Development of magnetic solid-phase extraction coupled with dispersive liquid–liquid microextraction method for the simultaneous determination of biphenyl and biphenyl oxide in water Samales

• Autorzy: Noori Arezoo Hassan , Rezaee Mohammad , Kazemipour Maryam , Mashayekhi Hossein Ali

Identyfikatory

DOI

10.1556/1326.2018.00134

• Języki publikacji: EN

Abstrakty

EN

A new and sensitive method, termed magnetic solid phase extraction combined with dispersive liquid–liquid microextracton (MSPE–DLLME), has been developed for the simultaneous determination of biphenyl and biphenyl oxide in water samples. Different parameters influencing the extraction efficiency, including the amount of sorbent, sorption time, type of elution solvent and its volume, type of extraction solvent and its volume, and elution time were optimized. The calibration curves were linear in the range of 0.5–100 μg/L for both of them. The limits of detection (LODs) were achieved, 0.03 μg/L for biphenyl and 0.07 μg/L for biphenyl oxide, respectively. Ultimately, the applicability of the method was successfully confirmed by the extraction and determination of biphenyl and biphenyl oxide in sea, river, tap, and water well.

Słowa kluczowe

EN

Magnetic solid-phase extraction; dispersive liquid-liquid microextraction; biphenyl; biphenyl oxide; gas chromatography

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2019
• Tom: Vol. 31, no. 1
• Strony: 1--7
• Opis fizyczny: Bibliogr. 37 poz., rys., tab.

Twórcy

autor

Noori Arezoo Hassan

• Department of Chemistry, Kerman Branch, Islamic Azad University, Kerman, Iran

autor

Rezaee Mohammad

• Materials and Nuclear Fuel Research School, Nuclear Science & Technology Research Institute, Atomic Energy Organization of Iran, P.O. Box 14395-836, Tehran, Iran

autor

Kazemipour Maryam

• Department of Chemistry, Kerman Branch, Islamic Azad University, Kerman, Iran

autor

Mashayekhi Hossein Ali

• Department of Chemistry, Tonekabon Branch, Islamic Azad University, Tonekabon, Iran

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).