Microscopic and spectroscopic investigation of carbon nanotubes-rhenium nanocomposites fabricated in different conditions

• Autorzy: Dobrzańska-Danikiewicz A. D. , Wolany W. , Gołombek K.

Identyfikatory

DOI

10.1016/j.acme.2017.04.008

• Języki publikacji: EN

Abstrakty

EN

The article describes the morphology of carbon-metal nanocomposites consisting of nanostructured rhenium permanently attached to carbon nanomaterials, in the form of single-walled (SWCNTs), double-walled (DWCNTs) or multi-walled carbon nanotubes (MWCNTs). Such nanocomposites are produced as a result of the high-temperature reduction of a rhenium precursor, including HReO4 or NH4ReO4, to metallic rhenium, deposited on the previously functionalised carbon nanomaterials in the form of nanoparticles whose size and dispersion are dependent upon the conditions of a technological process. Microscopic examinations carried out with scanning electron microscopy (SEM) and transmission electron microscopy (TEM) confirmed a differentiated structure of the presented nanocomposites depending on impregnation time in a rhenium precursor, which is one of the manufacturing steps of such materials. It has been demonstrated that longer impregnation time brings favourable results for material homogeneity in the whole volume. Moreover, the Raman spectroscopy results of functionalised carbon nanotubes and carbon nanotubes decorated with rhenium also has been presented.

Słowa kluczowe

EN

rhenium nanoparticles; carbon nanotube; nanocomposites; electron microscopy; Raman spectroscopy

PL

nanocząsteczki; nanokompozyty; mikroskopia elektronowa

• Wydawca: Springer ; Wrocław University of Science and Technology
• Czasopismo: Archives of Civil and Mechanical Engineering
• Rocznik: 2017
• Tom: Vol. 17, no. 4
• Strony: 978--985
• Opis fizyczny: Bibliogr. 37 poz., rys., tab., wykr.

Twórcy

autor

Dobrzańska-Danikiewicz A. D.

• Silesian University of Technology, Faculty of Mechanical Engineering, Konarskiego St. 18a, 44-100 Gliwice, Poland

autor

Wolany W.

• Silesian University of Technology, Faculty of Mechanical Engineering, Konarskiego St. 18a, 44-100 Gliwice, Poland

autor

Gołombek K.

• Silesian University of Technology, Faculty of Mechanical Engineering, Konarskiego St. 18a, 44-100 Gliwice, Poland

Bibliografia

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Uwagi

PL

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017)