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The proposed approach to the processing of plant materials using membrane methods is new in the field of developing new methods for isolating pectin substances and obtaining not only pectin itself, but also new low-cost high-quality pectin-containing products. The studies were carried out on pressings obtained after squeezing juice from citrus fruits (Georgia): lemon (“Meer”), Washington-Navel orange variety, “Unshiu” mandarin and the largest citrus pomelo fruit (China). From the fruits harvested in April-December, the juice was squeezed out and from the remaining mass, which was crushed, by adding HCl (1:10) pectin isolates were obtained, which were concentrated by ultrafiltration. Soluble pectin was precipitated from the concentrated extract with ethyl alcohol, i.e. converted to an insoluble form. The resulting precipitate was thoroughly washed with alcohol and then dried at T = 55°C. The concentration of isolates was carried out by tangential filtration in dynamic mode on a UPL-06 unit, an AR-0.2 ultrafiltration separating apparatus was used as a membrane, which was located vertically in the unit and was a ready-made module with a filtration area of 2 m2; obtained on the basis of polyamide and phenylone – C 2-B hollow fibers VPU-15PA with a pore size of 500 A. Ultrafiltration was carried out in circulation mode to the maximum possible concentration of the extract. The dependence of the productivity of the process of purification-concentration of pectin extracts from citrus fruit waste without their morphological division, pressure, duration and filtration mode, type and term of fruit harvesting was studied. The work performed has shown that the use of semi-permeable membranes for concentrating pectin extracts allows: to a large extent to remove carbohydrates from the extract, to achieve partial discoloration of the pectin extract; ensure 100% retention of pectin substances by membranes; to achieve a high degree of concentration of the extract and made it possible to obtain a pectin preparation with a purity of 95%. The proposed technology using membrane technology makes it possible to obtain pectin with a purity of 95% or more by purifying it from ballast impurities at the stage of extract concentration.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
117--126
Opis fizyczny
Bibliogr. 24 poz., rys.
Twórcy
autor
- Georgian Technical University, LTD Batumi Water, 19 Tabukashvili str., Batumi GE 6000, Georgia
Bibliografia
- 1. Abdelrahman Mosaad Khattab 2022. The Microbial Degradation for Pectin, 153.
- 2. Alekseev G.V., Egorova O.A., Leu A.G. 2020. Efficiency of pre-treatment of raw materials to increase the yield of pectin. http://dx.doi.org/10.33236/2307–910x-2020–2-30–78–84
- 3. Bejanidze I., Kharebava T., Pohrebennyk V., Didmanidze N., Nakashidze N. 2021a. High-quality pectin from waste of citrus juice production using ecologically pure and reagent-free method – electrodialysis. Proceedings of VIII International Congress of Ecologists – 2021. Vinnytsya, 1, 3.
- 4. Bejanidze I., Pogrebennyk V., Kharebava T., Dydmanidze N., Nakashidze N. 2021b. Vegetable waste is a source of high-quality dietary fiber. Collection of Theses. Papers of the V Specialized International Zaporizh Ecological Forum “ECO FORUM – 2021”, 1, 2.
- 5. Bejanidze I., Pohrebennyk V., Kharebava T., Koncelidze Z., Jun S. 2019. Development of waste- free, eco-pure combined technology for fruit processing. 19th International Multidisciplinary Scientific Geoconference Albena Resort, Bulgaria. Conference proceeding & EXPO SGEM, 19(5.1), 173–180.
- 6. Bejanidze I., Kontselidze Z., Kharebava T. 2018. Dietary fiber – multifunctional food ingredients. Review Publisher – RS Global Sp. z o.o., Scientific Educational Center Warsaw, Poland, 1(8)2, 30–35.
- 7. Bejanidze I., Pogrebennik V., Kharebava T., Didmanidze N., Nakashidze N. 2021. Intensification of technological processes for processing waste of citrus productions. Actual problems, priority directions and development strategies of Ukraine: abstracts of reports of the III International scientific and practical online conference, Kyiv, 1, 371–373.
