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Purpose: The main aim of this work was to determine structure and properties massive Fe-C materials obtained by mechanical alloying and sintering. Design/methodology/approach: The results of experiments on the fabrication of powders materials and solid materials using pure iron and graphite powders are presented. The powders of the Fe-C alloys obtained by mechanical alloying method and after that the powders were sintering. The sintering process was conducted by using the impulse-plasma method. In this article the usability of mechanical alloying method and sintering to produce the massive materials were presented. Findings: The laboratory tests show that, by using the mechanical alloying method, one can produce powder of Fe-6.67% mass.C alloy with intentional chemical constitution and desirable structure. The structure of the materials is homogeneous and fine-grained and inside the materials didn’t find some impurities and undesirable phases. The sintering by using the impulse-plasma method makes the sinters with close to theoretical density with non-variable nanocrystaline microstructure possible. The hardness of the sinters was 1300 HV. Research limitations/implications: The mechanical alloying method is one of the techniques which enables to improve property of Fe-C alloys. It is possible by refinement of structure and modification of phases composition. Nanocrystaline size of grain is advisable to make it in correct technology of producing massive materials with nanocrystaline structure. All of the presented experiments in this article are conducted on a laboratory scale. At the present time, all over the world, the mechanical alloying and the sintering processes of nanocrystaline materials are only just in the laboratory scientific research. In the nearest future the producing of nanomaterials will take place not only in the laboratory and move to the industry. Originality/value: The nanomaterials have an unusual mechanical, physical and chemical properties.
Wydawca
Rocznik
Tom
Strony
167--170
Opis fizyczny
Bibliogr. 16 poz., rys., tab., wykr.
Twórcy
autor
- Division of Nanocrystalline and Functional Materials and Sustainable Pro-ecological Technologies, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
autor
- Division of Nanocrystalline and Functional Materials and Sustainable Pro-ecological Technologies, Institute of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
Bibliografia
- [1] R. Nowosielski, W. Pilarczyk, Structure and properties of Fe-6,67%C alloy obtained by mechanical alloying, Journal of Materials Processing Technology 162-163 (2005) 373-378.
- [2] R. Nowosielski, W. Pilarczyk, Structure and properties of metallic powders Co78B11Si11 obtained by mechanical alloying, Proceedings of the 12th Scientific International Conference „Achievements in Mechanical and Materials Engineering” AMME’2003, Gliwice-Zakopane, 2003, 675-680.
- [3] M. Jurczyk, Mechanical Alloying, Published by Poznan University of Technology, 2003, (in Polish).
- [4] J. Nowacki, Sintered metals and composites with metallic matrix, WNT, Warsaw, 2005, (in Polish).
- [5] A. Michalski, M. Rosiński, J. Jaroszewicz, D. Oleszak, Sintering of nanocrystalline powders by high current electric impulses, Archives of Materials Science 24 (2003) 547-560.
- [6] T. Lou, B. Ding, X. Gu, G. Li, Z. Hu, Mechanical alloying of Fe-Nb-C materials, Materials Letters 28 (1996) 129-132.
- [7] A. Michalski, J. Jaroszewicz, M. Rosiński, The synthesis of NiAl using the pulse plasma method with the participation of the SHS reaction, International Journal of Self-Propagating High-Temperature Synthesis 12 (2003) 237-246.
- [8] N.T. Rochman, K. Kawamoto, H. Sueyoshi, Y. Nakamura, T. Nishida, Effect of milling temperature and additive elements on an Fe-C system alloy prepared by mechanical alloying, Journal of Materials Processing Technology 89-90 (1999) 367-372.
- [9] G.M. Wang, S.J. Campbell, A. Calka, W.A. Kaczmarek, Ball-milling of Fe-C (20-75% Fe), NanoStructured Materials, 6 (1995) 389-392.
- [10] H. Hidaka, T. Tsuchiyama, S. Takaki, Relation between microstructure and hardness in Fe-C alloys with ultra fine grained structure, Scripta Materiala 44 (2001) 1503-1506.
- [11] L. Lü, M.O. Lai, S. Zhang, Modeling of the mechanical alloying process, Journal of Materials Processing Technology 52 (1995) 539-546.
- [12] L. Lü, M.O. Lai, S. Zhang, Diffusion in mechanical alloying, Journal of Materials Processing Technology 67 (1997) 100-104.
- [13] C. Suryanarayana, Mechanical alloying and milling, Progress in Materials Science 46 (2001) 1-184.
- [14] P. Matteazzi, Gerard Le Caër, A. Mocellin, Synthesis of nanostructured materials by mechanical alloying, Ceramics International 23 (1997) 39-44.
- [15] M. Jurczyk, Nanomaterials, Published by Poznan University of Technology, 2001, (in Polish).
- [16] J.W. Kaczmar, K. Pietrzak, W. Włosiński, The production and application of metal matrix composite materials, Journal of Materials Processing Technology 106 (2000) 58-67.
Typ dokumentu
Bibliografia
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bwmeta1.element.baztech-59a92968-2657-43c4-9c62-38505f1f4e1a