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This study presents the preliminary results of investigation of the lime mortars and plasters from archaeological excavations in Hippos (Israel), using Electron Paramagnetic Resonance (EPR) spectroscopy. The research was conducted in order to characterize the building material and its reaction to ionizing radiation. The ancient settlement Hippos, situated on the east shore of the Sea of Galilee, functioned from the 3rd cent. BC until it was destroyed by the earthquake in 749 AD. Lime mortars and plasters show carbonate and locally gypsum character of binder and different kind of aggregate. Samples were γ-irradiated and measured using X-band EPR spectrometer. Computer Resolution Enhancement Method was applied to the complex spectra. Some of the γ-induced EPR signals were attributed to CO 2 and CO 33- paramagnetic centres. Exponential growth of the dose response curve above 1 kGy and saturation for doses above 20 kGy was observed. For doses lower than 1 kGy the dose response curve has a linear character. The presence of γ-sensitive carbonate paramagnetic centres could indicate that, after further studies, well-chosen samples of mortars and plasters might be suitable for EPR dating, assuming the centres have been sufficiently bleached during the manufacturing process.
Słowa kluczowe
Wydawca
Czasopismo
Rocznik
Tom
Strony
112--120
Opis fizyczny
Bibliogr. 30 poz., rys., tab., wykr.
Twórcy
autor
- Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznań, Poland
autor
- Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznań, Poland
autor
- Department of Dynamic and Regional Geology, Institute of Geology, Faculty of Geographical and Geological Sciences, Adam Mickiewicz University, Maków Polnych 16, 61-606 Poznań, Poland
autor
- Medical Physics Division, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznań, Poland
Bibliografia
- 1.Amiran DHK, Arieh E and Turcotte T, 1994. Earthquakes in Israel and adjacent areas: macroseismic observations since 100 BCE. Israel Exploration Journal 44: 260–305.
- 2.Barabas M, 1992. The nature of the paramagnetic centres at g = 2.0057 and g = 2.0031 in marine carbonates. Nuclear Tracks and Radiation Measurements 20(3): 453–464, DOI 10.1016/1359-0189(92)90031-P.
- 3.Barabas M, Bach A, Mudelsee M and Mangini A, 1992. General properties of the paramagnetic centre at g = 2.0006 in carbonates. Quaternary Science Reviews 11(1–2): 165–171, DOI 10.1016/0277-3791(92)90059-H.
- 4.Callens F, Vanhaelewyn G, Matthys P and Boesman E, 1998. EPR of carbonate derived radicals: applications in dosimetry, dating and detection of irradiated food. Applied Magnetic Resonance 14(2–3): 235–254, DOI 10.1007/BF03161892.
- 5.Dobosz B and Krzyminiewski R, 2007a. Characteristic of paramagnetic centres in burnt clay and pottery by the EPR method. Radiation Measurements 42(2): 213–219, DOI 10.1016/j.radmeas.2006.11.003.
- 6.Dobosz B and Krzyminiewski R, 2007b. Linear transformation of EPR spectra as a method proposed for improving identification of paramagnetic species in ceramic. Applied Radiatiation and Isotopes 65(4): 392–396, DOI 10.1016/j.apradiso.2006.09.008.
- 7.Goedicke C, 2003. Dating historical mortars by blue OSL: results from known age samples. Radiation Measurements 37(4–5): 409–415, DOI 10.1016/S1350-4487(03)00010-6.
- 8.Goedicke C, 2011. Dating mortar by optically stimulated luminescence: a feasibility study. Geochronometria 38(1): 42–49, DOI 10.2478/s13386-011-0002-0.
- 9.Goslar T, Nawrocka D and Czernik J, 2009. Foraminiferous limestone in 14C dating of mortar. Radiocarbon 51(3): 987–993.
- 10.Hale J, Heinemeier J, Lancaster L, Lindroos A and Ringbom Å, 2003. Dating ancient mortar. American Scientist 91(2): 130–137, DOI 10.1511/2003.2.130.
- 11.Heinemeier J, Ringbom Å, Lindroos A and Sveinbjörnsdóttir Á, 2010. Successful AMS 14C dating of non-hydraulic lime mortars from the medieval churches of the Åland Islands, Finland. Radiocarbon 52(1): 171–204.
- 12.Ikeya M, 1993. New Applications of Electron Spin Resonance: Dating, Dosimetry and Microscopy. World Scientifc, Singapore.
