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Electrochemical codeposition of molybdenum and selenium

Treść / Zawartość
Identyfikatory
Warianty tytułu
PL
Elektrochemiczne osadzanie molibdenu z selenem
Języki publikacji
EN
Abstrakty
EN
The electrodeposition of Mo-Se thin films from a sulfate solution containing Na2MoO4 and H2SeO3 was studied. The process of deposition was conducted under potentiostatic conditions on a copper electrode. The effect of potential value, pH, and time of deposition were examined. The deposits were characterized by X-ray diffraction, X-ray fluorescence, and scanning electron microscopy. The obtained results have shown the possibility of co-deposition of molybdenum and selenium with different stoichiometric ratios.
PL
Przeprowadzono badania dotyczące procesu elektrochemicznego osadzania molibdenu z selenem z roztworów siarczanowych zawierających Na2Mo4 i H2SeO3. Proces osadzania przeprowadzono w warunkach potencjostatycznych na elektrodach miedzianych. Zbadano wpływ potencjału, pH elektrolitu oraz długości czasu osadzania na jakość otrzymanych powłok. Otrzymane warstwy były badane z wykorzystaniem dyfrakcji rentgenowskiej, spektrofluorymetrii rentgenowskiej oraz skaningowego mikroskopu elektronowego. Wykazano możliwość otrzymania powłok o różnym stosunku molibdenu do selenu
Rocznik
Strony
7--16
Opis fizyczny
Bibliogr. 32 poz., yab., wykr.
Twórcy
autor
  • AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Krakow, Poland
autor
  • AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Krakow, Poland
autor
  • AGH University of Science and Technology, Academic Centre for Materials and Nanotechnology, Krakow, Poland
autor
  • AGH University of Science and Technology, Faculty of Metal Engineering and Industrial Com¬puter Science, Krakow, Poland
autor
  • AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Krakow, Poland
  • AGH University of Science and Technology, Faculty of Non-Ferrous Metals, Krakow, Poland
Bibliografia
  • [1] Yang J., Shin H.S.: Recent advances in layered transition metal dichalcogenides for hydrogen evolution reaction. Journal of Materials Chemistry A, 2, 17 (2014), 5979-5985
  • [2] Pumera M., Sofer Z., Ambrosi A.: Layered transition metal dichalcogenides for electrochemical energy generation and storage. Journal of Materials Chemistry A, 2, 24 (2014), 8981-8987
  • [3] Chan K., Tsai C., Hansen H. A., Norskov J. K.: Molybdenum sulfides and selenides as possible electrocatalysts for CO2 reduction. Chemcatchem, 6, 7 (2014), 1899-1905
  • [4] Ponomarev E.A., Neumann-Spallart M., Hodes G., Levy-Clement C.: Electrochemical deposition of MoS2 thin films by reduction of tetrathiomolybdate. Thin Solid Films, 280, 1-2 (1996), 86-89
  • [5] Le Berre F., Tshimanga D., Guilloux A.L., Leclercq J., Sergent M., Pena O., Horyn R., Wojakowski A.: Rare-earth doping of the Mo3Se4 superconductor. Physica B: Condensed Matter, 228, 3-4 (1996), 261-271
  • [6] Aruchamy A.: Photoelectrochemistry and photovoltaics of layered semiconductors. Kluwer Academic, Dordrecht - Boston, 1992.
