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Bound water content measurement in cement pastes by stoichiometric and gravimetric analyses

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
The cement hydration is one of the most complex processes creating the cement matrix. The degree of hydration is a quantity of Portland clinker with gypsum, that as a whole react with water. For purposes of this analysis it was found to be directly proportional to the bound water in the cement paste specimens. Using the gravimetric method the bound water content was determined in samples by calculating the quantitative loss of the dry specimens weight after igniting to 1000°C and keeping the temperature for 5h. Obtained results were collated with theoretical stoichiometric analysis based on the Bogue and Taylor equations and XRD testing for Portland cement, CEM I 42.5. Obtained outcome has confirmed the relationship between the degree of hydration and the bound water content in cement paste. The influence of the w/c ratio and cement oxide components on bound water quantity were also noticed.
Rocznik
Strony
18--25
Opis fizyczny
Bibliogr. 25 poz., rys., tab. wykr.
Twórcy
autor
  • Department of Building Materials Engineering, Faculty of Civil Engineering, Warsaw University of Technology, Al. Armii Ludowej 16, 00-637 Warsaw, Poland
  • Department of Building Materials Engineering, Faculty of Civil Engineering, Warsaw University of Technology, Al. Armii Ludowej 16, 00-637 Warsaw, Poland
Bibliografia
  • Aitcin P.-C., Flatt R.: Science and Technology of Concrete Admixtures. Woodhead Publishing, 2015.
  • Bednarek Z., Krzywobłocka-Laurów R., Drzymała T.: The high temperature influence on structure, phase composition and strength of concrete (in Polish). Zeszyty Naukowe SGSP 38 (2009), 5-27.
  • Bentz P.D, Stutzman E.P.: Curing, hydration, and microstructure of cement paste. ACI Materials Journal 103-M39 (2006), 348-356.
  • Czarnecki L., Broniewski T., Henning O.: Building chemistry (in Polish). Arkady, Warszawa, 1994.
  • Dillshad K.H.A.: Degree of hydration and strength development of low water-to-cement ratios in silica fume cement system. International Journal of Civil & Environmental Engineering 5/11 (2011), 10-16.
  • EN 196-1, 2005. Methods of testing cement. Determination of strength.
  • EN 206, 2013. Concrete. Specification, performance, production and conformity.
  • Fagerlund G.: Chemically bound water as measure of degree of hydration. Method and potential errors. Report TVBM-3150, Lund University, 2009.
  • Gambal P.: The influence of the structure of the copper-slag from the electrical furnace on chosen features of the cement-matrix (in Polish). PhD Thesis, Politechnika Poznańska, Poznań, 2013.
  • Hager I.: Behaviour of cement concrete at high temperature. Bulletin of the Polish Academy of sciences, Technical Sciences 61 (2013), 1-10.
  • Jamroży Z: Concrete technology (in Polish). PWN, Warszawa, 2009.
  • Kurdowski W.: Cement and concrete chemistry. Springer, New York, 2014.
  • Mazgaj M., Piotrowski T.: Improvement of neutron sheilding properties of concrete by innovative material modification. 11th International Symposium on Brittle Matrix Composites "Brittle Matrix Composites 11", Institute of Fundamental Technological Research, Warsaw, 2015
  • Mouret M., Bascoul A., Escadeillas G.: Study of the degree of hydration of concrete by means of image analysis and chemically bound water. Advanced Cement Based Materials 6 (1997), 109-155. http://dx.doi.org/10.1016/S1065-7355(97)90017-1
  • Naus J.D.: The effect of elevated temperature on concrete materials and structures – a literature review. Oak Ridge National Laboratory, 2005.
  • Nocuń-Wczelik W.: The mineral additives influence on heat of hydration of cement (in Polish). Reologia w technologii betonu, Górażdże Cement Group, Gliwice, 2003, 47-58.
  • Peukert S.: Common and special cements (in Polish). Polski Cement, Kraków, 2000.
  • Piotrowski T., Mazgaj M., Żak A., Skubalski J.: Importance of atomic composition and moisture content of cement based composites in neutron radiation shielding. Procedia Engineering 108 (2015), 616-623, 7th Scientific-Technical Conference on Material Problems in Civil Engineering MATBUD'2015. http://dx.doi.org/10.1016/j.proeng.2015.06.188
  • Piotrowski T., Skubalski J.: Analysis of neutrons transport through concrete member and the possibilities of its use in building material investigation (in Polish). Materiały Budowlane 5/501 (2014), 94-96.
  • Piotrowski T., Tefelski D.B., Skubalski J., Żak A.: Experiments on neutron transport through concrete member and the potential for the use in material investigation. Acta Physica Polonica A, 128 (2015), B-13-18. http://dx.doi.org/10.12693/APhysPolA.128.B-14
  • PN-B-06250, 1988. Normal concrete.
  • Tamtsia B.T., Beaudoin J.J.: Basic creep of hardened cement paste a re-examination of the role of water. Cement and Concrete Research 30 (2000), 1465-1475. http://dx.doi.org/10.1016/S0008-8846(00)00279-9
  • Taylor H.F.W: Cement Chemistry. 2nd Ed., Thomas Telford, London, 1997.
  • Quincot G., Azenha M., Barros J., Faria R.: State of the art – Methods to measure moisture in concrete. FCT, Guimaraes, 2011.
  • Witakowski P.: Remote monitoring of changes of structure inner humidity (in Polish). Czasopismo Techniczne 3-Ś/105 (2008), 161-182.
Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-53741f16-f401-4e66-8900-10c9cb39bc58
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