A fast chemometrics approach to quantitative analysis of metformin hydrochloride, enalapril maleate, and captopril in tablets based on HPLC-PAD spectra

• Autorzy: Muhire Jules , Li Bao Qiong , Zhai Hong Lin , Wang Xue , Xu Min Li

Identyfikatory

DOI

10.1556/1326.2018.00479

• Języki publikacji: EN

Abstrakty

EN

Diabetes mellitus and concurrent hypertension disorder are dreadful all over the world and are often managed by some drugs, such as metformin hydrochloride (MFH), enalapril maleate (ENM), and captopril (CAP). In this work, a reliable and fast quantitative analysis of these three components in tablets was carried out by Tchebichef image moment method and multivariate curve resolution with alternating least squares on three-dimensional (3D) spectra obtained by high-performance liquid chromatography coupled with photodiode array detection (HPLC-PAD). 3D spectra were obtained within only 2 min, and linear quantitative models were established by stepwise regression based on the calculated image moments. Among these two methods, Tchebichef image moment method showed outcome distinction. The correlation coefficients of cross-validation (R_Loo-cv) are more than 0.988, while their recoveries are 100.1 ± 1.7% (MFH), 95.4 ± 5.4% (ENM), and 105.3 ± 5.7% (CAP), respectively. The intra- and inter-day precisions (RSD) are less than 5.42%. The proposed methods were also applied to the analysis of real tablets. This study reveals the effectiveness and convenience of the proposed image-moment method that may be a potential technology for the quality control and investigation of drugs in routine analysis.

Słowa kluczowe

EN

HPLC-PAD; Tchebichef moments; quantitative analysis; metformin hydrochloride; enalapril maleate; captopril

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2019
• Tom: Vol. 31, no. 3
• Strony: 228--234
• Opis fizyczny: Bibliogr. 31 poz., rys., tab.

Twórcy

autor

Muhire Jules

• College of Chemistry & Chemical Engineering, Lanzhou University, Lanzhou, 730000, PR China

autor

Li Bao Qiong

• College of Chemistry & Chemical Engineering, Lanzhou University, Lanzhou, 730000, PR China

autor

Zhai Hong Lin

• College of Chemistry & Chemical Engineering, Lanzhou University, Lanzhou, 730000, PR China

autor

Wang Xue

• College of Chemistry & Chemical Engineering, Lanzhou University, Lanzhou, 730000, PR China

autor

Xu Min Li

• College of Chemistry & Chemical Engineering, Lanzhou University, Lanzhou, 730000, PR China

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Uwagi

PL

Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2019).