Use of magnetic nanoparticles in an Ionic liquid (BMIM-PF6) based vortex‐assisted dispersive liquid-liquid microextraction (VSLLME) for measuring the traces amounts of cadmium in environmental, biological and nutritional samples

• Autorzy: Payab Meghdad , Maleki Fatemeh Yousefnezhad , Sheikhloie Hossein , Baghban Ali

Identyfikatory

DOI

10.58332/scirad2023v2i4a05

• Języki publikacji: EN

Abstrakty

EN

In the present project, the magnetic nanoparticles were used in a type of an ionic liquid based micro-extraction to measure trace amounts of cadmium in different real samples containing environmental water samples, saliva and human hair. In the optimum condition, the recovery percentages for the real sample were about 94.5% to 101.3%, showing the designed method is suitable to be used for analyzing the real environmental and biological samples. The main parameters were evaluated and optimized as follows: pH was 2.5, the volume of ionic liquid was 150 μl, the amount of Fe3O4 magnetic nanoparticles was 50mg, the volume of the complexing agent was 12 μl, and the vortex time was 1 min and 2 min for ionic liquid, and magnetic nanoparticle distribution steps, respectively. Also, the volume of the medium was 10 to 20 ml.

Słowa kluczowe

EN

VSLLME; cadmium; vortex-assisted; heavy metal; real sample

PL

VSLLME; kadm; vortex-assisted; metale ciężkie; próbka rzeczywista

• Wydawca: Radomskie Towarzystwo Naukowe
• Czasopismo: Scientiae Radices
• Rocznik: 2023
• Tom: Vol. 2, Iss. 4
• Strony: 359--377
• Opis fizyczny: Bibliogr. 57 poz., 1 il. kolor., wykr.

Twórcy

autor

Payab Meghdad

• Department of Chemistry, University of Mazandaran, Mazandaran, Iran

autor

Maleki Fatemeh Yousefnezhad

• Department of Chemistry, Payam Noor University, Maragheh, Iran

autor

Sheikhloie Hossein

• Department of Chemistry, Maragheh branch, Islamic Azad University, Maragheh, Iran

autor

Baghban Ali

• Department of Chemistry, Payam Noor University, Maragheh, Iran

Bibliografia

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2024).