Effect of Mn Amount on Phase Transformations and Magnetic Properties in Fe-Mn-Mo-Si Alloys

Armağan, Osman; Kirindi, Talip

doi:10.24425/amm.2021.134783

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Tytuł artykułu

Effect of Mn Amount on Phase Transformations and Magnetic Properties in Fe-Mn-Mo-Si Alloys

Autorzy

Armağan Osman , Kirindi Talip

Treść / Zawartość

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DOI

10.24425/amm.2021.134783

Warianty tytułu

Języki publikacji

Abstrakty

In this study, microstructural and crystallographic properties of phase transformations occurring with thermal effect in Fe-XMn-Mo-Si (X = 15.14wt.% ve 18.45wt.%) alloys have been investigated. The effects of (wt.%) Mn rates in the alloy on the characteristics of phase transformations were investigated by using Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) and X-Ray Diffraction (XRD). SEM and TEM investigations was observed that two different martensite (ε and α') structures were formed in austenite grain. In addition, in TEM observations, the interface regions were selected over the bright field image. Crystallographic orientation relationships were obtained by the analyses of electron diffraction patterns from the interface regions. γ → α' type transformation was observed for α' particle formation, and orientation relationship was found as (111)_γ // (011)_α', [101]_γ // [111]_α' and, γ → ε type transformation was observed for ε martensite plate formation, and the orientation relationship was found as (111)_γ // (0002)_ε, [110]_γ // [2110]_ε. It was noticed that this orientation relationships were compatible with the literature (Kurdjumov-Sachs and Shoji-Nishiyama orientation relationship). Precipitation phase (carbide) formation was observed in microstructure analyses. The changes in the magnetic properties of the alloys having different ratesof Mn as a consequence of thermal effect phase transformations was investigated by using Mössbauer Spectroscopy. The internal magnetic field, volume fractions (transformation rates), isomer shift values and magnetic characteristics of the main and product phases were revealed by Mössbauer Spectroscopy. In the Mössbauer Spectrum, it was noticed that ε-martensite and γ-austenite structures showed paramagnetic single-peak, and α'-martensite showed ferromagnetic six-peaks.

Słowa kluczowe

Fe-Mn-Mo-Si alloys heat treatment martensitic transformation crystallographic properties Mössbauer Spectroscopy

Wydawca

Institute of Metallurgy and Materials Science of Polish Academy of Sciences
Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences

Czasopismo

Archives of Metallurgy and Materials

Rocznik

2021

Tom

Vol. 66, iss. 1

Strony

259--266

Opis fizyczny

Bibliogr. 69 poz., fot., rys., tab., wzory

Twórcy

autor

Armağan Osman

o_armagan@windowslive.com

Karamanoğlu Mehmetbey University, Department of Medical Services and Techniques, Vocational School of Health Service, Program of Opticianry, 70200, Karaman, Turkey

autor

Kirindi Talip

Kirikkale University, Faculty of Education, Department of Mathematic and Science Education, Yahsihan 71450, Kirikkale, Turkey

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Uwagi

1. This study was supported by Kırıkkale University Scientific Research Fund with Project number 2016/131.

2. Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).

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Bibliografia

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