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In the present work, we performed the ultra-rapid annealing (URA) process for amorphous Fe78Ni8B14 melt-spun ribbons in order to obtain fine excellent microstructure assuring the best soft magnetic properties. Several microscopic methods mainly based on transmission electron microscopy (TEM) and Lorentz TEM (L-TEM) were applied for detailed studies of the microstructure and magnetic domains structure. The investigation revealed that the optimized parameters of the URA process (500°C/0.5-5 s) lead to outstanding soft magnetic properties. A mixture containing close to 50% amorphous phase and 50% α-Fe nanocrystals of size up to 30 nm has been already obtained after annealing for 3 s. These annealing conditions appear to be the most suitable in terms of microstructure providing the best magnetic properties.
Wydawca
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Strony
1165--1170
Opis fizyczny
Bibliogr. 19 poz., fot., rys., tab.
Twórcy
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Kraków, Poland
autor
- Lukasiewicz Research Network - Institute of Non-Ferrous Metals, 5 Generała Józefa Sowińskiego str., 44-121 Gliwice, Poland
autor
- Warsaw University of Technology, the Faculty of Materials Science and Engineering, 141 Wołoska Str., 02-507 Warszawa, Poland
autor
- Warsaw University of Technology, the Faculty of Materials Science and Engineering, 141 Wołoska Str., 02-507 Warszawa, Poland
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Kraków, Poland
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Kraków, Poland
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Kraków, Poland
autor
- Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Kraków, Poland
Bibliografia
- [1] Y. Yoshizawa, S. Oguma, K. Yamauchi, J. Appl. Phys. 64, 6044 (1988).
- [2] A. Makino, T. Hatanai, A. Inoue, T. Masumoto, Mater. Sci. Eng. A 226-228, 594 (1997).
- [3] K. Suzuki, A. Makino, A. Inoue, T. Masumoto, J. Appl. Phys. 74, 3316 (1993).
- [4] A. Hsiao, M.E. McHenry, D.E. Laughlin, M.J. Kramer, C. Ashe, T. Ohkubo, IEEE Trans. Magn. 38, 3039 (2002).
- [5] L. Hawelek, T. Warski, A. Radon, A. Pilsniak, W. Maziarz, M. Szlezynger, M. Kadziolka-Gawel, A. Kolano-Burian, Materials 14, 7807 (2021).
- [6] A. Wojcik, W. Maziarz, M. Kowalczyk, R. Chulist, M. Szlezynger, P. Czaja, L. Hawelek, P. Zackiewicz, P. Wlodarczyk, A. Kolano-Burian, Materials 13, 1639 (2020).
- [7] M.A. Willard, M.-Q. Haung, D.E. Laughlin, M.E. McHenry, J.O. Cross, V.G. Harris, C. Franchetti, J. Appl. Phys. 85, 4421 (1999).
- [8] A. Kolano-Burian, P. Zackiewicz, A. Grabias, A. Wojcik, W. Maziarz, M. Szlezynger, P. Wlodarczyk, M. Kowalczyk, L. Hawelek, Materials 14, 3433 (2021).
- [9] L. Hawelek, T. Warski, P. Wlodarczyk, M. Polak, P. Zackiewicz, W. Maziarz, A. Wojcik, M. Steczkowska-Kempka, A. Kolano-Burian, Materials 14, (2021).
- [10] N. Aronhime, E. Zoghlin, V. Keylin, X. Jin, P. Ohodnicki, M.E. McHenry, Scr. Mater. 142, 133-137 (2018).
- [11] N. Aronhime, V. DeGeorge, V. Keylin, P. Ohodnicki, M.E. McHenry, JOM 69, 2164-2170 (2017).
- [12] T. Warski, A. Radon, P. Zackiewicz, P. Wlodarczyk, M. Polak, A. Wojcik, W. Maziarz, A. Kolano-Burian, L. Hawelek, Materials 14, 726 (2021).
- [13] G. Herzer, Modern soft magnets: Amorphous and nanocrystalline materials, Acta Materialia 61, 718-734 (2013).
- [14] P. Sharma, X. Zhang, Y. Zhang, A. Makino, Scr. Mater. 95, 3-6 (2015).
- [15] K. Saito, H.S. Park, D. Shindo, Y. Yoshizawa, Journal of Magnetism and Magnetic Materials 305, 304-309 (2006).
- [16] M. Hiraoka, Z. Akase, D. Shindo, Y. Ogawa, Y. Yoshizawa, Materials Transactions 50, 12, 2839-2843 (2009).
- [17] A. Kolano-Burian, M. Kowalczyk, A. Grabias, A. Radoń, P. Błyskun, T. Warski, M. Karpiński, L. Hawelek, T. Kulik, Journal of Alloys and Compounds 921, 165943 (2022).
- [18] T. Kulik, H.T. Sevage, A.J. Hernando, Appl. Phys. 73, 6855-6857 (1993).
- [19] K. Sato, K. Takenaka, A. Makino, Y. Hirotsu, AIP Adv. 5, 067166 (2015).
Uwagi
This research was founded by National Centre for Research and Development (POLAND) within the frame of project no TECHMATSTRATEG 2/410941/4/nCBR/2019.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-5210b0f6-6e51-46d6-b7b0-cd1942d49561