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Comparison of Matrix Solid-Phase Dispersion and Liquid—Solid Extraction Methods Followed by Solid-Phase Extraction in the Analysis of Selected Furanocoumarins from Pimpinella Roots by HPLC—DAD

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The use of matrix solid-phase dispersion (MSPD) was tested to extract some coumarins (umbelliferone, xanthotoxin, isopimpinellin, bergapten, and pimpinellin) from Pimpinella roots. The method was compared with liquid—solid extraction methods (LSE) such as accelerated solvent extraction (ASE), ultrasound-assisted extraction (USAE) and Soxhlet extraction followed by solid-phase extraction (SPE). Several methanol concentrations and temperature conditions were examined during the liquid—solid extraction techniques. The analysis was performed by high-performance liquid chromatography with diode array detector (HPLC—DAD). MSPD extracted furanocoumarins with satisfactory recoveries ranging from 91.65% to 97.55% and relative standard deviations lower than 5,0415%. The results presented in the paper reveal that MSPD is an efficient, fast, simple and easy-to-perform method suitable for the isolation of furanocoumarins from herbs.
Rocznik
Strony
687--696
Opis fizyczny
Bibliogr. 22 poz., rys., tab.
Twórcy
autor
  • Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland
  • Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland
  • Department of Inorganic Chemistry, Medical University in Lublin, 4A Chodzki Street, 20 093 Lublin, Poland
autor
  • Department of Pharmaceutical Botany, Medical University in Lublin, 1 Chodzki Street, 20-093 Lublin, Poland
  • Department of Allergology and Environmental Hazards, Institute of Rural Health, 2 Jaczewskiego Street, 20-090 Lublin, Poland
  • Department of Rehabilitation and Orthopedics, Medical University in Lublin, 8 Jaczewskiego Street, 20-954 Lublin, Poland
Bibliografia
  • [1] S. Redzic, J. Med. Plant. Res., 4, 1003 (2010)
  • [2] T.D. Chermenskaya, E.A. Stepanycheva, A.V. Shchenikova, and A. Chakaeva, Ind. Crops Prod., 32, 157 (2010)
  • [3] Y.Q. Tiana, Z.X. Zhanga, and H.H. Xua, Ind. Crops Prod., 41, 90 (2013)
  • [4] A. Bhatnagar, A.J. Kanwar, D. Parsad, and D. De, J. Eur. Acad. Dermatol. Venerol., 21, 638 (2007)
  • [5] J. Trott, W. Gerber, S. Hammes, and H.M. Ockenfels, Eur. J. Dermatol., 18, 55 (2008)
  • [6] Ł. Cieśla, A. Bogucka-Kocka, M. Hajnos, A. Petruczynik, and M. Waksmundzka-Hajnos, J. Chromatogr. A, 1207, 160 (2008)
  • [7] R. Heinke, K. Franke, A. Porzel, L.A. Wessjohann, N.A. Awadh Ali, and J. Schmidt, Phytochemistry, 72, 929 (2011)
  • [8] C.H. Lee, A.J. Mamela, and E.C. Vonderheid, Int. J. Dermatol., 46, 1198 (2007)
  • [9] M.D. Luque de Castro and M.P. Silva, Trends Anal. Chem., 16 (1997)
  • [10] M. Waksmundzka-Hajnos, A. Petruczynik, A. Dragan, D. Wianowska, and A.L. Dawidowicz, Phytochem. Anal., 15, 313 (2004)
  • [11] A.L. Capriotti, C. Cavaliere, P. Giansanti, R. Gubbiotti, R. Samperi, and A. Laganà, J. Chromatogr. A, 1217, 2521 (2010)
  • [12] T. Visnevschi-Necrasov, C.S. Cunha, E. Nunes, and M.B.P. Oliveira, J. Chromatogr. A, 1216, 3720 (2009)
  • [13] S.A. Baker, J. Chromatogr. A, 880, 63 (2000)
  • [14] S.A. Baker, J. Biochem. Biophys. Meth., 70, 151 (2007)
  • [15] J.Y. Chen, Z. Guo, X. Wang, and C. Qiu, J. Chromatogr. A, 1184, 191 (2008)
  • [16] E.M. Kristenson, U.A. Brinkman, and L. Ramos, Trends Anal. Chem., 25, 96 (2006)
  • [17] M.S. Dopico-Garcia, P. Valentao, A. Jagodzinska, J. Klepczynska, L. Guerra, P.B. Andrade, and R.M. Seabra, Talanta, 74, 20 (2007)
  • [18] M. Garcia-Lopez, P. Canosa, and I. Rodriguez, Anal. Bioanal. Chem., 391, 963 (2008)
  • [19] P.C. Abhilash, S. Jamil, and N. Singh, J. Chromatogr. A, 1176, 43 (2007)
  • [20] A.L. Dawidowicz and E. Rado, J. Pharm. Bioanal. Anal., 52, 79 (2010)
  • [21] A.L. Dawidowicz, D. Wianowska, and E. Rado, Phytochem. Anal., 22, 51 (2011)
  • [22] A. Oniszczuk, M. Waksmundzka-Hajnos, K. Skalicka, and K. Głowniak, Ind. Crops Prod., 50, 131 (2013)
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-567a753a-a2f6-4dfe-8b76-e64da658fe72
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