PL EN


Preferencje help
Widoczny [Schowaj] Abstrakt
Liczba wyników
Tytuł artykułu

Enhancement of ilmenite magnetic properties by oxidation roasting and magnetic separation

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Oxidation roasting was proposed to treat the problem of the weak magnetic properties of ilmenite. The effects of roasting temperature, roasting time and cooling method on the results of ilmenite magnetic separation were studied. At the same time, the mechanism of the oxidation roasting process was analyzed by XRD, VSM, SEM-EDS. Determine ilmenite suitable oxidation roasting conditions for roasting temperature 750 °C, roasting time of 20 min, and cooling method of air cooling; at this time, the yield of 96.79% can be achieved in the magnetic field intensity of 238.74 kA/m. The XRD results showed that phase changes in the roasting process occur in the order of ilmenite to hematite and rutile to pseudobrookite. The results of VSM showed that the maximum specific magnetization coefficient of ilmenite increased from 3.25×10-5 m3/kg to 5.58×10-5 m3/kg after roasting, and the magnetic property was enhanced. The results of SEM-EDS showed that the phase transition of ilmenite during the roasting process occurs in a spatial order from the edge of the particles to the interior.
Rocznik
Strony
art. no. 190706
Opis fizyczny
Bibliogr. 40 poz., rys., tab., wykr.
Twórcy
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
autor
  • College of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China
Bibliografia
  • BHOGESWARA RAO, D.,RIGAUD, M. 1975. Kinetics of the oxidation of ilmenite. Oxidation of Metals 9,99-116.
  • CHEN, J., WANG, T. X., ZHOU, W., LI, Q., GE, P.,WEIXIN, S. 2015. Domestic and Foreign Marine Titanium Alloy and Its Application. Titanium Industry Progress 32,8-12.
  • CHEN, J. S., SUN, B. S.,AN, K. 2020. Titanium Alloys for Ordnance Equipment Applications. Journal of Ordnance Equipment Engineering 41,14-20.
  • CHEN, P., LIU, J. Y., ZHAI, J. H., YANG, Y. H.,SUN, W. 2023. Selective flotation separation of ilmenite from titanaugite using noctylphosphonic acid as a collector in acidic pulp. Transactions of Nonferrous Metals Society of China,1-22.
  • CHEN, P., ZHAI, J. H., WANG, H. B., WEI, S.,LAI, X. S. 2018. Experimental Study on Modification of Collector for Fine Grained Ilmenite. Chinese Journal of Rare Metals 42,205-212.
  • CHEN, Y. 1997. Low-temperature oxidation of ilmenite (FeTiO3) induced by high energy ball milling at room temperature. Journal of Alloys and Compounds 257,156-160.
  • CHEN, Y. 1998. Different oxidation reactions of ilmenite induced by high energy ball milling. Journal of Alloys and Compounds 266,150-154.
  • CHENG, P., YINGCHUN, Z., GUOJIE, L., YUSHI, J., LIANXIANG, Y.,YOUYOU, T. 2022. Recovery of Titanium and lron from Titanium Rough Concentrate in Malawi by Reduction Roasting-Magnetic Separation Process. Conservation and Utilization of Mineral Resources 42,150-157.
  • CHONGHUI, Z., CHENXIN, G., XIANZHONG, B., HE, W., SEN, W.,JIWEI, X. 2023. Experimental Study on Separation and Recovery of lron and Titanium from llmenite Rough Concentrate by Direct Reduction. Mining and Metallurgical Engineering 43,99-102.
  • CUI, Z., LIU, Q.,ETSELL, T. H. 2002. Magnetic properties of ilmenite, hematite and oilsand minerals after roasting. Minerals Engineering 15,1121-1129.
  • DAI, H., RINZLER, A. G., NIKOLAEV, P., THESS, A., COLBERT, D. T.,SMALLEY, R. E. 1996. Single-wall nanotubes produced by metal-catalyzed disproportionation of carbon monoxide. Chemical Physics Letters 260,471-475.
  • DESHEN, T.,YIXIN, Z. 1985. Magnetic property changes in primary ilmenite oxidation roasting and magnetic separation. Multipurpose Utilization of Mineral Resources,7-13.
  • GOU, H. P., ZHANG, G. H.,CHOU, K. C. 2015. Phase Evolution During the Carbothermic Reduction Process of Ilmenite Concentrate. Metallurgical&Materials Transactions B 46,48-56.
  • GUPTA, S. K., RAJAKUMAR, V.,GRIEVESON, P. 1989. Phase Relationships in the System Fe–Fe2O3–TiO2 at 700 and 900°C. Canadian Metallurgical Quarterly 28,331-335.
  • JIN, H. X., WEI, K. X., LI, J. M., ZHOU, J. Y.,PENG, W. J. 2015. Research development of titanium alloy in aerospace industry. The Chinese Journal of Nonferrous Metals 25,280-292.
  • LEI, C., CHEN, T., YAN, B.,XIAO, X. M. 2022. Reaction characteristics and kinetics of gallium in chlorination roasting of copper tailings using calcium chloride. Rare Metals 41,1063-1070.
