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Tytuł artykułu

Application of thermal analysis and calorimetry for assessment of safety and quality of nitrogen fertilizers

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Języki publikacji
EN
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EN
The paper presents the results of studies carried out using differential thermal analysis (DTA) and differential scanning calorimetry (DSC), conjugated with thermogravimetry (TG). Measurements were made for samples with differentiated compositions, mainly consisting of ammonium nitrate with fertilizer purity and compounds that may be present in nitrogen fertilizers as potential additives or contaminants. The possibilities of applied techniques and recommendations concerning proper selection of measurement conditions are described. Furthermore, the method of interpretation of the obtained results is presented, which allows evaluating the thermal stability of the tested mixtures for the safety and quality of nitrogen fertilizers.
Twórcy
autor
  • Department of Technology and Chemical Engineering, Wroclaw University of Technology, Poland
autor
  • Department of Technology and Chemical Engineering, Wroclaw University of Technology, Poland
autor
  • Department of Technology and Chemical Engineering, Wroclaw University of Technology, Poland
autor
  • Department of Technology and Chemical Engineering, Wroclaw University of Technology, Poland
Bibliografia
  • Biskupski, A., Ochal, A. and Malinowski, P. (2006). Wplyw rozwiazan technologicznych i parametrow procesowych na jakosc granulatow nawozow zawierajacych azotan amonu, Przemysl Chemiczny, no. 85(3), pp. 193-200.
  • Chaturvedi, S. and Dave, P.N. (2013). Review on Thermal Decomposition of Ammonium Nitrate. Journal of Energetic Materials, no. 31, pp. 1-26.
  • Colvin, C.I., Fearnow, P.W. and Keenan, A.G. (1965). The induction period of the chloride-catalyzed decomposition of ammonium nitrate. Inorganic Chemistry, no. 4(2), pp. 173-176.
  • Keenan, A.G. and Dimitriades, B. (1962). Mechanism for the chloride‐catalyzed thermal decomposition of ammonium nitrate. The Journal of Chemical Physics, no. 37(8), pp. 1583-1586.
  • Kolaczkowski, A., Pekalski, A. and Meissner, Z. (2000). Estimation of the liability to detonating of prilled ammonium nitrate fertiliser grade. Journal of Loss Prevention in the Process Industries, no. 13, pp. 555-561.
  • Li, X.R. and Koseki, H. (2005). Study on the contamination of chlorides in ammonium nitrate. Process Safety and Environmental Protection, no. 83(B1), pp. 31-37.
  • Oxley, J.C., Smith, J.L., Rogers, E. and Yu, M. (2002). Ammonium nitrate: thermal stability and explosivity modifiers. Thermochimica Acta, 384, pp. 23-45.
  • Pittman, W., Han, Z., Harding, B. et al. (2014). Lessons to be learned from an analysis of ammonium nitrate disasters in the last 100 years. The Journal of Hazardous Materials, no. 280, pp. 472-477.
  • Poplawski, D., Hoffmann, J. and Hoffmann, K. (2016). Effect of carbonate minerals on the thermal stability of fertilisers containing ammonium nitrate. The Journal of Thermal Analysis and Calorimetry, no. 124, pp. 1561-1574.
  • Produkcja wyrobow przemyslowych w 2015 r. (2016). Warszawa: Glowny Urzad Statystyczny.
  • Rubtsov, Y.I., Kazakov, A.I., Rustambekov, M.K. and Starshinov, M.S. (2005). Kinetic aspects and heats of reaction between components in thermal decomposition of ammonium nitrate-calcium (magnesium) carbonate mixtures. The Russian Journal of Applied Chemistry, no. 78(11), pp. 1795-1800.
  • Saunders, H.L. (1922). The decomposition of ammonium nitrate by heat. Journal of the Chemical Society, no. 121, pp. 698-711.
  • Sinditskii, V.P., Egorshev, V.Y., Levshenkov, A.I. and Serushkin, V.V. (2005). Ammonium nitrate: combustion mechanism and the role of additives. Propellants, Explosives, Pyrotechnics, no. 30(4), pp. 269-280.
  • Sun, J., Sun, Z., Wang, Q. et al. (2005). Catalytic effects of inorganic acids on the decomposition of ammonium nitrate. The Journal of Hazardous Materials, B127, pp. 204-210.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-655f1e1a-520f-4803-b1d2-4f79d8bdbbff
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