  • [7] Shariza S., Anand T.J.S.: Effect of deposition time on the structural and optical properties of molybdenum chalcogenides thin films. Chalcogenide Letters, 8, 9 (2011), 529-539
  • [8] Landolt D.: Electrodeposition science and technology in the last quarter of the twentieth century. Journal of the Electrochemical Society, 149, 3 (2002), S9-S20
  • [9] Mech K., Żabiński P., Mucha M., Kowalik R.: Electrodeposition of catalytically active Ni-Mo alloys. Archives of Metallurgy and Materials, 58, 1 (2013), 227-229
  • [10] Rajeshwar K.: Electrosynthesized thin films of group II—VI compound semiconductors, alloys and superstructures. Advanced Materials, 4, 1 (1992), 23-29
  • [11] Lincot D.: Electrodeposition of semiconductors. Thin Solid Films, 487, 1-2 (2005), 40-48
  • [12] Kowalik R., Żabiński P., Fitzner K.: Electrodeposition of ZnSe. Electrochimica Acta, 53, 21 (2008), 6184-6190
  • [13] Alkire R.C.: Advances in Electrochemical Science and Engineering, vol. 12. Wiley-VCH, Chichester, 2010
  • [14] Zabiński P., Mech K., Kowalik R.: Co-Mo and Co-Mo-C alloys deposited in a magnetic field of high intensity and their electrocatalytic properties. Archives of Metallurgy and Materials, 57, 1 (2012), 127-133
  • [15] Chandra S., Sahu S.N.: Electrodeposited semiconducting molybdenum selenide films. I. Preparatory technique and structural characterisation. Journal of Physics D: Applied Physics, 17, 10 (1984), 2115-2123
  • [16] Joseph Sahaya Anand T., Sanjeeviraja C., Jayachandran M.: Preparation of layered semiconductor (MoSe2) by electrosynthesis. Vacuum, 60, 4 (2000), 431-435
  • [17] Dukstiene N., Kazancev K., Prosicevas I., Guobiene A.: Electrodeposition of Mo-Se thin films from a sulfamatic electrolyte. Journal of Solid State Electrochemistry, 8, 5 (2004), 330-336
  • [18] Delphine S.M., Jayachandran M., Sanjeeviraja C.: Pulsed electrodeposition and characterization of molybdenum diselenide thin film. Materials Research Bulletin, 40, 1 (2005), 135-147
  • [19] Dukstiene N., Tatariskinaite L.: Electrochemical examination of the influence of H2SeO3 on molybdenum electrodeposition on tin oxide electrode from aqueous citrate electrolyte. Polish Journal of Chemistry, 80, 10 (2006), 1715-1729
  • [20] Hahn B.P., Stevenson K.J.: Cathodic electrodeposition of mixed molybdenum-selenium oxides. Journal of Electroanalytical Chemistry, 638, 1 (2010), 151-160
  • [21] Kröger F.A.: Cathodic deposition and characterization of metallic or semiconducting binary alloys or compounds. Journal of the Electrochemical Society, 125, 12 (1978), 2028-2034
  • [22] Gawęda S., Kowalik R., Kwolek P., Macyk W., Mech J., Oszajca M., Podborska A., Szaciłowski K.: Nanoscale digital devices based on the photoelectrochemical photocurrent switching effect: Preparation, proper¬ties and applications. Israel Journal of Chemistry, 51 (2011), 36-55
  • [23] Baker H.: Alloy phase diagrams. Materials Park, Ohio, ASM International, 1992
  • [24] Kowalik R., Fitzner K.: About the conditions of zinc selenide electrodeposition from aqueous solutions. Metallurgy and Foundry Engineering, 30, 2 (2004), 140-141
  • [25] Kowalik R., Fitzner K.: Analysis of the mechanism for electrodeposition of the ZnSe phase on Cu substrate. Journal of Electroanalytical Chemistry, 633, 1 (2009), 78-84
  • [26] Kowalik R., Szaciłowski K., Zabiński P.: Photoelectrochemical study of ZnSe electrodeposition on Cu electrode. Journal of Electroanalytical Chemistry, 674 (2012), 108-112
  • [27] Pourbaix M.: Atlas of Electrochemical Equilibria in Aqueous Solutions. Pergamon, New York, 1966
  • [28] Pope M.T.: Heteropoly and isopoly oxometalates. Springer-Verlag, Berlin - New York, 1983
  • [29] Bouroushian M.: Electrochemistry of metal chalcogenides. Springer, Berlin, 2010
  • [30] Nunez M.: Metal electrodeposition. Nova Science Publishers, New York, 2005
  • [31] Podlaha E.J., Landolt D.: Induced codeposition. III. Molybdenum alloys with nickel, cobalt, and iron. Journal of the Electrochemical Society, 144, 5 (1997), 1672-1680
  • [32] Podlaha E.J., Landolt D.: Induced codeposition: I. An experimental investigation of Ni-Mo alloys. Journal of the Electrochemical Society, 143, 3 (1996), 885-892
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-36de1abf-8cdc-42d5-958c-1d763dbdfc4f
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