Gas-sensing properties and in-situ diffuse-reflectance Fourier-transform infrared spectroscopy study of diethyl ether adsorption and reactions on SnO2 film

Wang, N.; Huang, K.; Song, J.

doi:10.1515/msp-2017-0037

Artykuł - szczegóły

Tytuł artykułu

Gas-sensing properties and in-situ diffuse-reflectance Fourier-transform infrared spectroscopy study of diethyl ether adsorption and reactions on SnO2 film

Autorzy

Wang N. , Huang K. , Song J.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1515/msp-2017-0037

Warianty tytułu

Języki publikacji

Abstrakty

Diethyl ether is a common industrial reagent and medical anesthetic. It is necessary to carry out real-time monitoring of this molecule due to its harmful effects on human health. In this paper, a highly sensitive diethyl ether SnO₂ gas-sensing material has been prepared by a sol-gel method. The gas sensitivity was tested by a home-made gas-sensing equipment. The surface adsorption and reaction processes between the SnO₂ gas-sensing film and the diethyl ether have been studied by in situ diffuse-reflectance Fourier-transform infrared spectroscopy (DRFT-IR) at different temperatures. The results show that the SnO₂ gas-sensing material has high sensitivity to diethyl ether, and the lowest detection limit can reach 1 ppm. Furthermore, ethyl (CH₃CH₂•), oxoethyl (CH₃CH₂O•), ethanol (CH₃CH₂OH), formaldehyde (HCHO), acetaldehyde (CH₃CHO), ethylene (C₂H₄), H₂O and CO₂ surface species are formed during diethyl ether adsorption at different temperatures. A possible mechanism of the reaction process is discussed.

Słowa kluczowe

gas sensitivity SnO2 film diethyl ether situ DRFT-IR

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2017

Tom

Vol. 35, No. 2

Strony

265--274

Opis fizyczny

Bibliogr. 55 poz., rys., tab.

Twórcy

autor

Wang N.

State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, P.R. China

autor

Huang K.

huangkaijin@hust.edu.cn

State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, P.R. China
State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, P.R. China

autor

Song J.

State Key Laboratory of Materials Processing and Die & Mould Technology, Huazhong University of Science and Technology, Wuhan 430074, P.R. China

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-55f87e57-fdd6-4c97-af6b-d7dc8b5e8e3a