Comparison of Matrix Solid-Phase Dispersion and Liquid—Solid Extraction Methods Followed by Solid-Phase Extraction in the Analysis of Selected Furanocoumarins from Pimpinella Roots by HPLC—DAD

• Autorzy: Oniszczuk A. , Waksmundzka-Hajnos M. , Podgórski R. , Nowak R. , Żukiewicz-Sobczak W. , Blicharski T.
• Języki publikacji: EN

Abstrakty

EN

The use of matrix solid-phase dispersion (MSPD) was tested to extract some coumarins (umbelliferone, xanthotoxin, isopimpinellin, bergapten, and pimpinellin) from Pimpinella roots. The method was compared with liquid—solid extraction methods (LSE) such as accelerated solvent extraction (ASE), ultrasound-assisted extraction (USAE) and Soxhlet extraction followed by solid-phase extraction (SPE). Several methanol concentrations and temperature conditions were examined during the liquid—solid extraction techniques. The analysis was performed by high-performance liquid chromatography with diode array detector (HPLC—DAD). MSPD extracted furanocoumarins with satisfactory recoveries ranging from 91.65% to 97.55% and relative standard deviations lower than 5,0415%. The results presented in the paper reveal that MSPD is an efficient, fast, simple and easy-to-perform method suitable for the isolation of furanocoumarins from herbs.

Słowa kluczowe

EN

matrix solid-phase dispersion; solid-liquid extraction; solid phase; extraction; Pimpinella saxifraga L; furanocoumarins; high-performance liquid; chromatography

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2015
• Tom: Vol. 27, no. 4
• Strony: 687--696
• Opis fizyczny: Bibliogr. 22 poz., rys., tab.

Twórcy

autor

Oniszczuk A.

• Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland

autor

Waksmundzka-Hajnos M.

• Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland

autor

Podgórski R.

• Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland

autor

Nowak R.

• Department of Pharmaceutical Botany, Medical University in Lublin, 1 Chodzki Street, 20-093 Lublin, Poland

autor

Żukiewicz-Sobczak W.

• Department of Allergology and Environmental Hazards, Institute of Rural Health, 2 Jaczewskiego Street, 20-090 Lublin, Poland

autor

Blicharski T.

• Department of Rehabilitation and Orthopedics, Medical University in Lublin, 8 Jaczewskiego Street, 20-954 Lublin, Poland

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