- 8. Davitadze N, Bejanidze I. 2012. Effective way to obtain food fiber by membrane methods technology. Second International Conference of young scientists “Chemistry today. ICYC– 2012. 21–23 April 2012. Tbilisi. Collection of works of International Conference, 29–31
- 9. Durán-Aranguren D.D., Ramírez C.J., Díaz L., Valderrama M.A., Sierra R. 2022. Pectins – the new-old polysaccharides: production of pectin from citrus residues: process alternatives and insights on its integration under the biorefinery concept. http://dx.doi.org/10.5772/intechopen.100153
- 10. Davitadze N., Bejanidze I., Tsintsadze M.. 2022. High quality pectin from citrus juice waste. Book of Abstracts Kyiv Conference on Analytical Chemistry Modern Trends, 2, 53–59.
- 11. Davitadze N., Bejanidze I., Tsintsadze M.. 2023. Electrodialysis in pectin production technology. Tbilisi, Chemistry Advances and Prospects, 1, 0–20.
- 12. Davitadze N., Bejanidze I.M. Tsintsadze..2023. Development of technology for the extraction of natural pectin from juice production waste. Ecological Engineering & Environmental Technology, 24(5), 117–130.
- 13. Davitadze N., Bejanidze I. 2023.valorization of citrus fruit processing waste. SGEM Multidisciplinary Scientific GeoConference (SWS Scholarly Societ ) Albena Resort & Spa, Bulgaria y Vienna), 1–2, 7.
- 14. Fidalgo A., Ciriminna R., Carnaroglio D., et al. 2016. Eco-friendly extraction of pectin and essential oils from orange and lemon peels. ACS Sustain Chem Eng, 4, 2243–2251.
- 15. Güzel M., Akpınar Ö. 2019. Valorisation of fruit by-products: Production characterization of pectins from fruit peels. Food Bioprod Process 2019; 115, 126–133.
- 16. Ilyina S.I., Ravichev L.V., Bykov V.I., Loginov V.Ya., Svittsov A.A., Titov A.A. 2022. Mathematical description of electromass transfer processes. Membranes-2022. XV Anniversary All-Russian Scientific Conference with International Participation. Abstracts of reports. M.RKhTU im. DI.Mendeleev, S., 290–291.
- 17. Kebaili M., Djellali S., Radjai M., et al. Valorization of orange industry residues to form a natural coagulant and adsorbent. J Ind Eng Chem 2018; 64, 292–299.
- 18. Kopylova L.E., Svittsov A.A. 2018. Baromembrane processes in extraction. extraction and membrane methods in the separation of substances: Abstracts of the International Conference Dedicated to the 90th Anniversary of Academician B.A. Purin, Ed. corresponding member RAS E. V. Yurtova. Moscow: RKhTU im. Mendeleev, S., 106.
- 19. Kagramanov G.G., Svittsov A.A., Kashirina O.V. 2013. Unrealized potential. Membrane technology in the world and in Russia. Water use. Water supply. Water disposal, 11(75), 34–38.
- 20. Rodsamran P., Sothornvit R. 2019. Microwave heating extraction of pectin from lime peel: Characterization and properties compared with the conventional heating method. Food Chem, 278, 364–372.
- 21. Sedysheva S.A., Kopylova L.E., Svittsov A.A. 2012. Membrane emulsification in extraction processes. Membranes and membrane technologies, 2(4), 260–275.
- 22. Sebaoui O., Moussaoui R., Kadi H., et al. 2017. Kinetic modeling of pectin extraction from wasted citrus Lemon L. Waste and Biomass Valorization, 8, 2329–2337.
- 23. Senit J.J., Velasco D., Gomez Manrique A., et al. 2019. Orange peel waste upstream integrated processing to terpenes, phenolics, pectin and monosaccharides: Optimization approaches. Ind Crops Prod, 134, 370–381.
- 24. Tovar A.K., Godínez L.A., Espejel F., et al. 2019. Optimization of the integral valorization process for orange peel waste using a design of experiments approach: Production of high-quality pectin and activated carbon. Waste Manag, 85, 202–213.
Uwagi
Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-5cfa6fee-5c51-44ea-a30a-a855aeb0e9e6