Degradation and physical properties of sugar palm starch/ sugar palm nanofibrillated cellulose bionanocomposite

• Autorzy: Atikah M. S. N. , Ilyas R. A. , Sapuan S. M. , Ishak M. R. , Zainudin E. S. , Ibrahim R. , Atiqah A. , Ansari M. N. M. , Jumaidin R.

Identyfikatory

DOI

10.14314/polimery.2019.10.5

Warianty tytułu

PL

Degradacja i właściwości fizyczne bionanokompozytów skrobi palmy cukrowej wzmocnionej nanowłóknami celulozowymi tej palmy

• Języki publikacji: EN

Abstrakty

EN

This paper aims to study the degradation rate of sugar palm nanofibrillated cellulose (SPNFCs) and sugar palm starch (SPS). SPNFCs were isolated from sugar palm fiber, while SPS is extracted from sugar palm trunk. The SPNFCs were reinforced with SPS biopolymer as biodegradable reinforcement materials of different diameter/length based on the number of passes of high pressurize homogenization process (5, 10 and 15 passes represented by SPS/SPNFCs-5, SPS/SPNFCs-10, and SPS/SPNFCs-15). These SPNFCs were incorporated into SPS plasticized with glycerol and sorbitol via solution casting method. Soil burial experiment performed on SPS and SPS/SPNFCs bionanocomposites showed that SPS was degraded more rapidly by losing 85.76% of its mass in 9 days compared to 69.89% by SPS/SPNFCs-15 bionanocomposite. The high compatibility between SPNFCs nanofiber and SPS biopolymer matrices can be observed through field emission scanning electron microscopy (FE-SEM).

PL

Zbadano szybkość degradacji nanowłóknistej celulozy wyizolowanej z palmy cukrowej (Arenga pinnata) (SPNFCs) oraz skrobi wydzielonej przez ekstrakcję z rdzenia pnia tej palmy (SPS). SPNFCs uzyskiwano z włókien palmy cukrowej, poddawanych homogenizacji pod wysokim ciśnieniem w 5, 10 lub 15 cyklach, otrzymując nanowłókna celulozy o różnej długości i średnicy. SPNFCs wprowadzano do SPS uplastycznionego mieszaniną (1 : 1) glicerolu isorbitolu. Metodą odlewania z roztworu wytwarzano błony nanokompozytowe SPS/SPNFCs-5, SPS/SPNFCs-10 i SPS/SPNFCs-15. Test glebowy procesu biodegradacji wykazał, że SPS ulegało szybszej degradacji, tracąc 85,76% swojej masy w ciągu 9 dni, w porównaniu z ubytkiem masy 69,89% w wypadku bionanokompozytu SPS/SPNFCs-15. Na podstawie analizy metodą skaningowej mikroskopii elektronowej z emisją polową (FE-SEM) stwierdzono dużą kompatybilność między nanowłóknami SPNFCs i biopolimerową osnową SPS.

Słowa kluczowe

EN

sugar palm; high pressurized homogenizer; nanofibrillated cellulose; nanocomposites; soil burial degradation

PL

palma cukrowa; homogenizacja wysokociśnieniowa; nanowłóknista celuloza; nanokompozyty; degradacja w glebie

• Wydawca: Sieć Badawcza Łukasiewicz – Instytut Chemii Przemysłowej
• Czasopismo: Polimery
• Rocznik: 2019
• Tom: T. 64, nr 10
• Strony: 680--689
• Opis fizyczny: Bibliogr. 57 poz., rys. kolor.

Twórcy

autor

Atikah M. S. N.

• Universiti Putra Malaysia, Department of Chemical and Environmental Engineering, 43400 UPM Serdang, Selangor, Malaysia

autor

Ilyas R. A.

• Universiti Putra Malaysia, Institute of Tropical Forestry and Forest Products, Laboratory of Biocomposite Technology, 43400 UPM Serdang, Selangor, Malaysia
• Universiti Putra Malaysia, Advanced Engineering Materials and Composites Research Centre, Department of Mechanical and Manufacturing Engineering, 432400 UPM Serdang, Selangor, Malaysia

autor

Sapuan S. M.

• Universiti Putra Malaysia, Institute of Tropical Forestry and Forest Products, Laboratory of Biocomposite Technology, 43400 UPM Serdang, Selangor, Malaysia
• Universiti Putra Malaysia, Advanced Engineering Materials and Composites Research Centre, Department of Mechanical and Manufacturing Engineering, 432400 UPM Serdang, Selangor, Malaysia
• [e-mail]

autor

Ishak M. R.

• Universiti Putra Malaysia, Department of Aerospace Engineering, 43400 UPM Serdang, Selangor, Malaysia

autor

Zainudin E. S.

• Universiti Putra Malaysia, Advanced Engineering Materials and Composites Research Centre, Department of Mechanical and Manufacturing Engineering, 432400 UPM Serdang, Selangor, Malaysia

autor

Ibrahim R.

• Forest Research Institute Malaysia, Pulp and Paper Branch, 52109 Kepong, Selangor, Malaysia

autor

Atiqah A.

• Universiti Tenaga Nasional, Institute of Power Engineering, 43000 Kajang, Selangor, Malaysia

autor

Ansari M. N. M.

• Universiti Tenaga Nasional, Institute of Power Engineering, 43000 Kajang, Selangor, Malaysia

autor

Jumaidin R.

• Universiti Teknikal Malaysia Melaka, Fakulti Teknologi Kejuruteraan Mekanikal dan Pembuatan, Hang Tuah Jaya, 76100 Durian Tunggal, Melaka, Malaysia

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).