Towards cubic modification of Li7La3Zr2O12 compound by mechanical milling and annealing of powders

• Autorzy: Oleszak D. , Kurowski B. , Pikula T. , Pawlyta M. , Senna M. , Suzuki H.

Identyfikatory

DOI

10.24425/amm.2019.126211

• Języki publikacji: EN

Abstrakty

EN

The aim of these studies was to obtain single phase cubic modification of Li₇La₃Zr₂O₁₂ by mechanical milling and annealing of La(OH)₃, Li₂CO₃ and ZrO₂ powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li₇La₃Zr₂O₁₂ in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

Słowa kluczowe

EN

lithium-ion batteries; solid state electrolyte; mechanical milling; XRD; DSC/TG

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2019
• Tom: Vol. 64, iss. 1
• Strony: 13--16
• Opis fizyczny: Bibliogr. 9 poz., fot., rys.

Twórcy

autor

Oleszak D.

• Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., 02-507 Warsaw, Poland

autor

Kurowski B.

• Warsaw University of Technology, Faculty of Materials Science and Engineering, 141 Woloska Str., 02-507 Warsaw, Poland

autor

Pikula T.

• Lublin University of Technology, Faculty of Electronics and Information Technology, 38a Nadbystrzycka Str., 20-618 Lublin, Poland

autor

Pawlyta M.

• Silesian University of Technology, Institute of Engineering Materials and Biomaterials, 18a Konarskiego Str., 44-100 Gliwice, Poland

autor

Senna M.

• Keio University, Faculty of Science and Technology, Yokohama, Japan

autor

Suzuki H.

• Shizuoka University, Research Institute of Electronics, Hamamatsu, Japan

Bibliografia

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• [4] H. M. Rietveld, J. Appl. Cryst. 2, 65-71 (1969).
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• [6] G. Hongxia, Ch. Kai, Y. Di, M. Ao, H. Mian, L. Yuanhua, N. Cewen, Rare Metal Materials and Engineering 45 (3), 612-616 (2016).
• [7] E. Yi, W. Wang, J. Kieffer, R. M. Laine, Journal of Power Sources 352, 156-164 (2017).
• [8] X. P. Wang, Y. Xia, J. Hu, Y. P. Xia, Z. Zhuang, L. J. Guo, H. Lu, T. Zhang, Q. F. Fang, Solid State Ionics 253, 137-142 (2013).
• [9] I. Quinzeni, D. Capsoni, V. Berbenni, P. O. Mustarelli, M. Sturini, M. Bini, Materials Chemistry and Physics 185, 55-64 (2017).

Uwagi

EN

1. Financial support from the National Centre for Research and Development in the framework of V4-Japan joint research project “AdOX” under the contract no V4-Jap/4/2016 is highly appreciated.

PL

2. Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).