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The effect of aging time at 850°C for 300 s, 600 s, 1800 s, and 84600 s on the microstructural evolution and corrosion resistance of 2205 duplex stainless steel (DSS) was studied after cold rolling up to 60% of reduction. X-ray diffraction, scanning electron and transmission electron microscopy were used for microstructural characterization. The corrosion behavior was studied by cyclic potentiodynamic polarization (CPP) and electrochemical impedance technique (EIS) in 3.5% NaCl solution and the susceptibility to sensitization was investigated through the double loop electrochemical potentiodynamic reactivation (DL-EPR) test in 0.5 M H2SO4 + 0.1 M NaCl + 0.002 M KSCN solution. After cold working, increasing aging time led to an increase in sigma phase precipitation and a decrease in pitting corrosion resistance. However, the ultrafine microstructure had a beneficial influence on the self-healing effect in Cr and Mo depleted areas with the increasing of aging time, resulting in higher passivation ability. The DSS 2205 type was not susceptible to intergranular corrosion for the aged conditions applied.
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681--688
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Bibliogr. 27 poz., rys., tab.
Twórcy
autor
- Universidade Federal de Minas Gerais, Department of Metallurgical and Materials Engineering, Belo Horizonte, Brazil
- Universidade Federal de Ouro Preto, Department of Chemistry, Campus Morro do Cruzeiro, Brazil
autor
- Universidade Federal de Ouro Preto, Department of Chemistry, Campus Morro do Cruzeiro, Brazil
autor
- Universidade Federal de Minas Gerais, Department of Metallurgical and Materials Engineering, Belo Horizonte, Brazil
autor
- Universidade Federal de Ouro Preto, Department of Chemistry, Campus Morro do Cruzeiro, Brazil
Bibliografia
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- [8] D.C. Sicupira, R. Cardoso Junior, A.Q. Bracarense, G.S. Frankel, V.F.D. Lins, Mater. Corros. 68, 604-612 (2017).
- [9] L. V. Jin-Long, L. Hong-Yun, Mater. Chem. Phys. 135, 973-978 (2012).
- [10] Q. Zhou, R. Wang, Z. Zheng, Y. Gao, Appl. Surf. Sci. 462, 804-814 (2018).
- [11] S. Shukla, A.P. Patil, A.P. Kawale, R.K. Haldkar, A. Dahiwale, A. Bansod, Mater. Today Proc. 44, 2802-2807 (2021).
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- [19] D.M. Escriba, E. Materna-Morris, R.L. Plaut, A.F. Padilha, Mater. Charact. 60, 1214-1219 (2009).
- [20] I. Calliari, M. Zanesco, E. Ramous, J. Mater. Sci. 41, 7643-7649 (2006).
- [21] W. Reick, M. Pohl, A.F. Padilha, Isij Int. 38, 567-571 (1998).
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Uwagi
The authors are grateful to Aperam South America for the steel samples supply. Also thank the CAPES-PPGEM/UFMG-REDEMAT/UFOP, CNPq and FAPEMIG for the student fellowship and financial support. Thanks to Centro de Microscopia - UFMG for transmission electron microscopy examination.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-5e22dc33-8bb8-431a-a7f3-1c7359f77219