Study of Zeolite Phase Made from Rice Husk Ash and Sidrap Clay

• Autorzy: Armayani M. , Mansur Musdalifa , Asra Reza , Irwan Muh , Ramadhanty Dhian , Subaer Subaer , Abdullah Mohd Mustafa Al Bakri , Aziz Ikmal Hakem A. , Jeż Bartłomiej , Nabiałek Marcin

Identyfikatory

DOI

10.24425/amm.2023.141503

• Języki publikacji: EN

Abstrakty

EN

Zeolite has been successfully synthesized from clay and rice husk ash in the form of powder by using the hydrothermal method with variations in chemical compositions of alkaline solution and the amount of rice husk ash. The clay raw material was obtained from the Sidrap area of South Sulawesi and rice husk ash is obtained from the burning pile of rice husks. Sidrap clay and rice husk ash were activated using an alkaline solution of NaOH and varied rice husk ash and the addition of AlCl₃. The addition of AlCl₃, an alkaline solution of NaOH and H₂O was used in the amount of 25.5 grams and variations of rice husk ash were 2.5 grams and 6.5 grams. Meanwhile, without the addition of AlCl₃, an alkaline solution of NaOH and H₂O was used for 20.5 grams and variations of rice husk ash from 2.5 grams and 6.5 grams. Then the mixture was then put into an autoclave with a temperature of 100°C for 3 hours. The basic material used in the manufacture of zeolite is carried out by X-ray Fluorescence (XRF) characterization to determine the constituent elements of basic material, which showed the content of SiO₂ was 45.80 wt% in the clay and 93.40% in the rice husk ash. The crystalline structure of the zeolite formed was characterized by X-Ray Diffraction (XRD). It was found the resulting zeolite were identified as Zeolite-Y, Hydrosodalite, and ZSM-5. The microstructure properties of the resulting zeolite were determined by using Scanning Electron Microscopy (SEM).

Słowa kluczowe

EN

autoclave; clay; rice husk ash; zeolite

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2023
• Tom: Vol. 68, iss. 1
• Strony: 269--274
• Opis fizyczny: Bibliogr. 21 poz., fot., rys., tab.

Twórcy

autor

Armayani M.

• Universitas Muhammadiyah Sidenreng Rappang, Faculty of Sciences and Technology, Jl. Angkatan 45 lt. Salo No. 1A Macarowalie Rappang 91651, Indonesia

• https://orcid.org/0000-0002-1871-2490

autor

Mansur Musdalifa

• Universitas Muhammadiyah Sidenreng Rappang, Faculty of Sciences and Technology, Jl. Angkatan 45 lt. Salo No. 1A Macarowalie Rappang 91651, Indonesia

• https://orcid.org/0000-0002-5202-8625

autor

Asra Reza

• Universitas Muhammadiyah Sidenreng Rappang, Faculty of Sciences and Technology, Jl. Angkatan 45 lt. Salo No. 1A Macarowalie Rappang 91651, Indonesia

• https://orcid.org/0000-0001-6960-0926

autor

Irwan Muh

• Universitas Muhammadiyah Sidenreng Rappang, Faculty of Sciences and Technology, Jl. Angkatan 45 lt. Salo No. 1A Macarowalie Rappang 91651, Indonesia

• https://orcid.org/0000-0001-9420-6939

autor

Ramadhanty Dhian

• Universitas Muhammadiyah Sidenreng Rappang, Faculty of Sciences and Technology, Jl. Angkatan 45 lt. Salo No. 1A Macarowalie Rappang 91651, Indonesia

• https://orcid.org/0000-0002-8358-8086

autor

Subaer Subaer

• Universitas Negeri Makassar, Faculty of Mathematics and Natural Sciences, Jl. Mallengkeri Raya Parang Tambung Kec Tamalate Kota Makassar 90224, Indonesia

• https://orcid.org/0000-0002-0307-5396

autor

Abdullah Mohd Mustafa Al Bakri

• Universiti Malaysia Perlish (UniMAP), Centre of Excellence Geopolymer and Green Technology (CEGeoGTech), Perlis, Malaysia

• https://orcid.org/0000-0002-9779-8586

autor

Aziz Ikmal Hakem A.

• Universiti Malaysia Perlish (UniMAP), Centre of Excellence Geopolymer and Green Technology (CEGeoGTech), Perlis, Malaysia

• https://orcid.org/0000-0002-2152-8918

autor

Jeż Bartłomiej

• Częstochowa University of Technology, Faculty of Production Engineering and Materials Technology, Department of Physics, 19 Armii Krajowej Av., 42-200 Częstochowa, Poland

• https://orcid.org/0000-0002-7918-5946

autor

Nabiałek Marcin

• Częstochowa University of Technology, Faculty of Production Engineering and Materials Technology, Department of Physics, 19 Armii Krajowej Av., 42-200 Częstochowa, Poland

• https://orcid.org/0000-0001-6585-3918

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Uwagi

1. This research has been funded by PDP Kemenristek Dikti No.189 / SP2H/AMD/LT/DRPM/2020.

2. Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023).