Synthesis and characterization of binary and ternary nanocomposites based on TiO2, SiO2 and ZnO with PVA based template-free gel combustion method

Fakoori, Elham; Karami, Hassan; Nezhadali, Azizollah

doi:10.2478/msp-2019-0051

Artykuł - szczegóły

Tytuł artykułu

Synthesis and characterization of binary and ternary nanocomposites based on TiO2, SiO2 and ZnO with PVA based template-free gel combustion method

Autorzy

Fakoori Elham , Karami Hassan , Nezhadali Azizollah

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.2478/msp-2019-0051

Warianty tytułu

Języki publikacji

Abstrakty

Binary and ternary nanocomposites based on TiO₂, SiO₂ and ZnO were synthesized by PVA-based template-free gel combustion method. The morphology and the particles sizes of the synthesized samples depended on some parameters including the initial concentrations of metal salts and PVA amount in the sol, solvent composition and solution pH. Effects of these parameters were investigated and optimized by using the Taguchi method. In the experimental design, the Taguchi L₂₅ array was used to investigate six factors at five levels. The samples were characterized by dynamic light scattering (DLS), transmission electron microscopy (TEM), Brunauer-Emmett-Teller (BET) specific surface areas, scanning electron microscopy (SEM). The obtained results showed that the present method can be used to synthesize TiO₂/SiO₂/ZnO ternary nanocomposite with an effective surface area of 0.3 m² · g⁻¹ and ZnO/TiO₂, TiO₂/SiO₂, ZnO/SiO₂ binary nanocomposites with an effective surface area of 234 m² · g^-1, 6 m² · g^-1 and 0.5 m² · g^-1, respectively. The ZnO/TiO₂ nanocomposite which was synthesized under the following experimental conditions: 2.5 wt.% Zn salt, 2.5 wt.% Ti salt, 2.0 wt.% PVA, pH = 1 and ethanol:water ratio 30:70 was selected by the Taguchi method as an optimum sample with the smallest particles (average diameter = 50 nm).

Słowa kluczowe

titanium oxide sulphur dioxide zinc oxide TiO2 SiO2 ZnO nanocomposite sol-gel method pyrolysis experimental design Taguchi method

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2019

Tom

Vol. 37, No. 3

Strony

426--436

Opis fizyczny

Bibliogr. 45 poz., tab., rys.

Twórcy

autor

Fakoori Elham

Department of Chemistry, Payamr Noor University, P. O. Box 19395-3697, Tehran, Iran

autor

Karami Hassan

karami_h@yahoo.com

Department of Chemistry, Payamr Noor University, P. O. Box 19395-3697, Tehran, Iran
Nano Research Laboratory, Department of Chemistry, Payame Noor University, Abhar, Iran

autor

Nezhadali Azizollah

Department of Chemistry, Payamr Noor University, P. O. Box 19395-3697, Tehran, Iran

