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Durability of crystalline phase in concrete microstructure modified by the mineral powders: evaluation by nanoindentation tests

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
This paper presents the nanoindentation investigation of the evolution of concrete microstructure modified by the Internal Crystallization Technology mineral powders. The samples under study were retrieved from a fragment of a circular concrete lining of the vertical mine shaft at a depth of approximately 1,000 m. Due to the aggressive environment and exposure to contaminated water, the internal surface of the structure was deteriorated, decreasing its strength significantly. The mineral powders were applied directly on the surface lining. The specimens were investigated one month, three months and one year after the application of the aforementioned substance in order to verify the time dependence of the strengthening processes and durability of the crystalline phase. The microstructural changes of concrete were assessed with the use of nanoindentation technique. The testing procedure involved including the previously cut specimens in the epoxy resin and grinding and polishing in order to reduce the surface roughness. As a result of the nanoindentation tests the hardness as well as Young’s modulus of the material were evaluated. The results were then compared and statistically analyzed. As a consequence, the disintegration time of the crystalline network in the pores of concrete was identified.
Wydawca
Rocznik
Strony
65--74
Opis fizyczny
Bibliogr. 22 poz., rys.
Twórcy
  • Wrocław University of Science and Technology, Faculty of Civil Engineering, Wrocław, Poland
autor
  • Wrocław University of Science and Technology, Faculty of Civil Engineering, Wrocław, Poland
Bibliografia
  • 1. Bobko C.P., 2008, Assessing the mechanical microstructure of shale by nanoindentation: The link between mineral composition and mechanical properties, Doctoral dissertation, Massachusetts Institute of Technology.
  • 2. Boussinesq J., 1885, Applications des potentiels h l’rtude de l’rquilibre et du mouvement des solides 61 astiques, Gauthier-Villars.
  • 3. Constantinides G., Ulm F.J., Van Vliet K., 2003, On the use of nanoindentation for cementitious materials, Materials and Structures, 36(3), 191–196.
  • 4. Constantinides G., Chandran K.R., Ulm F.J., Van Vliet K.J., 2006, Grid indentation analysis of composite microstructure and mechanics: principles and validation, Materials Science and Engineering: A, 430(1), 189–202.
  • 5. Doerner M.F., Nix W.D., 1986, A method for interpreting the data from depth-sensing indentation instruments, Journal of Materials Research, 1(04), 601–609.
  • 6. Fan Z., Swadener J.G., Rho J.Y., Roy M.E., Pharr G.M., 2002, Anisotropic properties of human tibial cortical bone as measured by nanoindentation. Journal of Orthopaedic Research, 20(4), 806–810.
  • 7. Krakowiak K.J., Lourenço P.B., Ulm F.J., 2011, Multitechnique investigation of extruded clay brick microstructure, Journal of the American Ceramic Society, 94(9), 3012–3022.
  • 8. Krakowiak K.J., 2011, Assessment of the mechanical microstructure of masonry clay brick by nanoindentation.
  • 9. Mondal P., Shah S., Marks L., Gaitero J., 2010, Comparative study of the effects of microsilica and nanosilica in concrete, Transportation Research Record: Journal of the Transportation Research Board, 2141, 6–9.
  • 10. Němeček J., Kopecký L., Bittnar Z., 2005, Size effect in nanoindentation of cement paste, [in:] Proceedings of the International Conference on Applications of Nanotechnology in Concrete Design, Eds. Dhir, RK, 47–53.
  • 11. Nežerka V., Němeček J., Slížková Z., Tesárek P., 2015, Investigation of crushed brick-matrix interface in lime-based ancient mortar by microscopy and nanoindentation, Cement and Concrete Composites, 55, 122–128.
  • 12. Oliver W.C., Pharr G.M., 2004, Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology, Journal of Materials Research, 19(01), 3–20.
  • 13. Pharr G.M., Oliver W.C., 1992, Measurement of thin film mechanical properties using nanoindentation, Mrs Bulletin, 17(07), 28–33.
  • 14. Rho J.Y., Tsui T.Y., Pharr G.M., 1997, Elastic properties of human cortical and trabecular lamellar bone measured by nanoindentation, Biomaterials, 18(20), 1325–1330.
  • 15. Rho J.Y., Zioupos P., Currey J.D., Pharr G.M., 2002, Microstructural elasticity and regional heterogeneity in human femoral bone of various ages examined by nano-indentation, Journal of Biomechanics, 35(2), 189–198.
  • 16. Sorelli L., Constantinides G., Ulm F.J., Toutlemonde F., 2008, The nano-mechanical signature of ultra-high performance concrete by statistical nanoindentation techniques, Cement and Concrete Research, 38(12), 1447–1456.
  • 17. Syed Asif S.A., Pethica J.B., 1997, Nanoindentation creep of single-crystal tungsten and gallium arsenide, Philosophical Magazine A, 76(6), 1105–1118.
  • 18. Tarefder R., Faisal H., 2013, Nanoindentation characterization of asphalt concrete aging, Journal of Nanomechanics and Micromechanics, 4(1), A4013003.
  • 19. Ulm F.J., Vandamme M., Bobko C., Alberto Ortega J., Tai K., Ortiz C., 2007, Statistical indentation techniques for hydrated nanocomposites: concrete, bone, and shale, Journal of the American Ceramic Society, 90(9), 2677–2692.
  • 20. Vandamme M., 2008, The nanogranular origin of concrete creep: a nanoindentation investigation of microstructure and fundamental properties of calcium-silicate-hydrates, Doctoral dissertation, Massachusetts Institute of Technology.
  • 21. Xiao J., Li W., Sun Z., Lange D.A., Shah S.P., 2013, Properties of interfacial transition zones in recycled aggregate concrete tested by nanoindentation, Cement and Concrete Composites, 37, 276–292.
  • 22. Zadeh V.Z., Bobko C.P., 2013, Nanoscale mechanical properties of concrete containing blast furnace slag and fly ash before and after thermal damage, Cement and Concrete Composites, 37, 215–221.
Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-54ab47e6-e4d4-45c0-b315-3f30aeab8947
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