Identification and determination of compounds belonging to the group of OUN pharmaceutical agents by thin-layer chromatography with densitometric detection in biological material

Maślanka, A.; Krzek, J.; Żuromska, B; Stolarczyk, M.

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Tytuł artykułu

Identification and determination of compounds belonging to the group of OUN pharmaceutical agents by thin-layer chromatography with densitometric detection in biological material

Autorzy

Maślanka A. , Krzek J. , Żuromska B , Stolarczyk M.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

Warianty tytułu

Języki publikacji

Abstrakty

The chromatographic-densitometric method was developed for the simultaneous determination of various pharmaceutical agents, such as haloperidol, fluxetine, promazine, doxepin, clonazepam, alprazolam, and risperidone in biological material. Two mobile phases, A (acetone-diethylamine-cyclohexane (2.5:2.5:20, υ/υ/υ)) and B (trichloromethane-acetone-25% NH3 (25:25:0.5, υ/υ/υ)), were used for the separation of the above-mentioned compounds. Silica gel-covered F254 TLC plates were used as stationary phases. Densitometric recording was carried out at 254 nm wavelength. Well-developed peaks, easy to quantify, and quality analysis were obtained after achieving the separation of compounds in the developed conditions. It was demonstrated that the presence of a matrix (plasma or urine) did not affect the shape of the peaks and their localization on the chromatograms.

Słowa kluczowe

tricyclic antidepressant drugs antipsychotics (also called neuroleptics) benzodiazepine derivatives TLC densitometry

Wydawca

University of Silesia in Katowice
Akademiai Kiado

Czasopismo

Acta Chromatographica

Rocznik

2011

Tom

Vol. 23, no. 2

Strony

247--266

Opis fizyczny

Bibliogr. 63 poz., rys., tab.

Twórcy

autor

Maślanka A.

agiellonian University, Collegium Medicum Department of Inorganic and Analytical Chemistry 9 Medyczna Street 30-688 Cracow Poland

autor

Krzek J.

jankrzek@cm-uj.krakow.pl

agiellonian University, Collegium Medicum Department of Inorganic and Analytical Chemistry 9 Medyczna Street 30-688 Cracow Poland

autor

Żuromska B

agiellonian University, Collegium Medicum Department of Inorganic and Analytical Chemistry 9 Medyczna Street 30-688 Cracow Poland

autor

Stolarczyk M.

agiellonian University, Collegium Medicum Department of Inorganic and Analytical Chemistry 9 Medyczna Street 30-688 Cracow Poland

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Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-65c4a1ee-5b9e-4881-9cfc-f1cc5d275121