Bibliografia

[1] WANG L., MUHAMMED M., J. Mater. Chem., 9 (1999), 2871.
[2] MEULENKAMP E.A., J. Phys. Chem. B, 102 (1998), 5566.
[3] SONG Z., LI Q., GAO L., J. Mater. Sci. Technol., 13 (1997), 321.
[4] ZHUANG J., LIU M., LIU H., Sci. China B, 52 (2009), 2125.
[5] USUI H., Mater. Lett., 63 (2009), 1489.
[6] LI F., HUANG X., JIANG Y., LIU L., LI Z., Mater. Res. Bull., 44 (2009), 437.
[7] KIM S., FISHER B., EISLER H.J., BAWENDI M., J. Am. Chem. Soc., 125 (2003), 11466.
[8] TAK Y., HONG S.J., LEE J.S., YONG K., J. Mater. Chem., 19 (2009), 5945.
[9] KIM C., CHOI M., JANG J., Catal. Commun., 11 (2010), 378.
[10] RAHMAN I.A., PADVETTAN V., J. Nanomater., (2012), 1. DOI: 10.1155/2012/132424.
[11] HOFFMANN M.R., MARTIN S.T., CHOI W., BAHNEMANN D.W., Chem. Rev., 95 (1995), 69.
[12] WANG C., AO Y., WANG P., HOU J., QIAN J., ZHANG S., J. Hazard. Mater., 178 (2010), 517.
[13] WANG C., AO Y., WANG P., HOU J., QIAN J., Mater. Lett., 64 (2010), 1003.
[14] ARAI Y., TANAKA K., KHLAIFAT A.L., J. Mol. Catal. A: Chem., 243 (2006), 85.
[15] BISWAS S., HOSSAIN M.F., TAKAHASHI T., KUBOTA Y., FUJISHIMA A., Thin Solid Films, 516 (2008), 7313.
[16] HOUŠKOVÁ V., ŠTENGL V., BAKARDJIEVA S., MURAFA N., J. Phys. Chem. Solids, 69 (2008), 1623.
[17] LEE H.C., HWANG W.S., Appl. Surf. Sci., 253 (2006), 1889.
[18] SERPONE N., MARUTHAMUTHU P., PICHAT P., PELIZZETTI E., HIDAKA H., J. Photochem. Photobiol. A: Chem., 85 (1995), 247.
[19] LIAO D.L., BADOUR C.A., LIAO B.Q., J. Photochem. Photobiol. A: Chem., 194 (2008) 11.
[20] WANG J., JIANG Z., ZHANG L., KANG P., XIE Y., LV Y., ZHANG X., Ultrason. Sonochem., 16 (2009), 225.
[21] XU X., WANG J., TIAN J., WANG X., DAI J., LIU X., Ceram. Int., 37 (2011), 2201.
[22] JANITABAR-DARZI S., MAHJOUB A.R., J. Alloy. Compd., 486 (2009), 805.
[23] GIESCHE H., J. Eur. Ceram. Soc., 14 (1994), 205.
[24] VENKATATHRI N., Bull. Mater. Sci., 30 (2007) 615.
[25] STÖBER W., FINK A., BOHN E., J. Colloid Interface Sci., 26 (1968), 62.
[26] LINDBERG R., SJÖBLOM J., SUNDHOLM G., Colloids Surf. A, 99 (1995), 79.
[27] CHAN Y., ZIMMER J.P., STROH M., STECKEL J.S., JAIN R.K., BAWENDI M.G., Adv. Mater., 16 (2004), 2092.
[28] EPIFANI M., GIANNINI C., TAPFER L., VASANELLI L., J. Am. Ceram. Soc., 83 (2000), 2385.
[29] GONELLA F., MATTEI G., MAZZOLDI P., SADA C., BATTAGLI N.G., CATTARUZZA E., Appl. Phys. Lett., 75 (1999) 55.
[30] LIZ-MARZÁN L.M., GIERSIG M., MULVANEY P., Langmuir, 12 (1996), 4329.
[31] HE J., ICHINOSE I., KUNITAKE T., NAKAO A., Langmuir, 18 (2002), 10005.
[32] SONG J.H, ATAY T., SHI S., URABE H., V. NURMIKKO A., Nano Lett., 15 (2005), 1557.
[33] SHTER G.E., BEHAR-LEVY H., GELMAN V., GRADER G.S., AVNIR D., Adv. Funct. Mater., 17 (2007), 913.
[34] TRAVERSA E., DI VONA M.L., LICOCCIA S., SACERDOTI M., CAROTTA M.C., CREMA L., MARTINELLI G., J. Sol-Gel Sci. Technol., 22 (2001), 167.
[35] KARAMI H., AMIFAR A., TAVALLALI H., NAMDAE Z.A., J. Clust. Sci., 21 (2011), 1.
[36] SAYILKAN F., ASILTURK M., SENER S., ERDEMOGLU S., ERDEMOGLU M., SAYILKAN H., Turk. J. Chem., 31 (2007), 211.
[37] CALLEJA G., SERRANO D.P., SANZ R., PIZARRO P., Microporous Mesoporous Mater., 111 (2008), 429.
[38] GARZELLA C., COMINI E., BONTEMPIL E., DEPEROL L.E., FRIGERI C., SBERVEGLIERI G., Mater. Res. Soc. Symp. Proc., 638 (2001), 111.
[39] WANG Z., HELMERSSON U., KALL P., Thin Solid Films, 405 (2002), 50.
[40] IVANOVA T., HARIZANOVA A., SURTCHEV M., Mater. Lett., 55 (2002), 327.
[41] DOHSHI S., TAKEUCHI M., ANPO M., Catal. Today, 85 (2003), 75.
[42] GONÇALVES R.R., MESSADDEQ Y., ATIK M., RIBEIRO S.J., Mater. Res., 2 (1999), 11.
[43] NISHIDE T., SATO M., HARA H., J. Mater. Sci., 35 (2000), 465.
[44] CABBRERA S., EL HASKOURI J., BELTRA’N-PORTER A., BELTRA’N-PORTER D., MARCOS M.D., AMORO’S P., J. Solid State Sci., 2 (2000) 513.
[45] ROSTAMKHANI F., KARAMI H., GHASEMI A., Desalin. Water Treat., 60 (2017), 319.

Uwagi

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-4c2f5465-5d45-4d85-a146-3de48572a7f4