Evaluation of capabilities of the nanoindentation test in the determination of flow stress characteristics of the matrix material in porous sinters

• Autorzy: Madej Lukasz , Legwand Adam , Setty Mohan , Mojzeszko Mateusz , Perzyński Konrad , Roskosz Stanisław , Chrapoński Jacek

Identyfikatory

DOI

10.1007/s43452-021-00343-y

• Języki publikacji: EN

Abstrakty

EN

Herein, we evaluate the nanoindentation test capabilities in the determination of flow stress characteristics of the matrix material in porous sinters. The Distaloy AB sample with 15% porosity after the sintering operation is selected as a case study for the investigation. 2D and 3D imaging techniques are employed first to highlight difficulties in identifying reliable nano hardness measurement zones for further properties evaluation. Then, nanoindentation test results are acquired with Berkovich tip pressed under various loads at different locations in the sample. Systematic indentations in the quartz sample are used as a cleaning procedure to minimize the effect of the possible build-up around the indenter tip. The representative indentation load range is selected based on the extracted material characteristics. With that, the stress–strain response of the sinter matrix material is identified. The reliability of the determined flow stress curve is confirmed with the use of conical nanoindentation measurement results and finite element simulations. Obtained results show that it is possible to calculate reliable flow stress characteristics of the matrix in the porous samples, with the assumption that experiments under various loading conditions and from various locations in the matrix are performed. It is also pointed out that various indentation loads should be used to eliminate the influence of the pile-up or scale effects that affect the overall material response.

Słowa kluczowe

EN

sintered steel; nanoindentation; flow stress

PL

stal spiekana; nanowgniecenie; naprężenie

• Wydawca: Springer ; Wrocław University of Science and Technology
• Czasopismo: Archives of Civil and Mechanical Engineering
• Rocznik: 2022
• Tom: Vol. 22, no. 1
• Strony: art. no. e21, 2022
• Opis fizyczny: Bibliogr. 34 poz., rys., wykr.

Twórcy

autor

Madej Lukasz

• Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Mickiewicza 30 av., 30-059 Krakow, Poland

• https://orcid.org/0000-0003-1032-6963

autor

Legwand Adam

• Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Mickiewicza 30 av., 30-059 Krakow, Poland

autor

Setty Mohan

• Institute for Frontier Materials, Deakin University, Geelong, VIC 3217, Australia

autor

Mojzeszko Mateusz

• Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Mickiewicza 30 av., 30-059 Krakow, Poland

autor

Perzyński Konrad

• Faculty of Metals Engineering and Industrial Computer Science, AGH University of Science and Technology, Mickiewicza 30 av., 30-059 Krakow, Poland

autor

Roskosz Stanisław

• Faculty of Materials Engineering and Metallurgy, Silesian University of Technology, Krasińskiego 8 st., 40-019 Katowice, Poland

autor

Chrapoński Jacek

• Faculty of Materials Engineering and Metallurgy, Silesian University of Technology, Krasińskiego 8 st., 40-019 Katowice, Poland

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Uwagi

PL

Opracowanie rekordu ze środków MEiN, umowa nr SONP/SP/546092/2022 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2022-2023)