- 13.Ikeya M, 2004. EPR Dating, Dosimetry and Microscopy for Terrestrial and Planetary Materials. In: Gilbert BC, Davies MJ, Murphy DM, eds., Electron Paramagnetic Resonance. Specialist Periodical Reports (Royal Society of Chemistry) 19: 1–32.
- 14.Jonas M, 1997. Concepts and Methods of EPR Dating. Radiation Measurements 27(5–6): 943–973, DOI 10.1016/S1350-4487(97)00202-3.
- 15.Kabacińska Z, Krzyminiewski R, Dobosz B and Nawrocka D, 2012. EPR investigation of structure and dynamics of paramagnetic centres in lime mortars from Budinjak, Croatia. Radiation Measurements 47(9): 825–829, DOI 10.1016/j.radmeas.2012.03.017.
- 16.Krzyminiewski R, 1994. Computer Enhancement of Complex Spectroscopic Spectra Resolution. Molecular Physics Reports 6: 174–179.
- 17.Krzyminiewski R and Frąckowiak M, 2000. CREM in application to EPR dating technique. Geologos 5: 65–75.
- 18.Krzyminiewski R, Kowalczyk RM, Bielewicz-Mordalska A, Pająk Z and Czarnecki P, 1998. Computer enhancement of CW-EPR experimental spectra resolution as a new method in investigation of molecular dynamics in pyridiniumtetrafluoroborate. Journal of Molecular Structure 471(1–3): 243–249, DOI 10.1016/S0022-2860(98)00442-6.
- 19.Lindroos A, Heinemeier J, Ringbom Å, Braskén M and Sveinbjörnsdóttir Á, 2007. Mortar dating using AMS 14C and sequential dissolution: examples from medieval, non-hydraulic lime mortars from the Åland Islands, SW Finland. Radiocarbon 49(1): 47–67.
- 20.Marco S, Hartal M, Hazan N, Lev L and Stein M, 2003. Archaeology, history, and geology of the A.D. 749 earthquake, Dead Sea transform. Geology 31(8): 665–668, DOI 10.1130/G19516.1.
- 21.Michniewicz J and Nawrocka D, 2005. Petrography of the plasters from Hippos. In: Segal A, Młynarczyk J, Burdajewicz M, Schuler M, Eisenberg M, Hippos-Sussita. Zinman Institute of Archaeology University of Haifa, Israel: 82-91. ISBN 965-90418-4-5.
- 22.Michalska Nawrocka D, Michczyńska DJ, Pazdur A and Czernik J, 2007. Radiocarbon chronology of the ancient settlement in the Golan Heights area, Israel. Radiocarbon 49: 625–637.
- 23.Młynarczyk J, 2001. Polsko-izraelskie wykopaliska w Hippos (Sussita) 2000–2001. Kosciol Polnocno-zachodni (NWC) (Polish-Israeli ex-cavation in Hippos (Sussita) 2000-2001. North-West Church (NWC)). Światowit III (XLIV), fasc. A: 133–41 (in Polish).
- 24.Nawrocka D, Czernik J and Goslar T, 2009. 14C Dating of carbonate mortars from Polish and Israeli sites. Radiocarbon 51: 857–866.
- 25.Nawrocka D, Michniewicz J, Pawlyta J and Pazdur A, 2005. Application of radiocarbon method for dating of lime mortars. Geochronometria 24: 109–115.
- 26.Polikreti K, Maniatis Y, Bassiakos Y, Kourou N and Karageorghis V, 2004. Provenance of archaeological limestone with EPR spectroscopy: the case of the Cypriote-type statuettes. Journal of Archaeological Science 31(7): 1015–1028, DOI 10.1016/j.jas.2003.12.013.
- 27.Segal A, Młynarczyk J, Burdajewicz M, Schuler M, Eisenberg M, 2004. Hippos (Sussita). Fifth Season of Excavations and Summary of All Five Seasons (2000–2004). Haifa: Zinman Institute of Archaeology, University of Haifa (in Hebrew and English)
- 28.Seleţchi ED and Duliu OG, 2007. Comparative Study on EPR Spectra of Carbonates. Romanian Journal of Physics 52: 657–666.
- 29.Wencka M and Krzyminiewski R, 2004. Identification of paramagnetic centers and the dating of cave dripstones by electron paramagnetic resonance. Applied Magnetic Resonance 26(4): 561–578, DOI 10.1007/BF03166583.
- 30.Zacharias N, Mauz B and Michael CT, 2002. Luminescence quartz dating of lime mortars. A first research approach. Radiation Protection Dosimetry 101: 379–382.
Typ dokumentu
Bibliografia
Identyfikator YADDA
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