Analityka spektrochemiczna - emisyjna spektrometria atomów i cząsteczek dwuatomowych wybranych plazm bezelektrodowych

• Autorzy: Borkowska-Burnecka J.

Warianty tytułu

EN

Spectrochemical analytics - emission spectrometry of atoms and diatomic molecules of selected electrodeless plasmas

• Języki publikacji: PL

Abstrakty

PL

Omówiono zastosowanie spektrometrii emisyjnej plazm bezelektrodowych w analizie składu pierwiastkowego różnorodnych materiałów, w analizie oscylacyjno-rotacyjnej cząsteczek oraz do wyznaczania parametrów fizykochemicznych plazmy. W pierwiastkowej analizie spektrochemicznej wykorzystano plazmę indukcyjnie sprzężoną (ICP). Badania obejmowały testowanie różnych metod wprowadzania próbek do plazmy, analizę efektów matrycowych i interferencji spektralnych w powiązaniu z diagnostyką spektroskopową wyładowania oraz opracowanie nowych, przyjaznych środowisku metod przygotowania próbek do analiz wielopierwiastkowych. Określono efektywność różnych procedur mineralizacji próbek oraz zaproponowano alternatywne nowe procedury przeprowadzenia analitu do roztworu oparte na ekstrakcji wspomaganej energią mikrofalową lub ultradźwiękową. Przedstawiono możliwość izolowania analitów od matrycy, wzbogacania analitów, obniżenia granic wykrywalności, redukcji efektów matrycowych oraz uproszczenia procedury kalibracyjnej dzięki wykorzystaniu ekstrakcji w punkcie zmętnienia. Określono wpływ różnych matryc na parametry charakteryzujące plazmę, takie jak temperatura, gęstość elektronowa, stopień jonizacji oraz zależność efektów matrycowych od parametrów fizycznych stosowanych linii analitycznych. Przedstawiono wykorzystanie bezelektrodowej plazmy chemiluminescencyjnej w badaniach struktury widm cząsteczek dwuatomowych i wyznaczaniu ich podstawowych stałych molekularnych oraz rolę i zastosowanie w analizie pierwiastkowej i diagnostyce plazmy. Stosując głównie metodę wysokorozdzielczej spektrometrii fourierowskiej, analizowano widma GeBr, PbH, PbD, Pb2 i PbLi wzbudzone w niskociśnieniowym wyładowaniu mikrofalowym oraz w reakcji chemiluminescencji połączonej z wyładowaniem mikrofalowym. Wyznaczono po raz pierwszy stałe molekularne wzbudzonych stanów elektronowych tych cząsteczek. Zaproponowano wykorzystanie widm ciężkich molekuł, takich jak Bi2 i BiN do określenia równowagi termodynamicznej w układach emitujących promieniowanie.

EN

The study demonstrates application of emission spectrometry of electrodeless plasma in analysis of elemental composition of various materials and in vibrational-rotational analysis of diatomic molecules as well as in determination of physical plasma parameters. Inductively coupled argon plasma was utilized for elemental spectrochemical analysis. Various methods of introduction of samples into the plasma, matrix effects and spectral interferences were studied in relation with physical parameters of the analytical lines and plasma characteristics. New, environmen- tal friendly methods of sample preparation for multi-elemental spectrochemical analysis have been devel- oped and verified. Various sample digestion methods were compared in terms of their effectiveness and altemative pro- cedures based on microwave or ultrasound assisted extraction have been proposed and validated. Possibil- ities of analyte isolation from complex matrix and its enrichment as well as lowering of detection limits and simplification of the calibration step were achieved by the cloud point extraction. Effects of various matrices on linę intensities and plasma parameters such as electron number density, excitation and ioniza- tion temperatures have been presented and discussed. lnvestigation of structure and determination of spectroscopic constants of diatomic molecules as well as their role and application in elemental analysis and plasma diagnostics were presented. Spectra of GeBr, PbH, PbD, Pb2 and PbLi were excited in plasma generated by microwave or chemiluminescence combined with microwave discharges. The analyses were mainly performed by the high resolution Fourier transform spectrometry. Rotational and vibrational analyses of new electronic transitions were carried out and molecular spectroscopic constants of excited electronic States have been determined for the first time. Spectra of heavy molecules such as Bi2 or BiN were proposed for plasma diagnostics and estimation of thermodynamic eąuilibrium in objects emitting radiation.

Słowa kluczowe

PL

spektrometria emisyjna; plazma bezelektrodowa; preparatyka analityczna; interferencje; analiza rotacyjna; analiza oscylacyjna; diagnostyka plazmy

EN

emission spectrometry; plasma electrodeless; spectral interferences; rotational analysis; vibration analysis; plasma diagnostics

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Prace Naukowe Wydziału Chemicznego Politechniki Wrocławskiej. Monografie
• Rocznik: 2012
• Tom: Nr 9, nr 9
• Strony: 178--178
• Opis fizyczny: Bibliogr. 257 poz., tab., rys.

Twórcy

autor

Borkowska-Burnecka J.

• Zakład Chemii Analitycznej Wydziału Chemicznego Politechniki Wrocławskiej, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław

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