  • LUO, L. Q., LEI, Y. M., SHEN, H. T., LIU, C.,YE, Y. L. 2023. Performance and mechanism of oxidative roasting desulphurisation of hematite-limonite containing lead and zinc. Journal of Central South University(Science and Technology) 54,2529-2539.
  • MA, C. Z., ZHANG, J. W., LIAO, Q.,LIANG, H. 2021. Experimental Study on Beneficiation of a Refractory lImenite Ore Abroad. Nonferrous Metals(Mineral Processing Section),92-97+102.
  • MEHDILO, A., IRANNAJAD, M.,REZAI, B. 2014. Effect of oxidation roasting on ilmenite flotation. Physicochemical Problems of Mineral Processing 50,493−505.
  • NING, C. Q.,ZHOU, Y. 2002. Development and research status of biomedical titanium alloys. Materials Science and Technology,100-106.
  • PENG, J., ZHENG, Y., WANG, Z., DAI, Z.,GUO, Z. 2024. Study on the surface activation of ilmenite by persulfate and flotation response. Separation and Purification Technology 343.
  • SAMANTA, S., MUKHERJEE, S.,DEY, R. 2014. Oxidation behaviour and phase characterization of titaniferous magnetite ore of eastern India. Transactions of Nonferrous Metals Society of China 24,2976-2985.
  • SHEN, S. P. 2021. Research on Separation Characteristics of Micro-fine Ilmenite and its Enhanced Recovery Technology. Northeastern University, Shenyang.
  • SONG, H. X., XV, D. L., JIU, S. W.,LI, H. 2007. Siderite Magnetization by Suspension Roasting and Effect of Cooling Conditions on Product. Metal Mine,52-54+62.
  • USGS. 2024. Mineral commodity summaries 2024. USGS Numbered Series. U.S. Geological Survey, Reston, VA.
  • WANG, Q., LIU, C. H., ZHANG, L. B., GAO, J. Y., WANG, F.,DAI, Y. 2023a. Preparation and mechanism of molybdenum trioxide by microwave oxidation roasting of molybdenite. The Chinese Journal of Nonferrous Metals 33,2015-2030.
  • WANG, X. D., LU, F. S., JIA, H., HAO, B.,MA, Y. F. 2008. The Outline of Titanium Industry in China. Titanium Industry Progress,5-8.
  • WANG, Y.,YUAN, Z. 2006. Reductive kinetics of the reaction between a natural ilmenite and carbon. International Journal of Mineral Processing 81,133-140.
  • WANG, Z. S., ZANG, J. K., WANG, X. R.,CHENG, W. 2023b. Extraction of Lithium from Coal Gangue by Oxidation Roasting- Hydrochloric Acid Leaching Process. Hydrometallurgy of China 42,574-581.
  • WEI, X., XIONGGANG, L., XINGLI, Z., XUEMEI, W.,WEIZHONG, D. 2013. Phase transitions, micro-morphology and its oxidation mechanism in oxidation of ilmenite (FeTiO3) powder. Transactions of Nonferrous Metals Society of China 23,2439-2445.
  • WEI, Z.,NIANSUO, X. 2011. Research on the development and application of titanium and titanium alloys. Science and Technology Innovation Herald,71.
  • WU, B. F. 2024. Optimization of turning plan for titanium alloy parts and calculation of working hours. Metal Working(Metal Cutting),29-33.
  • XIAN, W.,JIAN, Z. 2006. Geographical Distribution and Characteristics of Titanium Resources in China. Titanium Industry Progress 23,8-12.
  • YANG, H., RONG, Y., TANG, R., XUE, X. X.,LI, Y. 2013. Recovery of iron from Baotou rare earth tailings by magnetizing roast. Rare Metals 32,616-621.
  • YUAN, Z., ZHAO, X., LU, J., LV, H.,LI, L. 2021. Innovative pre-concentration technology for recovering ultrafine ilmenite using superconducting high gradient magnetic separator. International Journal of Mining Science and Technology 31,1043-1052.
  • ZENG, J., CHEN, L., YANG, R., TONG, X., REN, P.,ZHENG, Y. 2017. Centrifugal high gradient magnetic separation of fine ilmenite. International Journal of Mineral Processing 168,48-54.
  • ZHANG, J. B., MIAO, H. J., CHENG, X. Z.,YE, E. D. 2016. Contrastive Study on Processes of Redox Modification- Acid Leaching of Panzhihua Ti-Slag and Ilmenite. Chinese Journal of Rare Metals 40,385-392.
  • ZHU, G. C., SHI, W. Z.,TIAN, J. 2002. Recovering germanium from coal ash by chlorination with ammonium chloride. Rare Metals 21,278-281.
  • ZHU, X. L.,QIN, C. X. 2021. Comparative Test and Research on Roasting Ore with Different Cooling Methods. Gansu Metallurgy 43,4-7.
  • ZHU, X. R., SUN, Y. S., HAN, Y. X., LI, Y. J.,LU, Z. L. 2019. Effect of Cooling Mode on Magnetic Properties of Cooling Product. Metal Mine, 66-70.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-60de5047-b051-4c11-b71c-34d9f7b4e5c7
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.