Quantitative evaluation and chromatographic fingerprinting for the quality assessment of Pudilan tablet

• Autorzy: Lu Mengya , Tang Qianqian , Zhou Chenyu , Fang Zhizheng , Fan Zheng , Li Xiangyu , Han Rongchun , Tong Xiaohui

Identyfikatory

DOI

10.1556/1326.2022.01084

• Języki publikacji: EN

Abstrakty

EN

An easy, quick, and sensitive approach adopting ultra-performance liquid chromatography (UPLC) equipped with diode array detector was used to analyze and systematically evaluate the quality of Pudilan tablets manufactured by 12 distinct pharmaceutical companies. In this research, 15 peaks were chosen as the common peaks to assess the similarities for different batches (S1–S43) of Pudilan tablet samples. In comparison with the control fingerprint, similarity values for 43 batches of samples exceeded 0.922. In addition, by analyzing the reference substances of epigoitrin, caffeic acid, chlorogenic acid, acetylcorynoline, baicalin and baicanshialein, the chromatogram of the 6 reference substances was established. The recoveries for the reference substances which demonstrated good regression in the linear range (r² > 0.999) were in the range of 98.3–101.1%. The results demonstrated that the established method was highly accurate, efficient and reliable. This study provides a valid, dependable and pragmatic method to evaluate the quality of Pudilan tablet.

Słowa kluczowe

EN

UPLC; Pudilan tablet; chromatographic fingerprinting; quality control; chlorogenic acid

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2023
• Tom: Vol. 35, no. 4
• Strony: 338--346
• Opis fizyczny: Bibliogr. 36 poz., rys., tab., wykr.

Twórcy

autor

Lu Mengya

• School of Pharmacy, Anhui University of Chinese Medicine, Hefei 230012, China

autor

Tang Qianqian

• School of Pharmacy, Anhui University of Chinese Medicine, Hefei 230012, China

autor

Zhou Chenyu

• School of Pharmacy, Anhui University of Chinese Medicine, Hefei 230012, China

autor

Fang Zhizheng

• School of Pharmacy, Anhui University of Chinese Medicine, Hefei 230012, China

autor

Fan Zheng

• Medical Department, Taihe Hospital of Chinese Medicine, Taihe 236600, China

autor

Li Xiangyu

• Department of Research and Development, Anhui Jiren Pharmaceutical Company, Bozhou 236800, China

autor

Han Rongchun

• School of Pharmacy, Anhui University of Chinese Medicine, Hefei 230012, China

• https://orcid.org/0000-0001-7520-9413

autor

Tong Xiaohui

• School of Life Sciences, Anhui University of Chinese Medicine, Hefei 230012, China

• https://orcid.org/0000-0001-8815-1230

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