Effect of electrochemical treatment in eutectic solvent and deposition of SiO2 sol-gel coating on corrosion resistance of 316L steel in Ringer’s solution

• Autorzy: Mazur-Nowacka Anna , Marczewski Marek , Tylus Włodzimierz , Szczygieł Bogdan , Chęcmanowski Jacek

Identyfikatory

DOI

10.15199/40.2022.5.3

Warianty tytułu

PL

Wpływ obróbki elektrochemicznej w rozpuszczalniku eutektycznym oraz osadzenia powłoki zol-żelowej SiO2 na odporność korozyjną stali 316L w roztworze Ringera

• Języki publikacji: EN

Abstrakty

EN

The 316L stainless steel samples were subjected to anodic polarization in a eutectic solvent and then theSiO2 coatings were deposited on them using the sol-gel method. The coatings were prepared from a sol containing TEOS as a precursor and ethanol as a solvent. The obtained samples were exposed in Ringer’s solution. Studies have shown that electrochemical treatment of 316L steel affects both the morphology, topography and roughness of the metallic material. Potentiodynamic tests showed that the best barrier properties after exposure to Ringer’s solution were obtained for 316L steel subjected to electrochemical treatment, additionally covered with a SiO2 coating. The deposition of the three-layer SiO2 coatings reduces the corrosion current density and an increase in the polarization resistance relative to the uncoated 316L steel.

PL

Próbki ze stali nierdzewnej 316L poddano polaryzacji anodowej w rozpuszczalniku eutektycznym, a następnie metodą zol-żel osadzono na nich powłoki SiO2. Powłoki otrzymywano z zolu zawierającego TEOS jako prekursor i etanol jako rozpuszczalnik. Otrzymane próbki eksponowano w roztworze Ringera. Badania dowiodły, że elektrochemiczna obróbka stali 316L wpływa zarówno na morfologię oraz topografię, jak i chropowatość materiału metalicznego. Potencjodynamiczne badania wykazały, że najlepsze właściwości barierowe po ekspozycji w roztworze Ringera uzyskano dla stali 316L poddanej obróbce elektrochemicznej i dodatkowo pokrytej powłoką SiO2. Osadzenie trójwarstwowych powłok SiO2 powoduje zmniejszenie gęstości prądu korozji oraz wzrost oporu polaryzacji względem niepokrytej stali 316L.

Słowa kluczowe

EN

corrosion resistance; electrochemical treatment; sol-gel method; ceramic coating; silica dioxide; Ringer’s solution

PL

odporność na korozję; obróbka elektrochemiczna; metoda zol-żel; powłoka ceramiczna; ditlenek krzemu; roztwór Ringera

• Wydawca: Wydawnictwo SIGMA-NOT
• Czasopismo: Ochrona przed Korozją
• Rocznik: 2022
• Tom: nr 5
• Strony: 152--156
• Opis fizyczny: Bibliogr. 25 poz., fot., wykr.

Twórcy

autor

Mazur-Nowacka Anna

• Department of Adwenced Materials Technologies, Faculty of Chemistry, Wrocław University of Science and Technology, Smoluchowskiego 25, 50-370 Wrocław, Poland

• https://orcid.org/0000-0002-3644-0855

autor

Marczewski Marek

• Department of Adwenced Materials Technologies, Faculty of Chemistry, Wrocław University of Science and Technology, Smoluchowskiego 25, 50-370 Wrocław, Poland

• https://orcid.org/0000-0002-2728-5363

autor

Tylus Włodzimierz

• Department of Adwenced Materials Technologies, Faculty of Chemistry, Wrocław University of Science and Technology, Smoluchowskiego 25, 50-370 Wrocław, Poland

• https://orcid.org/0000-0001-6780-5100

autor

Szczygieł Bogdan

• Department of Adwenced Materials Technologies, Faculty of Chemistry, Wrocław University of Science and Technology, Smoluchowskiego 25, 50-370 Wrocław, Poland

• https://orcid.org/0000-0003-3107-8778

autor

Chęcmanowski Jacek

• Department of Adwenced Materials Technologies, Faculty of Chemistry, Wrocław University of Science and Technology, Smoluchowskiego 25, 50-370 Wrocław, Poland

• https://orcid.org/0000-0001-7344-580X

Bibliografia

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Uwagi

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).