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Microstructural and micromechanical tests of titanium biomaterials intended for prosthetic reconstructions

Treść / Zawartość
Identyfikatory
Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Purpose: The aim of the present paper was a question of structural identification and evaluation of strength parameters of Titanium (Ticp – grade 2) and its alloy (Ti6Al4V) which are used to serve as a base for those permanent prosthetic supplements which are later manufactured employing CAD/CAM systems. Methods: Microstructural tests of Ticp and Ti6Al4V were conducted using an optical microscope as well as a scanning microscope. Hardness was measured with the Vickers method. Micromechanical properties of samples: microhardness and Young’s modulus value, were measured with the Oliver and Pharr method. Results: Based on studies using optical microscopy it was observed that the Ticp from the milling technology had a single phase, granular microstructure. The Ti64 alloy had a two-phase, fine-grained microstructure with an acicular-lamellar character. The results of scanning tests show that titanium Ticp had a single phase structure. On its grain there was visible acicular martensite. The structure of the two phase Ti64 alloy consists of a β matrix as well as released α phase deposits in the shape of extended needles. Micromechanical tests demonstrated that the alloy of Ti64 in both methods showed twice as high the microhardness as Ticp. In studies of Young’s modulus of Ti64 alloy DMLS technology have lower value than titanium milling technology. Conclusions: According to the results obtained, the following conclusion has been drawn: when strength aspect is discussed, the DMLS method is a preferred one in manufacturing load structures in dentistry and may be an alternate way for the CAD/CAM system used in decrement processing.
Rocznik
Strony
121--127
Opis fizyczny
Bibliogr. 24 poz., rys., tab., wykr.
Twórcy
  • AGH University of Science and Technology, Faculty of Mechanical Engineering and Robotics, Kraków, Poland
autor
  • AGH University of Science and Technology, Faculty of Mechanical Engineering and Robotics, Kraków, Poland
  • Jagiellonian University Medical College, Faculty of Medicine, Department of Prosthetic Dentistry, Kraków, Poland
Bibliografia
  • [1] BARRIOBERO-VILA P., Effect of heat treatments on the microstructure of deformed Ti-6Al-4V, Wien, 2010.
  • [2] BĘDZIŃSKI R., Experimental and numerical methods in biomechanics, Biocybernetics & Biomedical Engineering, 2007, 27(1/2), 275–292.
  • [3] BURNAT B., WALKOWIAK-PRZYBYŁO M., BŁASZCZYK T., KLIMEK L., Corrosion behaviour of polished and sandblasted titanium alloys in PBS solution, Acta Bioeng. Biomech., 2013, 15(1), DOI: 10.5277/abb130111
  • [4] CHAHINE G., KOIKE M., OKABE T., SMITH P., KOVACEVIC R., The Design and Production of Ti-6Al-4V ELI, Customized Dental Implants, JOM, 2008, 60, 50–55.
  • [5] CHLEBUS E., KUŹNICKA B., KURZYNOWSKI T., DYBAŁA B., Microstructure and mechanical behaviour of Ti-6al.-7Nb alloy produced by selective laser melting, Materials Characterization, 2011, 62(5), DOI: 10.1016/j.matchar.2011.03.006
  • [6] CIOCCA L., FANTINI M., DE CRESCENZIO F., CORINALDESI G., SCOTTI R., Direct metal laser sintering (DMLS) of a customized titanium mesh for prosthetically guided bone regeneration of atrophic maxillary arches, Med. Biol. Eng. Comput., 2011, 49(11), 1347–52.
  • [7] DAS M., BHATTACHARY K., DITTRICK S.A., MANDAL C., BALLA V.K., SAMPATH KUMAR T.S. et al., In situ synthesized TiB-TiN reinforced Ti6Al4V alloy composite coatings: Microstructure, tribological and in-vitro biocompatibility, Journal of the Mechanical Behavior of Biomedical Materials, 2014, 29, 259–271.
  • [8] ISERI U., OZKURT Z., KAZAZOGLU E., Shear bond strengths of veneering porcelain to cast, machined and laser-sintered titanium, Dent. Mater. J., 2011, 30(3), 274–80.
  • [9] MANGANO C., PIATTELLI A., RASPANTI M., MANGANO F., CASSONI A., IEZZI G., SHIBLI J.A., Scanning electron microscopy (SEM) and X-ray dispersive spectrometry evaluation of direct laser metal sintering surface and human bone interface: a case series, Lasers Med. Sci., 2011, 26(1), 133–138.
