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Methodology to develop liquid chromatographic fingerprints for the quality control of herbal medicines

Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
A liquid chromatographic fingerprinting methodology has been established for identification and quality control of traditional herbal medicines. The methodology was developed from four case studies. Samples of Herba Artemisia annua, Herba Artemisia scoparia, Rhizoma Ligusticum chuanxiong (also called Rhizoma chuanxiong ), and Rhizoma Ligusticum jeholense (also called Rhizoma ligustici ) were investigated. In each case study, sample preparation and chromatographic conditions (column, organic modifier, column temperature, detection wavelength, and mechanism) were varied to obtain good fingerprints, i.e. with the maximum number of peaks. Further optimization was then performed either by reducing the analysis time or increasing efficiency. The case studies led to the development of a general methodology consisting of sample preparation and HPLC fingerprint development. The fingerprints obtained with the developed methodology were then successfully used to distinguish between the two Artemisia species and between the two Ligusticum species. The methodology also was used to obtain fingerprints for a large number of different Vietnamese Mallotus species, and for Citri reticulatae pericarpium samples collected in different regions of China.
Rocznik
Strony
237--258
Opis fizyczny
Bibliogr. 30 poz., rys., tab.
Twórcy
autor
  • Vrije Universiteit Brussel - VUB Department of Analytical Chemistry and Pharmaceutical Technology, Pharmaceutical Institute Laarbeeklaan 103 1090 Brussels Belgium
autor
  • Vrije Universiteit Brussel - VUB Department of Analytical Chemistry and Pharmaceutical Technology, Pharmaceutical Institute Laarbeeklaan 103 1090 Brussels Belgium
autor
  • Vrije Universiteit Brussel - VUB Department of Analytical Chemistry and Pharmaceutical Technology, Pharmaceutical Institute Laarbeeklaan 103 1090 Brussels Belgium
Bibliografia
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  • [7] A.M. van Nederkassel, C.J. Xu, P. Lancelin, M. Sarraf, D.A. MacKenzie, N.J. Walton, F. Bensaid, M. Lees, G.J. Martin, J.R. Desmurs, D.L. Massart, J. Smeyers-Verbeke, and Y. Vander Heyden, J. Chromatogr. A, 1120 , 291–298 (2006)
  • [8] N. Nguyen Hoai, B. Dejaegher, C. Tistaert, V. Nguyen Thi Hong, C. Rivière, G. Chataigné, M. Chau Van, J. Quetin-Leclercq, and Y. Vander Heyden, J. Pharm. Biomed. Anal., 50 , 753–763 (2009)
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  • [20] CHMP, Guideline on quality of herbal medicinal products/traditional herbal medicinal products. Committee for medicinal products for human use (CHMP), European Medicines Agency Inspections, July 21, 2005, CPMP/QWP/2819/00 Rev 1, EMEA/CVMP/814/00 Rev 1, http://www.emea.europa.eu/home.htm (accessed February 22, 2010)
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  • [25] A.M. van Nederkassel, V. Vijverman, D.L. Massart, and Y. Vander Heyden, J. Chromatogr. A, 1085 , 230–239 (2005)
  • [26] G. Alaerts, N. Matthijs, J. Smeyers-Verbeke, and Y. Vander Heyden, J. Chromatogr. A, 1172 , 1–8 (2007)
  • [27] Y. Li and K. Bi, Biomed. Chromatogr., 17 , 543–546 (2003)
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Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-3d9efbe9-140c-4f84-911a-3af2eb1e1f1f
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