Characterization and identification of flavonoids from Bambusa chungii leaves extract by UPLC-ESI-Q-TOF-MS/MS

Yuan, Ting; Guo, Xue-Feng; Shao, Si-Yue; An, Rong-Miao; Wang, Jin; Sun, Jia

doi:10.1556/1326.2020.00777

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Tytuł artykułu

Characterization and identification of flavonoids from Bambusa chungii leaves extract by UPLC-ESI-Q-TOF-MS/MS

Autorzy

Yuan Ting , Guo Xue-Feng , Shao Si-Yue , An Rong-Miao , Wang Jin , Sun Jia

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1556/1326.2020.00777

Warianty tytułu

Języki publikacji

Abstrakty

Bamboo leaves extract (BLE) has a variety of physiological functions such as antitumour, anti-inflammatory, antioxidant and blood fat reduction activities and the flavonoids of bamboo leaves are the major active constituents. To profile the flavonoids in the complex BLE, a rapid and sensitive analytical method based on ultra-high-performance liquid chromatography coupled with electrospray ionization quadrupole time-of-flight tandem mass spectrometry (UPLC-ESI-Q-TOF-MS/MS) was developed for the structural identification of the flavonoids in Bambusa chungii leaves extract using accurate mass measurements and characteristic fragmentation patterns. After separation on an Agilent SB-C18 Rapid Resolution High Definition (RRHD) column (2.1 mm × 150 mm, 1.8 μm) by gradient elution with 0.1% formic acid aqueous solution and acetonitrile as the mobile phase, the sample was analysed by ESI-QTOF-MS/MS in the negative mode. A total of 22 flavonoids were detected, and eight of these were identified by comparison with reference standards, while the other fourteen were tentatively identified according to their MS/MS data. The main fragmentation pathways of flavonoid C-glycosides (compounds 1, 5 and 10), flavonoid di-C,O-glycosides (compound 4), flavonoid di-C-glycosides (compound 7) and flavonoid C,O-di-glycosides (compounds 2 and 14) are shown in this article. This is the first report on the analysis of the flavonoids in the extract of B. chungii leaves. The present work demonstrates that UPLC-ESI-Q-TOF-MS/MS is an efficient technique for identifying multiple flavonoids of BLE.

Słowa kluczowe

flavonoids bamboo leaves extract BLE UPLC-ESI-Q-TOF-MS/MS fragmentation pathway Bambusa chungii

Wydawca

University of Silesia in Katowice
Akademiai Kiado

Czasopismo

Acta Chromatographica

Rocznik

2021

Tom

Vol. 33, no. 3

Strony

281--294

Opis fizyczny

Biblior. 45 poz., rys., tab.

Twórcy

autor

Yuan Ting

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

autor

Guo Xue-Feng

gxf71622@icbr.ac.cn

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

autor

Shao Si-Yue

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

autor

An Rong-Miao

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

autor

Wang Jin

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

autor

Sun Jia

Key Laboratory of National Forestry and Grassland Administration, Beijing for Bamboo & Rattan Science and Technology, Beijing 100102, PR China

Bibliografia

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Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-319391ad-36bf-4af9-86d3-ffeeb6cc7e83