  • [10] MURR L.E., ESQUIVEL E.V., QUINONES S.A., GAYTAN S.M., LOPEZ M.I., MARTINEZ E.Y. et al., Microstructures and Mechanical Properties of Electron Beam- Rapid Manufactured Ti-6Al-4V Biomedical Prototypes Compared to Wrought Ti-6Al-4V, Mater. Charact., 2009, 60, 96–109.
  • [11] MURR L.E., QUINONES S.A., GAYTAN S.M., LOPEZ M.I., RODELA A., MARTINEZ E.Y. et al., Microstructure and mechanical behavior of Ti-6Al-4V produced by rapid-layer manufacturing, for biomedical applications, Journal of the Mechanical Behavior of Biomedical Materials, 2009, 2, 20–32.
  • [12] ÖZCAN M., HAMMERLE C.H., Titanium as a Reconstruction and Implant Material in Dentistry: Advantages and Pitfalls, Materials, 2012, 5, 1528–1545.
  • [13] PN-EN ISO 6507-1:2007: Metals – Vickers hardness test – Part 1: Test method.
  • [14] Przewodnik PKN-ISO/IEC Guide 99, Wydawnictwo PKN, Warszawa 2010.
  • [15] RAFI H.K., KARTHIK N.V., GONG H., STARR T.L. STUCKER B.E., Microstructures and Mechanical Properties of Ti6Al4V Parts Fabricated by Selective Laser Melting and Electron Beam Melting, Journal of Materials Engineering and Performance, 2013, 22, 3872–3883.
  • [16] RAMOSOEU M.E., CHIKWANDA H.K., BOLOKANG A.S., BOOYSEN G., NGONDA T.N., Additive manufacturing: characterization of TI-6AI-4V alloy intended for biomedical application, Southern African Institute of Mining and Metallurgy advanced metals initiative: Light Metals Conference, Misty Hills, Muldersdrift, 27–29 October 2010, 337–344.
  • [17] RYNIEWICZ A., BOJKO Ł., RYNIEWICZ W., Selected Mechanical Properties of Titanium in Dental Implantology Reconstruction Procedure, Engineering of Biomaterials, 2012, 112, 48–53.
  • [18] RYNIEWICZ A.M., RYNIEWICZ W., Strength tests and tribological properties of titanium intended for construction of permanent prosthetic restorations, Implant Prosthetics, 2008, 1(30), 42–47.
  • [19] RYNIEWICZ A., RYNIEWICZ W., The Estimation of Selected Properties of Titanium to Performance of Prosthetic Restorations in CAD/CAM, Polish Journal of Enviromental Studies, 2007, 16(6C), 348–353.
  • [20] SONG B., DONG S., ZHANG B., LIAO H., CODDET C., Effects of processing parameters on microstructure and mechanical property of selective laser melted Ti6Al4V, Mater. Design, 2012, 35, 120–125.
  • [21] SZYMCZYK P., JUNKA A., ZIÓŁKOWSKI G., SMUTNICKA D., BARTOSZEWICZ M., CHLEBUS E., The ability of S. aureus to form biofilm on the Ti-6Al-7Nb scaffolds produced by Selective Laser Melting and subjected to the different types of surface modifications, Acta Bioeng. Biomech., 2013, 15(1). DOI: 10.5277/abb130109
  • [22] TRAINI T., MANGANO C., SAMMONS R.L, MANGANO F., MACCHI A., PIATTELLI A., Direct laser metal sintering as a new approach to fabrication of an isoelastic functionally graded material for manufacture of porous titanium dental implants, Dent. Mater., 2008, 24(11), 1525–1533.
  • [23] VRANCKEN B., THIJS L., KRUTH J.P., VAN HUMBEECK J., Heat treatment of Ti6Al4V produced by Selective Laser Melting: Microstructure and mechanical properties, Journal of Alloys and Compounds, 2012, 541, 177–185.
  • [24] YADROITSEV I., KRAKHMALEV P., YADROITSAVA I., Selective laser melting of Ti6Al4V alloy for biomedical applications: Temperature monitoring and microstructural evolution, Journal of Alloys and Compounds, 2012, 583, 404–409
Uwagi
PL
Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-3b1d7f25-7641-4564-8eaf-521726d1a025
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