Preparation and spectroscopic analysis of zinc oxide nanorod thin films of different thicknesses

• Autorzy: Mia N. H. , Rana S. M. , Pervez F. , Rahman M. R. , Hossain K. , Al Mortuza A. , Basher M. K. , Hoq M.

Identyfikatory

DOI

10.1515/msp-2017-0066

• Języki publikacji: EN

Abstrakty

EN

Zinc oxide thin films with different thicknesses were prepared on microscopic glass slides by sol-gel spin coating method, then hydrothermal process was applied to produce zinc oxide nanorod arrays. The nanorod thin films were characterized by various spectroscopic methods of analysis. From the images of field emission scanning electron microscope (FESEM), it was observed that for the film thickness up to 200 nm the formed nanorods with wurtzite hexagonal structure were uniformly distributed over the entire surface substrate. From X-ray diffraction analysis it was revealed that the thin films had good polycrystalline nature with highly preferred c-axis orientation along (0 0 2) plane. The optical characterization done by UV-Vis spectrometer showed that all the films had high transparency of 83 % to 96 % in the visible region and sharp cut off at ultraviolet region of electromagnetic spectrum. The band gap of the films decreased as their thickness increased. Energy dispersive X-ray spectroscopy (EDS) showed the presence of zinc and oxygen elements in the films and Fourier transform infrared spectroscopy (FT-IR) revealed the chemical composition of ZnO in the film.

Słowa kluczowe

EN

ZnO nanorod; ZnO thin film; sol-gel; hydrothermal growth; thickness effect

• Wydawca: De Gruyter
• Czasopismo: Materials Science Poland
• Rocznik: 2017
• Tom: Vol. 35, No. 3
• Strony: 501--510
• Opis fizyczny: Bibliogr. 41 poz., rys., tab.

Twórcy

autor

Mia N. H.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Rana S. M.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Pervez F.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Rahman M. R.

• University of Liberal Arts Bangladesh (ULAB)

autor

Hossain K.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Al Mortuza A.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Basher M. K.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

autor

Hoq M.

• Institute of Electronics, Atomic Energy Research Establishment, Bangladesh Atomic Energy Commission, Savar, Dhaka, Bangladesh

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