Infrared studies and spectral properties of photochromic high silica glasses

• Autorzy: Girsova M A , Golovina G F , Drozdova I.A. , Polyakova I G , Antropova T V

Identyfikatory

DOI

10.5277/oa140214

• Języki publikacji: EN

Abstrakty

EN

The structure of photochromic high silica glasses (PHSGs) was studied by UV–VIS–NIR and IR spectroscopy, transmission electron microscopy (TEM) and X-ray diffraction (XRD) techniques. PHSG plates were obtained by impregnation of silica porous glasses at first with AgNO3 aqueous solution (in or without the presence of the sensitizers, such as Cu(NO3)2 or Ce(NO3)3), next in the mixed halide salt (NH4Cl, KBr, KI) solution. Then a part of the samples was sintered at temperatures from 850 to 900 °C up to closing of the pores. The results of TEM study have shown that the PHSG plates have two-phase structure with inclusions of the size of 10–100 nm. According to XRD data, the PHSGs contain the AgBr phase. IR spectra confirmed the presence of AgI, AgCl, CeO2, CuCl2, CuCl phases in PHSGs.

Słowa kluczowe

EN

silica porous glass; photochromic high silica glass; transmission electron microscopy TEM; X-ray diffraction; XRD; UV–VIS–IR transmission spectra

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Optica Applicata
• Rocznik: 2014
• Tom: Vol. 44, nr 2
• Strony: 337--344
• Opis fizyczny: Bibliogr. 37 poz., rys., wykr.

Twórcy

autor

Girsova M A

• Grebenshchikov Institute of Silicate Chemistry, RAS, Nab. Makarova 2, 199034, Saint-Petersburg, Russia

autor

Golovina G F

• Grebenshchikov Institute of Silicate Chemistry, RAS, Nab. Makarova 2, 199034, Saint-Petersburg, Russia

autor

Drozdova I.A.

• Grebenshchikov Institute of Silicate Chemistry, RAS, Nab. Makarova 2, 199034, Saint-Petersburg, Russi

autor

Polyakova I G

• Grebenshchikov Institute of Silicate Chemistry, RAS, Nab. Makarova 2, 199034, Saint-Petersburg, Russia

autor

Antropova T V

• Grebenshchikov Institute of Silicate Chemistry, RAS, Nab. Makarova 2, 199034, Saint-Petersburg, Russia

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