Comparison of Microstructure, Ageing Effect and Shape Memory Properties of Additively Manufactured NiTi Alloy using LENS and EBAM Methods

• Autorzy: Dutkiewicz Jan , Rogal Łukasz , Węglowski Marek , Czujko Tomasz , Durejko Tomasz , Cesari Eduard

Identyfikatory

DOI

10.24425/amm.2023.145480

• Języki publikacji: EN

Abstrakty

EN

Samples prepared using various additive manufacturing methods were compared in terms of structure, texture, transformation temperature and superelastic properties. Samples manufactured using laser engineered net shaping (LENS) method showed texture several degrees deviated from the <001> build direction, however with composition near to the initial powder composition, enabling superelastic effect. The electron beam additive manufacturing (EBAM) samples showed martensitic structure at room temperature due to a shift of transformation temperatures to the higher range. This shift occurs due to a lower Ni content resulting from different processing conditions. However, EBAM method produced sharper <001> texture in the build direction and made it possible to obtain a good superelastic effect above room temperature. Intermetallic particles of size 0.5-2 mm were identified as Ti₂Ni phase using EDS and electron diffraction analyses. This phase was often formed at the grain boundaries. Contrary to the LENS method, the EBAM prepared samples showed Ni-rich primary particles resulted from different processing conditions that reduce the Ni content in the solid solution thus increase the martensitic transformation temperature. Ageing at 500°C allowed for shifting the martensitic transformation temperatures to the higher range in both, LENS and EBAM, samples. It resulted from the formation of Ni rich coherent precipitates. In samples prepared by both methods and aged at 500°C, the presence of martensite B19’ twins was observed mainly on {011} B19’ planes.

Słowa kluczowe

EN

additive manufacturing; shape memory alloys; NiT; TEM studies

• Wydawca: Institute of Metallurgy and Materials Science of Polish Academy of Sciences ; Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences
• Czasopismo: Archives of Metallurgy and Materials
• Rocznik: 2023
• Tom: Vol. 68, iss. 3
• Strony: 1103--1108
• Opis fizyczny: Bibliogr. 24 poz., fot., rys.

Twórcy

autor

Dutkiewicz Jan

• Institute of Metallurgy and Materials Science, PAS, 25, Reymonta Str., 30-059 Kraków, Poland

• https://orcid.org/0000-0001-5206-1153

autor

Rogal Łukasz

• Institute of Metallurgy and Materials Science, PAS, 25, Reymonta Str., 30-059 Kraków, Poland

• https://orcid.org/0000-0003-2289-8117

autor

Węglowski Marek

• Łukasiewicz - Institute of Welding, Błogosławionego Czesława 16-18, 44-100 Gliwice, Poland

• https://orcid.org/0000-0002-7082-0069

autor

Czujko Tomasz

• Military University of Technology, 2, Institute of Materials Science and Engineering, Gen. S. Kaliskiego Str., 00-908, Warsaw, Poland

• https://orcid.org/0000-0003-1610-7446

autor

Durejko Tomasz

• Military University of Technology, 2, Institute of Materials Science and Engineering, Gen. S. Kaliskiego Str., 00-908, Warsaw, Poland

• https://orcid.org/0000-0002-3278-1265

autor

Cesari Eduard

• University of Balearic Islands, Department of Physics, E07122, Palma de Mallorca, Spain

• https://orcid.org/0000-0002-5992-4369

Bibliografia

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Uwagi

The presented research results are the effect of the project no. UMO2016/23/B/ST8/00754 financed by the National Science Center, Poland.