Synthesis of Nano-Calcium Fluoride–Based Materials from Phosphogypsum Waste and their Use in Wastewater Treatment–Adsorption of Reactive Blue 21 Dyes

Bensemlali, Meryem; Hatimi, Badreddine; Mortadi, Halima; Chajri, Fatima-Zahra; Aarfane, Abdellatif; Mohammed, El Idrissi; Joudi, Meryeme; Labjar, Najoua; Nasrellah, Hamid; Bakasse, Mina

doi:10.12911/22998993/189763

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Tytuł artykułu

Synthesis of Nano-Calcium Fluoride–Based Materials from Phosphogypsum Waste and their Use in Wastewater Treatment–Adsorption of Reactive Blue 21 Dyes

Autorzy

Bensemlali Meryem , Hatimi Badreddine , Mortadi Halima , Chajri Fatima-Zahra , Aarfane Abdellatif , Mohammed El Idrissi , Joudi Meryeme , Labjar Najoua , Nasrellah Hamid , Bakasse Mina

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DOI

10.12911/22998993/189763

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Abstrakty

A novel synthesis process and characterization of nano-calcium fluoride (n-CaF₂) single crystal prepared from phosphogypsum waste. The phosphogypsum (CaSO₄ 2H₂O) powder has been mechanically mixed with NH₄F in presence of a controlled amount of water. The mixture still sintered for 48 hours until the formation of nano calcium fluoride particles. The n-CaF₂ particles have been characterized by several techniques, The techniques utilized included X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). Therefore, it was confirmed that very pure n-CaF₂ was obtained with a Ca/F ratio of 0.5 and an average crystalizing size measured according to the Debye-Scherrer equation of 11 nm. Based on the findings reached, The characterization data revealed successful synthesis of n-CaF₂ from phosphogypsum. Additionally, the adsorption performance of the elaborated n-CaF₂ was tested in Reactive Blue 21 (RB21) anionic dye removal, Adsorption tests were conducted in a batch reactor, focusing on key factors such as contact time, which can significantly influence the adsorption results. adsorption amount, pH, and dye concentration were tested. Hence results show an important adsorption performance of n-CaF₂ with Reactive Blue 21 removal rate up to 90%.

Słowa kluczowe

phosphogypsum waste nano-calcium fluoride wastewater Reactive Blue 21 adsorption

Wydawca

Polskie Towarzystwo Inżynierii Ekologicznej
Lublin University of Technology

Czasopismo

Journal of Ecological Engineering

Rocznik

2024

Tom

Vol. 25, nr 8

Strony

62--71

Opis fizyczny

Bibliogr. 38 poz., rys., tab.

Twórcy

autor

Bensemlali Meryem

bensemlali.meryem@gmail.com

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco

https://orcid.org/0000-0002-4860-4829

autor

Hatimi Badreddine

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco

https://orcid.org/0000-0001-9200-2334

autor

Mortadi Halima

Faculty of Sciences, University Chouaib Doukkali, Chemistry Department, Laboratory of Materials’ Physical, Chemicals, El Jadida, Morocco

autor

Chajri Fatima-Zahra

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco

autor

Aarfane Abdellatif

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco
Higher School of Education and Training, Chouaib Doukkali University, Morocco

autor

Mohammed El Idrissi

Laboratory of Chemical Processes and Applied Materials, Polydisciplinary Faculty, Sultan Moulay Slimane University, Beni-Mellal, Morocco

autor

Joudi Meryeme

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco

autor

Labjar Najoua

Laboratory of Spectroscopy, Molecular Modelling, Materials, Nanomaterials, Water and Environnement, ENSAM University Mohammed V in Rabat, Morocco

autor

Nasrellah Hamid

nasrellah.h@ucd.ac.ma

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco
Higher School of Education and Training, Chouaib Doukkali University, Morocco

https://orcid.org/0000-0002-9224-2220

autor

Bakasse Mina

Laboratory of Organic Bioorganic and Environmental Chemistry, Chouaib Doukkali University.Morocco

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