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Development of manufacturing method of the MAP21 magnesium alloy prepared by selective laser melting (SLM)

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Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Magnesium alloys are well known for their biocompatibility and biodegradable properties [9], [27] owing to the fact that magnesium is a mineral crucial for human body, especially for bone tissue. There are studies [17] on using WE43 additively manufactured magnesium scaffolds for full bone and soft tissue regeneration. Moreover, magnesium implants in bones were investigated as having higher bone-implant interface strength than titanium ones [3]. In this paper, the results of the studies on MAP21 magnesium powder selective laser melting process optimization as a starting point for further bioapplications are presented. MAP21 magnesium alloy owing to its high mechanical properties, excellent vibration damping characteristic and good creep resistance is a promising material to be tested for scaffold structures. The study for the first time shows successful SLM manufacturing of dense samples made of MAP21 alloy. Using an algorithm based on design of experiment (DoE) method [21], the SLM process parameters were designated. The porosity was investigated as a SLM process optimization parameter. High density of produced sample, up to 99%, was achieved. Microstructure and oxidation level after selective laser melting (SLM) manufacturing were characterized. Fine grain microstructure and three kinds of precipitations were found Nd (Gd, Zr, Mg), Mg (Nd, Gd, Zr) and Mg (Zr, Nd, Gd, Zn)). In order to determine the mechanical properties of MAP21 alloy processed with SLM technology, static tensile tests and microhardness tests were conducted, resulting in mechanical properties (Rm = 167 MPa, E = 38.6 GPa, 63–74 HB) comparable with as-cast alloy. A discussion was held on further research opportunities for biomedical use of SLM-ed MAP21 alloy.
Rocznik
Strony
157--168
Opis fizyczny
Bibliogr. 30 poz., rys., tab., wykr.
Twórcy
  • Centre for Advanced Manufacturing Technologies – Fraunhofer Project Center, Wrocław University of Science and Technology, Wrocław, Poland
  • Department of Laser Technologies, Automation and Production management, Mechanical Engineering Faculty, Wrocław University of Science and Technology, Wrocław, Poland
  • Centre for Advanced Manufacturing Technologies – Fraunhofer Project Center, Wrocław University of Science and Technology, Wrocław, Poland
  • Centre for Advanced Manufacturing Technologies – Fraunhofer Project Center, Wrocław University of Science and Technology, Wrocław, Poland
  • Department of Laser Technologies, Automation and Production management, Mechanical Engineering Faculty, Wrocław University of Science and Technology, Wrocław, Poland
  • Centre for Advanced Manufacturing Technologies – Fraunhofer Project Center, Wrocław University of Science and Technology, Wrocław, Poland
  • Department of Laser Technologies, Automation and Production management, Mechanical Engineering Faculty, Wrocław University of Science and Technology, Wrocław, Poland
  • Centre for Advanced Manufacturing Technologies – Fraunhofer Project Center, Wrocław University of Science and Technology, Wrocław, Poland
  • 2 Department of Laser Technologies, Automation and Production management, Mechanical Engineering Faculty, Wrocław University of Science and Technology, Wrocław, Poland
Bibliografia
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  • [3] CASTELLANI C., LINDTNER R.A., HAUSBRANDT P., TSCHEGG E., STANZL-TSCHEGG S.E., ZANONI G., BECK S., WEINBERG A.-M., Bone–implant interface strength and osseointegration: Biodegradable magnesium alloy versus standard titanium control, Acta Biomater., 2011, 7(1), 432–440, DOI: 10.1016/j.actbio.2010.08.020.
  • [4] CHAKRABORTY B.P., AL-SAADI S., CHOUDHARY L., HARANDI S.E., SINGH R., Magnesium Implants: Prospects and Challenges, Materials, 2019, 12(1), 136, DOI: 10.3390/ma12010136.
  • [5] CHEN J., TAN L., YU X., ETIM I.P., IBRAHIM M., YANG K., Mechanical properties of magnesium alloys for medical application: A review, J. Mech. Behav. Biomed. Mater., 2018, 87, 68–79, DOI: 10.1016/j.jmbbm.2018.07.022.
