Formation of Fe and Ni substituted LiMn2–XMXO4 nanopowders and their crystal and electronic structure and magnetic properties

Talik, E.; Lipińska, L.; Guzik, A.; Zajdel, P.; Michalska, M.; Szubka, M.; Kądziołka-Gaweł, M.; Paul, R. L.

doi:10.1515/msp-2017-0014

Artykuł - szczegóły

Tytuł artykułu

Formation of Fe and Ni substituted LiMn2–XMXO4 nanopowders and their crystal and electronic structure and magnetic properties

Autorzy

Talik E. , Lipińska L. , Guzik A. , Zajdel P. , Michalska M. , Szubka M. , Kądziołka-Gaweł M. , Paul R. L.

Wybrane pełne teksty z tego czasopisma

Identyfikatory

DOI

10.1515/msp-2017-0014

Warianty tytułu

Języki publikacji

Abstrakty

The Pechini sol-gel method was applied to obtain LiMn_2–xT_xO₄ (T = Ni, Fe; x = 0.1 to 0.5) nanopowders. Crystal and electronic structures, chemical composition and magnetic properties of the materials were characterized by X-ray diffraction, XPS, SEM/EDX microscopy, prompt gamma-ray activation analysis (PGAA), Mössbauer spectroscopy and magnetic susceptibility, respectively. XRD measurements showed that the LiMn_2–xNi_xO₄ were single phase for x = 0.1 and 0.2. Three samples with higher Ni content contained some addition of a second phase. Analysis of the oxidation state of the dopants by XPS revealed ionic Ni²⁺ and Fe³⁺. Mössbauer spectroscopy also confirmed 3+ oxidation state of iron and its location in octahedral sites, which excluded the inverse spinel configuration. XPS examinations showed that Mn³⁺ ions dominated in the iron substituted series whereas the Mn⁴⁺ was dominant in the nickel series.

Słowa kluczowe

nanomaterials lithium manganese nickel oxides spinel

Wydawca

De Gruyter

Czasopismo

Materials Science Poland

Rocznik

2017

Tom

Vol. 35, No. 1

Strony

159--172

Opis fizyczny

Bibliogr. 66 poz., rys., tab.

Twórcy

autor

Talik E.

Institute of Physics, University of Silesia, Uniwersytecka 4, 40-007 Katowice, Poland
talik@us.edu.pl

autor

Lipińska L.

Institute of Electronic Materials Technology, Wólczynska 133, 01-919 Warszawa, Poland

autor

Guzik A.

Institute of Physics, University of Silesia, Uniwersytecka 4, 40-007 Katowice, Poland

autor

Zajdel P.

Institute of Physics, University of Silesia, Uniwersytecka 4, 40-007 Katowice, Poland

autor

Michalska M.

Institute of Electronic Materials Technology, Wólczynska 133, 01-919 Warszawa, Poland

autor

Szubka M.

Institute of Physics, University of Silesia, Uniwersytecka 4, 40-007 Katowice, Poland

autor

Kądziołka-Gaweł M.

Institute of Physics, University of Silesia, Uniwersytecka 4, 40-007 Katowice, Poland

autor

Paul R. L.

Analytical Chemistry Division, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA

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Uwagi

Opracowanie ze środków MNiSW w ramach umowy 812/P-DUN/2016 na działalność upowszechniającą naukę (zadania 2017).

Typ dokumentu

Bibliografia

Identyfikator YADDA

bwmeta1.element.baztech-2e591952-12a2-41d2-8d3f-a30ea4f6c051