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Występowanie i oznaczanie wybranych grup mikrozanieczyszczeń regulowanych dyrektywą 2000/60/WE w środowisku wodnym

Autorzy
Treść / Zawartość
Identyfikatory
Warianty tytułu
EN
Occurrence and determination of selected micropollutants in water environment regulated by directive 2000/60/WE
Języki publikacji
PL
Abstrakty
PL
Przeprowadzono studium literaturowe określające stan wiedzy w zakresie występowania oraz metod oznaczania wybranych grup mikrozanieczyszczeń, znacząco różniących się od siebie regulowanych dyrektywą 2000/60/ WE w środowisku wodnym. Do opracowania wybrano: 4-tert-oktylofenol, ftalan bis(2-etyloheksylu), heptachlor, epoksyd heptachloru i antracen. Opisano metody ekstrakcji, rozdziału chromatograficznego oraz detekcji poszczególnych związków. Procedury oznaczenia porównano pod kątem czułości analitycznej stosując jako parametry charakteryzujące instrumentalną granicę detekcji i oznaczalności. Dla każdego związku wybrano metodę oznaczania o największej czułości. Ponadto zestawiono wartości stężeń omawianych mikrozanieczyszczeń w wodnych próbkach środowiskowych oraz wskazano możliwe źródła ich pochodzenia.
EN
Residents of even small cities are struggling with air pollution. Municipalities and cities undertake various activities and allocate significant resources to counteract the problem related to air and soil pollution, which is growing continuously. The specialists in the field of ecology have stated that an ideal solution would be to increase the amount of plants in the neighbourhood of residents. Such actions have been undertaken for many years, but clear positive effects have not been observed yet. In these urban areas, the declining conditions of mature plants can be observed, and the longevity of newly planted trees is becoming shorter due to the poor growth conditions. In order to improve the current situation, it has become necessary to develop package/s of solutions allowing for new plantings in cities and rural areas, as well as supporting plants which already exist. The latest scientific trends have showed that one of the most important and promising elements of these solutions could be the use of a structural substrates (a rock and soil mixture prepared according to a special recipe) that can be used as an alternative growth medium for trees instead of the standard up-to-date used soils. In our research, the experimental plot was designed using this type of substrate. The carried out capacity tests showed that the structural substrate has a definite advantage over the substrates presently used in urban areas. The use of structural substrates also enhanced the physiological conditions of the tested trees. Our results allowed us to confirm that structural substrates can be successfully used in the urban and rural areas, which would significantly improve the environmental conditions.
Rocznik
Strony
38--47
Opis fizyczny
Bibliogr. 32 poz., tab.
Twórcy
autor
  • Przedsiębiorstwo Usług Technicznych DEMPOL-ECO, ul. Składowa 9, 45-125 Opole
  • Politechnika Śląska w Gliwicach, Instytut Inżynierii Wody i Ścieków, ul. Konarskiego 18, 44-100 Gliwice
autor
  • Politechnika Śląska w Gliwicach, Instytut Inżynierii Wody i Ścieków, ul. Konarskiego 18, 44-100 Gliwice
Bibliografia
  • 1. Baram G.I., Azarova I.N., Gorshkov A.G., Vereshchagin A.L., Lang B., Kiryukhina E.D. 2000. Determination of bis (2-ethylhexyl) phthalate in water by high-performance liquid chromatography with direct on-column preconcentration. Journal of Analytical Chemistry, 55, 750-754.
  • 2. Basheer C., Lee H.K., Obbard J.P. 2002. Determination of organochlorine pesticides in seawater using liquid-phase hollow fibre membrane microextraction and gas chromatography-mass spectrometry.Journal of Chromatography A, 968, 191-199.
  • 3. Bina B., Mohammadi F., Amin M.M., Pourzamani H.R., Yavari Z. 2017. Determination of 4-nonylphenol and 4-tert-octylphenol compounds in various types of wastewater and their removal rates in different treatment processes in nine wastewater treatment plants of Iran. Chinese Journal of Chemical Engineering, in press.
  • 4. Cai Y., Jiang G., Liu J., Zhou Q. 2003. Multiwalled carbon nanotubes as a solid-phase extraction adsorbent for the determination of bisphenol A, 4-n-nonylphenol, and 4-tert-octylphenol. Analytical Chemistry, 75 2517-2521.
  • 5. Cao X.-L. 2008. Determination of phthalates and adipate in bottled water by headspace solid-phase microextraction and gas chromatography/mass spectrometry. Journal of Chromatography A, 1178, 231-238.
  • 6. Cháfer-Pericás C., Campíns-Falcó P., Prieto-Blanco M.C. 2008. Automatic in-tube SPME and fast liquid chromatography: A cost-effective method for the estimation of dibuthyl and di-2-ethylhexyl phthalates in environmental water samples. Analytica Chimica Acta, 610, 268-273.
  • 7. Cortada C., Vidal L., Pastor R., Santiago N., Canals A. 2009a. Determination of organochlorine pesticides in water samples by dispersive liquid-liquid microextraction coupled to gas chromatography-mass spectrometry. Analytica Chimica Acta, 649, 218-221.
  • 8. Cortada C., Vidal L., Tejada S., Romo A., Canals A. 2009b. Determination of organochlorine pesticides in complex matrices by single-drop microextraction coupled to gas chromatography-mass spectrometry. Analytica Chimica Acta, 638, 29-35.
  • 9. Dat N.-D., Chang M.B. 2017. Review on characteristics of PAHs in atmosphere, anthropogenic sources and control technologies. Science of the Total Environment, 609, 682-693.
  • 10. Deng L., Wu F., Deng N., Yang Y. 2005. Determination of trace DEHP in aqueous solution by solid phase microextraction coupled with high performance liquid chromatography. Fresenius Environmental Bulletin, 14, 494-497.
