Investigations of the structure and properties of PVD coatings deposited onto sintered tool materials

• Autorzy: Pakuła D. , Staszuk M. , Dobrzański L. A.
• Języki publikacji: EN

Abstrakty

EN

Purpose: The paper presents investigation results of the structure and properties of the coatings deposited by cathodic arc evaporation - physical vapour deposition (CAE-PVD) techniques on the sialon tool ceramics. The Ti(B,N), Ti(C,N), (Ti,Zr)N, (Ti,Al)N and multilayer (Al,Cr)N+(Ti,Al)N, (Ti,Al)N+(Al,Cr)N coatings were investigated. Design/methodology/approach: The structural investigation includes the metallographic analysis on the scanning electron microscope. Examinations of the chemical compositions of the deposited coatings were carried out using the X-ray energy dispersive spectrograph EDS. The investigation includes also analysis of the mechanical and functional properties of the material: microhardness tests of the deposited coatings, surface roughness tests, evaluation of the adhesion of the deposited coatings and tribological test made with the „pin-on-disk”. Findings: Deposition of the multicomponent coatings with the PVD method, on tools made from sialon’s ceramics, results in the increase of mechanical properties in comparison with uncoated tool materials, deciding thus the improvement of their working properties. Practical implications: The multicomponent coating carried out on multi point inserts (made on sintered sialon’s ceramics) can be used in the pro-ecological dry cutting processes without using cutting fluids. However, application of this coating to cover sialon ceramics demands still both elaborating and improvement adhesion to substrates in order to introduce these to industrial applications. Originality/value: The paper presents some researches of multicomponent coatings deposited by PVD method on sialon tool ceramics

Słowa kluczowe

EN

thin and thick coatings; tool materials; PVD; multicomponent coatings

PL

cienkie i grube powłoki; materiały narzędziowe; PVD; powłoka wieloskładnikowa

• Wydawca: International OCSCO World Press
• Czasopismo: Archives of Materials Science and Engineering
• Rocznik: 2012
• Tom: Vol. 58, nr 2
• Strony: 219--226
• Opis fizyczny: Bibliogr. 33 poz.

Twórcy

autor

Pakuła D.

• Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Staszuk M.

• Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

autor

Dobrzański L. A.

• Division of Materials Processing Technology, Management and Computer Techniques in Materials Science, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland

Bibliografia

• [1] A.E. Reiter, V.H. Derflinger, B. Hanselmann, T. Bachmann, B. Sartory, Investigation of the properties of Al1-xCrxN coatings prepared by cathodic arc evaporation, Surface and Coatings Technology 200 (2005) 2114-2122.
• [2] W. Kwaśny, Predicting properties of PVD and CVD coatings based on fractal quantities describing their surface, Journal of Achievements in Materials and Manufacturing Engineering 37/2 (2009) 125-192.
• [3] L.A. Dobrzański, D. Pakuła, Comparison of the structure and properties of the PVD and CVD coatings deposited on nitride tool ceramics, Journal of Materials Processing Technology 164-165 (2005) 832-842.
• [4] D. Pakuła, L.A. Dobrzański, K. Gołombek, M. Pancielejko, A. Križ, Structure and properties of the Si3N4 nitride ceramics with hard wear resistant coatings, Journal of Materials Processing Technology 157-158 (2004) 388-393.
• [5] D. Pakuła, M. Staszuk, Multilayer and multicomponent PVD coatings deposited on the ceramic tool materials, Proceedings of the 10th Conference on “Coatings and Layers”, Rožnov pod Radhoštem, 2011, 129-134.
• [6] A.E. Reiter, V.H. Derflinger, B. Hanselmann, T. Bachmann, B. Sartory, Investigation of the properties of Al1-xCrxN coatings prepared by cathodic arc evaporation, Surface and Coatings Technology 200 (2005) 2114-2122.
• [7] B.A. Movchan, K.Yu. Yakovchuk, Graded thermal barrier coatings, deposited by EB-PVD, Surface and Coatings Technology 188-189 (2004) 85-92.
• [8] D. Pakuła, L.A. Dobrzański, A. Križ, M. Staszuk, Investigation of PVD coatings deposited on the Si3N4 and sialon tool ceramics, Archives of Materials Science and Engineering 46/1 (2010) 53-60.
• [9] D. Pakuła, L.A. Dobrzański, K. Gołombek,
• M. Pancielejko, A. Križ, Structure and properties of the Si3N4 nitride ceramics with hard wear resistant coatings, Journal of Materials Processing Technology 157-158 (2004) 388-393.
• [10] L.A. Dobrzański, D. Pakuła, E. Hajduczek, Structure and properties of the multi component TiAlSiN coatings obtained in the PVD process in the nitride tool ceramics, Journal of Materials Processing Technology 157-158 (2004) 331-340.
• [11] L.A. Dobrzański, D. Pakuła, A. Križ, M. Sokovic, J. Kopac, Tribological properties of the PVD and CVD coatings deposited onto the nitride tool ceramics, Journal of Materials Processing Technology 175 (2006) 179-185.
• [12] L.A. Dobrzański, D. Pakuła, Comparison of the structure and properties of the PVD and CVD coatings deposited on nitride tool ceramics, Journal of Materials Processing Technology 164-165 (2005) 832-842.
• [13] L.A. Dobrzański, D. Pakuła, Structure and properties of the wear resistant coatings obtained in the PVD and CVD processes on tool ceramics, Materials Science Forum 513 (2006) 119-133.
• [14]L.A. Dobrzański, M. Staszuk, K. Gołombek, A. Śliwa, M. Pancielejko, Structure and properties PVD and CVD coatings deposited onto edges of sintered cutting tools, Archives of Metallurgy and Materials 55/1 (2010) 187-193.
• [15]L.A. Dobrzański, M. Staszuk, PVD and CVD gradient coatings on sintered carbides and sialon tool ceramics, Journal of Achievements in Materials and Manufacturing Engineering 43/2 (2010) 552-576.
• [16]M. Betiuk, T. Borowski, K. Burdyński, The (Ti,Al)N, (Ti,Al)C and (Ti,Al)CN multicompound coatings synthesis in low pressure of DC arc discharge, Engineering Materials 6 (2008) 674-678 (in Polish).
• [17]M. Cłapa D. Batory, Improving adhesion and wear resista-nce of carbon coatings using TiC gradient layers, Journal of Achievements in Materials and Manufacturing Engineering 20 (2007) 415-418.
• [18]M. Sokovic, J. Kopac, L.A. Dobrzański, J. Mikuła, K. Gołombek, D. Pakuła, Cutting characteristics of PVD and CVD - Coated ceramic tool inserts, Tribology in Industry 28/1-2 (2006) 3-8.
• [19]M. Staszuk, The structure and properties of PVD and CVD gradient coatings deposited on sialons and sintered carbides. PhD Thesis, Silesian University of Technology Library, Gliwice, 2009 (in Polish).
• [20]M. Wysiecki, Contemporary Tool Materials, WNT, Warsaw, 1997, (in Polish).
• [21]S. PalDey, S.C. Deevi, Properties of single layer and gradient (Ti,Al)N coatings, Materials Science and Engineering A361 (2003) 1-8.
• [22]Shuichi Kawno, Junichi Takahashi, Shiro Shimada, The preparation and spark plasma sintering of silicon nitride-based materials coated with nano-sized TiN, Journal of the European Ceramic Society 24 (2004) 309-312.
• [23]T. Liu, C. Dong, S. Wu, K. Tang, J. Wang, J. Jia, TiN gradient and Ti/TiN multi-layer protective coatings on Uranium, Surface and Coating Technology 201 (2007) 6737-6741.
• [24]T. Wierzchoń, Structure and properties of multicomponent and composite layers produced by combined surface engineering methods, Surface and Coatings Technology 180-181 (2004) 458-464.
• [25]Yin-Yu Chang, Da-Yung Wang, Chi-Yung Hung, Structural and mechanical properties of nanolayered TiAlN/CrN coatings synthesized by a cathodic arc deposition process, Surface and Coatings Technology 200 (2005) 1702-1708.
• [26]L. Cunha, et al, Effect of thermal treatments on the structure of MoNxOy thin films, Vacuum 82/12 (2008) 1428-1432.
• [27]D. Pakuła, Structure and properties of multicomponent coatings deposited onto sialon tool ceramics, Archives of Materials Science and Engineering 52/1 (2011) 54-60.
• [28]L.A. Dobrzański, M. Staszuk, J. Konieczny, W. Kwaśny, M. Pawlyta, Structure of TiBN coatings deposited onto cemented carbides and sialon tool ceramics, Archives of Materials Science and Engineering 38/1 (2009) 48-54.
• [29]L.A. Dobrzański, D. Pakuła, J. Mikuła, K. Gołombek, Investigation of the structure and properties of coatings deposited on ceramic tool materials, International Journal of Surface Science and Engineering 1/1 (2007) 111-124.
• [30]M. Pancielejko, W. Precht, A. Czyżniewski, Tribological properties of PVD titanium carbides, Vacuum 53 (1999) 57-60.
• [31]W. Precht, M. Pancielejko, A. Czyżniewski, Structure and tribological properties of carbon and carbon nitride films, obtained by the ARC method, Vacuum 53 (1999) 109-112. [32]M. Pancielejko, A. Czyżniewski, V. Zavaleyev, A. Pander, K. Wojtalik, Optimization of the deposition parameters of DLC coatings with the MCVA method, Archives of Materials Science and Engineering, 54/2 (2012) 60-67.
• [33]A.D. Dobrzańska-Danikiewicz, K. Gołombek, D. Pakuła, J. Mikuła, M. Staszuk, L.W. Żukowska, Long-term development directions of PVD/CVD coatings deposited onto sintered tool materials, Archives of Materials Science and Engineering 49/2 (2011) 69-96.