Preparative separation of flavanones and terpenoids from olibanum by high-speed counter-current chromatography

• Autorzy: Zhao H. W. , Geng Y. L , Zhu H. , Yang P. , Yu J. Q.

Identyfikatory

DOI

10.1556/1326.2017.00323

• Języki publikacji: EN

Abstrakty

EN

Seven compounds, including two flavanones, dihydrokaempferol (1) and naringenin (2), and five terpenoids, boscartol A (3), 3,7-dioxo-tirucalla-8,24-dien-21-oic acid (4), 3α-acetoxyl-7-oxo-tirucalla-8,24-dien-21-oic acid (5), 11-keto-β-boswellic acid (6), and acetyl-11-keto-boswellic acid (7), have been purified by high-speed counter-current chromatography (HSCCC) from olibanum. For the separation, from 250 mg of the crude extract, 3.1 mg of 1 (95.2% purity), 2.7 mg of 2 (96.1% purity), 9.1 mg of 3 (96.7% purity), 4.5 mg of 4 (95.3% purity), 5.4 mg of 5 (96.3% purity), 48.1 mg of 6 (96.8% purity), and 45.5 mg of 7 (98.1% purity) were obtained by HSCCC with petroleum ether–ethyl acetate–methanol–water (1:0.8:1.1:0.6, v/v). The structures of these seven compounds were elucidated by a combination of electrospray ionization mass spectrometry (ESI–MS) and extensive nuclear magnetic resonance (NMR) spectroscopic.

Słowa kluczowe

EN

Olibanum; flavanone; terpenoids; separation; high-speed counter-current chromatography

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2019
• Tom: Vol. 31, no. 1
• Strony: 28--32
• Opis fizyczny: Bibliogr. 18 poz., rys.

Twórcy

autor

Zhao H. W.

• Shandong Key Laboratory of TCM Quality Control Technology, Shandong Analysis and Test Center, Jinan, 250014, P. R. China
• Current Affiliation: College of Pharmacy, Shandong University of Traditional Chinese Medicine, Jinan, 250014, P. R. China

autor

Geng Y. L

• Shandong Key Laboratory of TCM Quality Control Technology, Shandong Analysis and Test Center, Jinan, 250014, P. R. China

autor

Zhu H.

• Shandong Key Laboratory of TCM Quality Control Technology, Shandong Analysis and Test Center, Jinan, 250014, P. R. China

autor

Yang P.

• Senkang Sanfeng Biological Engineering Technology Co. Ltd., Jinan, 250014, P. R. China

autor

Yu J. Q.

• Shandong Key Laboratory of TCM Quality Control Technology, Shandong Analysis and Test Center, Jinan, 250014, P. R. China

Bibliografia

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).