  • 11. Dyrektywa, 2000. Dyrektywa Parlamentu Europejskiego i Rady z dnia 23 października 2000 r., nr 2000/60/WE.
  • 12. Jara S., Lysebo C., Greibrokk T., Lundanes E. 2000. Determination of phthalates in water samples using polystyrene solid-phase extraction and liquid chromatography quantification. Analytica Chimica Acta, 407, 165-171.
  • 13. Kayali N., Tamayo F.G., Polo-Díez L.M. 2006. Determination of diethylhexyl phtalate in water by solid phase microextraction coupled to high performance liquid chromatography. Talanta, 69, 1095-1099.
  • 14. King A.J., Readman J.W., Zhou J.L. 2004. Determination of polycyclic aromatic hydrocarbons in water by solid-phase microextraction-gas chromatography-mass spectrometry. Analytica Chimica Acta, 523, 259-267.
  • 15. Kuch H.M., Ballschmiter K. 2001. Determination of endocrine-disrupting phenolic compounds and estrogens in surface and drinking water by HRGC- (NCI)-MS in the picogram per liter range. Environmental Science and Technology, 35, 3201-3206.
  • 16. Leivadara S.V., Nikolaou A.D., Lekkas T.D. 2008. Determination of organic compounds in bottled waters. Food Chemistry, 108, 277-286.
  • 17. Li Y., Yoshida S., Chondo Y., Nassar H., Tang N., Araki Y., Toriba A., Kameda T., Hayakawa K. 2012. On-line concentration and fluorescence determination HPLC for polycyclic aromatic hydrocarbons in seawater samples and its application to Japan Sea. Chemical and Pharmaceutical Bulletin, 60, 531-535.
  • 18. Lien G.-W., Chen C.-Y., Wang G.-S. 2009. Comparison of electrospray ionization, atmospheric pressure chemical ionization and atmospheric pressure photoionization for determining estrogenic chemicals in water by liquid chromatography tandem mass spectrometry with chemical derivatizations. Journal of Chromatography A, 1216, 956-966.
  • 19. Liu R., Zhou J.L., Wilding A. 2004. Simultaneous determination of endocrine disrupting phenolic compounds and steroids in water by solid-phase extraction-gas chromatography-mass spectrometry. Journal of Chromatography A, 1022, 179-189.
  • 20. McManus S.-L., Coxon C.E., Richards K.G., Danaher M. 2013. Quantitative solid phase microextraction - gas chromatography mass spectrometry analysis of the pesticides lindane, heptachlor and two heptachlor transformation products in groundwater. Journal of Chromatography A, 1284, 1-7.
  • 21. Meng J., Bu J., Deng C., Zhang X. 2011. Preparation of polypyrrole-coated magnetic particles for micro solid-phase extraction of phthalates in water by gas chromatography-mass spectrometry analysis. Journal of Chromatography A, 1218, 1585-1591.
  • 22. Okumura T., Nishikawa Y., Yamamoto H., Konishi H. 1997. Gas chromatography-mass spectrometric determination of fthalide and heptachlor epoxide in environmental samples. Talanta, 44, 649-656.
  • 23. Polo M., Llompart M., Garcia-Jares C., Cela R. 2005. Multivariate optimization of a solid-phase microextraction method for the analysis of phthalate esters in environmental waters. Journal of Chromatography A, 1072, 63-72.
  • 24. Prapatpong P., Kanchanamayoon W. 2010. Determination of phthalate esters in drinking water using solid-phase extraction and gas chromatography. Journal of Applied Sciences, 10, 1987-1990.
  • 25. Ramirez C.E., Wang C., Gardinali P.R. 2014. Fully automated trace level determination of parent and alkylated PAHs in environmental waters by online SPE-LC-APPI-MS/MS. Analytical and Bioanalytical Chemistry, 406, 329-344.
  • 26. Rianawati E., Balasubramanian R. 2009. Optimization and validation of solid phase micro-extraction (SPME) method for analysis of polycyclic aromatic hydrocarbons in rainwater and stormwater. Physics and Chemistry of the Earth, 34, 857-865.
  • 27. Salgueiro-González N., Turnes-Carou I., Besada V., Muniategui-Lorenzo S., López-Mahía P., Prada-Rodríguez D. 2015. Occurrence, distribution and bioaccumulation of endocrine disrupting compounds in water, sediment and biota samples from a European river basin. Science of the Total Environment, 529, 121-130.
  • 28. Smuda K., Dudziak, M. 2016. Changes of the EU and Polish legislation concerning pollution of the aquatic environment in 2010-2016. Architecture Civil Engineering Environment, 9, 141-146.
  • 29. Titato G.M., Lanças F.M. 2006. Optimization and validation of HPLC-UV-DAD and HPLC-APCI-MS methodologies for the determination of selected PAHs in water samples. Journal of Chromatographic Science, 44, 35-40.
  • 30. Wang L., Jiang G.-B., Cai Y.-Q., He B., Wang Y.-W., Shen D.-Z. 2007. Cloud point extraction coupled with HPLC-UV for the determination of phthalate esters in environmental water samples. Journal of Environmental Sciences, 19, 874-878.
  • 31. Yazdanfar N., Yamini Y., Ghambarian M. 2014. Homogeneous liquid-liquid microextraction for determination of organochlorine pesticides in water and fruit samples. Chromatographia, 77, 329-336.
  • 32. Zhang Y., Lee H.K. 2012. Application of ultrasound-assisted emulsification microextraction based on applying low-density organic solvent for the determination of organochlorine pesticides in water samples. Journal of Chromatography A, 1252, 67-73.
Uwagi
PL
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-50389b10-406d-451a-aa0b-ec485cd92e01
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