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Sepiolite and the sepiolite-based materials were studied in terms of carbon dioxide adsorption. The pore structure and the surface characterization of the obtained materials were specified based on adsorption-desorption isotherms of nitrogen measured at –196°C and carbon dioxide at 0°C. The specifi c surface area (SSA) was calculated accord-ing to the BET equation. The pore volume was estimated using the DFT method. Pristine sepiolite has shown the following value of SSA and CO2 uptake at 0°C – 105 m2/g and 0.27 mmol/g, respectively. The highest value of these parameters was found for material obtained by KOH activation of mixture sepiolite and molasses (MSEP2) – 676 m2/g and 1.49 mmol/g. Sample MSEP2 also indicated the highest value of total pore volume and micropores volume with a diameter up to 0.8 nm.
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Tom
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1--6
Opis fizyczny
Bibliogr 54 poz., rys., tab.
Twórcy
autor
- West Pomeranian University of Technology, Szczecin, Faculty of Chemical Technology and Engineering, Department of Catalytic and Sorbent Materials Engineering, Piastów Ave. 42, 71-065 Szczecin, Poland
autor
- West Pomeranian University of Technology, Szczecin, Faculty of Chemical Technology and Engineering, Department of Catalytic and Sorbent Materials Engineering, Piastów Ave. 42, 71-065 Szczecin, Poland
Bibliografia
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- 6. Srenscek-Nazzal, J., Narkiewicz, U., Morawski, A.W., Wrobel, R.J., Gesikiewicz-Puchalska, A. & Michalkiewicz, B. (2016). Modification of Commercial Activated Carbons for CO2 Adsorption. Acta Phys. Pol. A 129, 394–401. DOI: 10.12693/APhysPolA.129.394.
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- 8. Gęsikiewicz-Puchalska, A., Zgrzebnicki, M., Michalkiewicz, B., Narkiewicz, U., Morawski, A.W. & Wróbel, R.J. (2017). Improvement of CO2 uptake of activated carbons by treatment with mineral acids. Chem. Eng. J. 309, 159–171. DOI: 10.1016/j.cej.2016.10.005.
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- 17. Młodzik, J., Sreńscek-Nazzal, J., Narkiewicz, U., Morawski, A.W., Wróbel, R.J. & Michalkiewicz, B. (2016). Activated Carbons from Molasses as CO2 Sorbents. Acta Phys. Pol. A. 129, 402–404. DOI: 10.12693/APhysPolA.129.402.
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- 19. Shi, X., Gong, J., Kierzek, K., Michalkiewicz, B., Zhang, S., Chu, P.K., Chen, X., Tang, T. & Mijowska, E. (2019) Multifunctional nitrogen-doped nanoporous carbons derived from metal-organic frameworks for efficient CO2 storage and high-performance lithium-ion batteries. New J. Chem. 43, 10405–10412. DOI: doi.org/10.1039/C9NJ01542F.
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- 35. Majewska, J. & Michalkiewicz, B. (2014). Carbon nanomaterials produced by the catalytic decomposition of methane over Ni/ZSM-5 Significance of Ni content and temperature. New Carbon Mater. 29, 102–108. DOI: 10.1016/S1872-5805(14)60129-3.
- 36. Ziebro, J., Łukasiewicz, I., Borowiak-Palen, E. & Michalkiewicz, B. (2010). Low temperature growth of carbon nanotubes from methane catalytic decomposition over nickel supported on a zeolite. Nanotechnology 21, 1–6. DOI: 10.1088/0957-4484/21/14/145308.
- 37. Ziebro, J., Łukasiewicz, I., Grzmil, B., Borowiak-Palen, E. & Michalkiewicz, B. (2009). Synthesis of nickel nanocapsules and carbon nanotubes via methane CVD. J. Alloys Compd. 485, 695–700. DOI: 10.1016/j.jallcom.2009.06.039.
- 38. Majewska, J. & Michalkiewicz, B. (2016). Preparation of Carbon Nanomaterials over Ni/ZSM-5 Catalyst Using Simplex Method Algorithm. Acta Phys. Pol., A. 129, 153–157. DOI: 10.12693/APhysPolA.129.153.
- 39. Börjesson, P., Lantz, M., Andersson, J., Björnsson, L., Möller, B.F., Fröberg, M., Hanarp, P., Hulteberg, C., Iverfeldt, E., Lundgren, J., Röj, A., Svensson, H. & Zinn, E. (2016). Methane as vehicle fuel – a well to wheel analysis (METDRIV). DOI: 10.13140/rg.2.2.24258.79045
- 40. Sreńscek-Nazzal, J., Kamińska, W., Michalkiewicz, B. & Koren, Z.C. (2013). Production, characterization and methane storage potential of KOH-activated carbon from sugarcane molasses. Ind. Crop. Prod. 47, 153–159. DOI: 10.1016/j.ind-crop.2013.03.004.
- 41. Wenelska, K., Michalkiewicz, B., Gong, J., Tang, T., Kaleńczuk, R., Chen, X. & Mijowska, E. (2013). In situ deposition of Pd nanoparticles with controllable diameters in hollow carbon spheres for hydrogen storage. Int. J. Of Hydrogen Energy 38, 16179–16184. DOI: 10.1016/j.ijhydene.2013.10.008.
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Uwagi
Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2021).
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Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-32005bf2-9a6f-4b42-b768-a886a1d9a95e