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  • [7] GANGIREDDY S., GWALANI B., LIU K., FAIERSON E.J., MISHRA R.S., Microstructure and mechanical behavior of an additive manufactured (AM) WE43-Mg alloy, Addit. Manuf., 2019, 26, 53–64, DOI: 10.1016/j.addma.2018.12.015.
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  • [9] GU X., ZHENG Y., CHENG Y., ZHONG S., XI T., In vitro corrosion and biocompatibility of binary magnesium alloys, Biomaterials, 2009, 30(4), 484–498, DOI: 10.1016/j.biomaterials.2008.10.021.
  • [10] GULBRANSEN E.A., The oxidation and evaporation of magnesium at temperatures from 400 °C to 500 °C, J. Electrochem. Soc., 1945 (87), 589–599, DOI: 10.1149/1.3071667.
  • [11] HU D., WANG Y., ZHANG D., HAO L., JIANG J., LI Z., CHEN Y., Experimental Investigation on Selective Laser Melting of Bulk Net-Shape Pure Magnesium, Mater. Manuf. Process, 2015, 30(11), 1298–1304, DOI: 10.1080/10426914.2015.1025963.
  • [12] JUNKA A.F., SZYMCZYK P.E., SECEWICZ A., PAWLAK A., SMUTNICKA D., ZIÓŁKOWSKI G.J., BARTOSZEWICZ M., CHLEBUS E., The chemical digestion of Ti6Al7Nb scaffolds produced by Selective Laser Melting reduces significantly ability of Pseudomonas aeruginosa to form biofilm, Acta Bioeng. Biomech., 2016, 012016, ISSN 1509-409X, DOI: 10.5277/ABB-00333-2015-01.
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  • [16] KURZYNOWSKI T., SZYMCZYK P.E., ZIÓŁKOWSKI G.J., DZIEDZIC R., PAWLAK A.P., GRUBER K., Annual report on the implementation of the AMgAvio project for 2017, Magnesium based alloys processed by selective laser melting for aerospace applications, Mechanical Depa tment of Wrocław University of Science and Technology, Wrocław 2018.
  • [17] LI Y., ZHOU J., PAVANRAM P., LEEFLANG M.A., FOCKAERT L.I., POURAN B., TÜMER N., SCHRÖDER K.-U., MOL J.M.C., WEINANS H., JAHR H., ZADPOOR A.A., Additively manufactured biodegradable porous magnesium, Acta Biomater., 2018, 67, 378–392, DOI: 10.1016/j.actbio.2017.12.008.
  • [18] LIU C., REN Z., XU Y., PANG S., ZHAO X., ZHAO Y., Biodegradable Magnesium Alloys Developed as Bone Repair Materials: A Review, Scanning, 2018, 1–15, DOI: 10.1155/2018/9216314.
  • [19] LIU C., ZHANG M., CHEN C., Effect of laser processing parameters on porosity, microstructure and mechanical properties of porous Mg-Ca alloys produced by laser additive manufacturing, Mater. Sci. Eng. A., 2017, 703, 359–371, DOI: 10.1016/j.msea.2017.07.031.
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  • [24] SALEHI M., MALEKSAEEDI S., FARNOUSH H., NAI M.L.S., MEENASHISUNDARAM G.K., GUPTA M., An investigation into interaction between magnesium powder and Ar gas: Implications for selective laser melting of magnesium, Powder Technol., 2018, 333, 252–261, DOI: 10.1016/j.powtec.2018.04.026.
  • [25] SAVALANI M.M., PIZARRO J.M., Effect of preheat and layer thickness on selective laser melting (SLM) of magnesium, Rapid Prototyp J., 2016, 22(1), 115–122, DOI: 10.1108/RPJ-07-2013-0076.
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Uwagi
Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-3c828384-c0bd-4f26-97bd-cc8057a0fa5c
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