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Abstrakty
Eladi Gutika is a polyherbal formulation official in “Ayurvedic formulary of India” and used for dry cough and throat infection. A simple, specific and precise high-performance thin-layer chromatography (HPTLC) method has been developed for quantification of piperine and 18-β glycyrrhetinic acid in Eladi Gutika. We report the extraction and estimation of these compounds in a laboratory prepared sample of Eladi Gutika and two of its marketed formulations. The compounds were chromatographed on precoated silica gel G 60254 plates in the mobile phase comprising of toluene, ethyl acetate, and glacial acetic acid. Under the optimized chromatographic conditions, the calibration plot was found to be linear in the range of 0.2–1 g mL-1 with a correlation coefficient R2 = 0.9902 for piperine and 0.9904 for 18-β glycyrrhetinic acid. Mean recovery for piperine was 99.75% w/w and for 18-β glycyrrhetinic acid was 101.36% w/w.
Słowa kluczowe
Czasopismo
Rocznik
Tom
Strony
135--146
Opis fizyczny
Bibliogr. 20 poz., rys., tab.
Twórcy
autor
- Saraswati Vidya Bhawan’s College of Pharmacy Sonarpada, Dombivli (East) 421 204 Maharashtra India
autor
- Saraswati Vidya Bhawan’s College of Pharmacy Sonarpada, Dombivli (East) 421 204 Maharashtra India
autor
- Saraswati Vidya Bhawan’s College of Pharmacy Sonarpada, Dombivli (East) 421 204 Maharashtra India
Bibliografia
- [1] The Ayurvedic Formulary of India, Government of India, Ministry of Health and Family Welfare, Department of Health, New Delhi, 1978, pp. 141–143
- [2] L.D. Kapoor, Handbook of Ayurvedic Medicinal Plants, 1st edn, CRC Publisher, 2005, pp. 264–265
- [3] L.D. Kapoor, Handbook of Ayurvedic Medicinal Plants, 1st edn, CRC Publisher, 2005, pp. 194–195
- [4] P.D. Hamrapurkar, J. Kavita, and Z. Sandip, J. App. Pharm. Sci., 01, 117–120 (2011)
- [5] A. Khajuria, N. Thusa, U. Zusthi, and K.L. Bedi, Indian Drugs, 34, 557–563 (1997)
- [6] K.K. Rout, O.M. Rout, and S.K. Mishra, J. Planar. Chromatogr. Mod. TLC, 20, 447–450 (2007)
- [7] S. Gawas and N.D. Grampurohit, Indian Drugs, 36, 175–180 (1999)
- [8] C.L. Gopu, S. Aher, H. Mehta, A.R. Paradkar, and K.R. Mahadik, Phytochem. Anal., 19, 116–121 (2007)
- [9] S.C. Jain, E. Menghani, and R. Jain, Int. J. Bot., 3, 208–213 (2007)
- [10] A.B. Wood, M.L. Barrow, and D.J. Janes, Flavour Frag. J., 3, 55–64 (1988)
- [11] Baljinder Singh, M. Pankaj, N. Manish, and A. Sheetal, Chromatographia, 70, 1665–1672 (2010)
- [12] S. Esmaaeili, F. Naghibi, M. Mossaddegh, and N. Nadar, Iran. J. Pharm. Res., 2, 137–141 (2006)
- [13] S.B. Song, J.K. Choi, and G.S. Yoo, Arch. Pharm. Res., 13, 174–179 (1990)
- [14] The Ayurvedic Pharmacopoeia of India, 1st edn, Part I, Vol I, Government of India, Ministry of Health and Family Welfare, Department of Health, 1998, pp. 101–127
- [15] W. Epstein and D. Netz, J. Chem. Educ., 70, 598–599 (1993)
- [16] The Merck Index, 11th edn, Merck and Co. Inc., U.S.A, 1989, p. 1186
- [17] Indian Herbal Pharmacopoeia, Revised New Edition, Indian Drug Manufacturers Association, Mumbai, 2002, pp. 306–315
- [18] Indian Herbal Pharmacopoeia Revised New Edition, Indian Drug Manufacturers Association, Mumbai, 2002, pp. 243–249
- [19] Validation of Analytical Procedures, Text and Methodology, ICH Harmonised tripartite guideline-Q2R1, 2005, pp. 1–13
- [20] Indian Pharmacopoeia, volume III, Government of India, Ministry of Health and Family Welfare, Indian Pharmacopoeia Commission, 2007, p. 2057
Typ dokumentu
Bibliografia
Identyfikator YADDA
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