypothetical end-members

Wydawca

Państwowy Instytut Geologiczny - Państwowy Instytut Badawczy

Czasopismo

Geological Quarterly

Rocznik

2023

Tom

Vol. 67, No. 4

Strony

art. no. 46

Opis fizyczny

Bibliogr. 93 poz., fot., tab., wykr.

Twórcy

autor

Kruszewski Łukasz

Institute of Geological Sciences PAS, Twarda 51/55 Str., PL-00-818 Warszawa, Poland

https://orcid.org/0000-0001-6332-9944

autor

Marciniak-Maliszewska Beata

Laboratory of Electron Microscopy, Microanalysis and X-Ray Diffraction, Faculty of Geology, University of Warsaw

https://orcid.org/0000-0001-9147-6639

autor

Kotowski Jakub

Laboratory of Electron Microscopy, Microanalysis and X-Ray Diffraction / Department of Geology of Sedimentary Basins, Faculty of Geology, University of Warsaw

https://orcid.org/0000-0002-3542-3519

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