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The study compares the microstructure of three commercial dental cobalt matrix alloys with related chemical composition declared by the manufacturer. Casts were produced with lost wax method, then melted and casted with centrifugal induction casting machine. The Co-Cr-Mo alloys were casted according to the manufacturers procedure. The samples’ chemical composition and phase composition, respectively, using WDXRF (Wavelength Dispersive X-Ray Fluorescence) and XRD (X-ray Diffarction) methods were analysed. Casts microstructure by mean of LOM (Light Optical Microscopy), SEM (Scanning Electron Microscopy) and EDS (Energy Dispersive X-ray Spectroscopy) were investigated. Vickers hardness HV10 was measured. Quantitative microstructure evaluation was performed by means of computer image processing. The results of the chemical composition indicate the high stability of the chemical composition for alloy A. In case of alloys B and C, there was a significant difference in carbon content. Quantitative differences in image of microstructure between of castings A and B, C were noticed. The greater amount of precipitates was recorded for castings with higher carbon content. In all investigated castings, the presence of β matrix solution and M23C6 carbide precipitations was found.
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Tom
Strony
76--82
Opis fizyczny
Bibliogr. 23 poz., fig., tab.
Twórcy
autor
- Department of Materials Engineering, Faculty of Mechanical Engineering, Lublin University of Technology, Nadbystrzycka Street 36, 20-618 Lublin, Poland
autor
- Department of Mechanical Engineering and Automation, Faculty of Production Engineering, University of Life Sciences in Lublin, Poland, Głęboka Street 28, 20-612, Lublin, Poland
autor
- Departament of Materials Science, Faculty of Mechanical Engineering and Aeronautics, Rzeszow University of Technology, 2 Wincentego Pola Str., 35-959 Rzeszów, Poland
autor
- Cumhuriyet University, Department of Metallurgical and Materials Engineering, 58140, Sivas, Turkey
autor
- Departament of Materials Science, Faculty of Mechanical Engineering and Aeronautics, Rzeszow University of Technology, 2 Wincentego Pola Str., 35-959 Rzeszów, Poland
autor
- Cumhuriyet University, Department of Metallurgical and Materials Engineering, 58140, Sivas, Turkey
autor
- Department of Mechanical Engineering and Automation, Faculty of Production Engineering, University of Life Sciences in Lublin, Poland, Głęboka Street 28, 20-612, Lublin, Poland
Bibliografia
- 1.Beer, K. et al.: A quality assessment of casting dental prosthesis elements. Eksploatacja i Niezawodnosc – Maintenance and Reliability. 15, 3, 230–236 (2013).
- 2.Beer-Lech, K., Surowska, B.: Research on resistance to corrosive wear of dental CoCrMo alloy containing post-production scrap. Eksploatacja i Niezawodnosc – Maintenance and Reliability. 17, 1, 90–94 (2015).
- 3.Caudillo, M. et al.: On carbide dissolution in an as-cast ASTM F-75 alloy. Journal of Biomedical Materials Research. 59, 2, 378–385 (2002).
- 4.Clemow, A.J.T., Daniell, B.L.: Solution treatment behavior of Co-Cr-Mo alloy. Journal of Biomedical Materials Research. 13, 2, 265–279 (1979).
- 5.Giacchi, J.V. et al.: Microstructural characterization of as-cast biocompatible Co–Cr–Mo alloys. Materials Characterization. 62, 1, 53–61 (2011).
- 6.Gómez, M. et al.: Relationship between microstructure and ductility of investment cast ASTM F-75 implant alloy. Journal of Biomedical Materials Research. 34, 2, 157–163 (1997).
- 7.Henriques, B. et al.: Microstructure, hardness, corrosion resistance and porcelain shear bond strength comparison between cast and hot pressed CoCrMo alloy for metal–ceramic dental restorations. Journal of the Mechanical Behavior of Biomedical Materials. 12, 83–92 (2012).
- 8.Knosp, H. et al.: Gold in dentistry: Alloys, uses and performance. Gold Bull. 36, 3, 93–102 (2003).
- 9.Kohn, D.H.: Metals in medical applications. Current Opinion in Solid State and Materials Science. 3, 3, 309–316 (1998).
- 10.Lu, Y. et al.: Nickel-based (Ni–Cr and Ni–Cr–Be) alloys used in dental restorations may be a potential cause for immune-mediated hypersensitivity. Medical hypotheses. 73, 5, 716–717 (2009).
- 11.Mancha, H. et al.: M23C6 carbide dissolution mechanisms during heat treatment of ASTM F-75 implant alloys. Metall and Mat Trans A. 32, 4, 979–984 (2001).
- 12.Marciniak, J.: Biomateriały w stomatologii. Wydawnictwo Politechniki Śląskiej, Gliwice (2008).
- 13.Mineta, S. et al.: Phase and Formation/Dissolution of Precipitates in Biomedical Co-Cr-Mo Alloys with Nitrogen Addition. Metallurgical and Materials Transactions A. 44, 494–503 (2013).
- 14.Montero-Ocampo, C., Salinas Rodriguez, A.: Effect of carbon content on the resistance to localized corrosion of as-cast cobalt-based alloys in an aqueous chloride solution. Journal of Biomedical Materials Research. 29, 4, 441–453 (1995).
- 15.Narushima, T. et al.: Precipitates in Biomedical Co-Cr Alloys. JOM. 65, 4, 489–504 (2013).
- 16.Rosenthal, R. et al.: Phase characterization in as-cast F-75 Co–Cr–Mo–C alloy. Journal of Materials Science. 45, 15, 4021–4028 (2010).
- 17.Walczak, M. et al.: Effect of recasting on the useful properties CoCrMoW alloy. Eksploatacja i Niezawodnosc – Maintenance and Reliability. 16, 2, 330–336 (2014).
- 18.Walczak, M. et al.: The issue of using remelted CoCrMo alloys in dental prosthetics. Archives of Civil and Mechanical Engineering. 12, 2, 171–177 (2012).
- 19.Zangeneh, S. et al.: Microstructure and tribological characteristics of aged Co–28Cr–5Mo–0.3C alloy. Materials & Design. 37, 292–303 (2012).
- 20.ASTM F75 – Standard Specification for Cobalt-28 Chromium-6 Molybdenum Alloy Castings and Casting Alloy for Surgical Implants (UNS R30075).
- 21.BEGO – Partners in progress, http://www.bego.com/.
- 22.Feguramed GmbH, http://www.feguramed.de/.
- 23.Interdent s.r.o., http://www.interdent.cz/.
Uwagi
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017)
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-5a40477b-bacb-4eb4-ac50-f08aa8577fff