Tytuł artykułu
Treść / Zawartość
Pełne teksty:
Identyfikatory
Warianty tytułu
Języki publikacji
Abstrakty
This study investigates the influence of various factors on shear flocculation in the apatitedolomite mixed ore flotation system. The Box-Behnken response surface methodology is employed to evaluate the interactions of these factors on flocculation behavior. Additionally, the Focused Beam Reflectance Measurement (FBRM) and Particle Vision Measurement (PVM) techniques are applied to investigate the mechanisms by which these factors affect shear flocculation. The results show that sodium oleate (NaOL) concentration, pH, and shear rate significantly influence the size of the flocculated particles. Notably, the interaction effect between NaOL concentration and pH is particularly pronounced. FBRM and PVM analysis reveals that pH and NaOL concentration play dominant roles in controlling particle flocculation, while H3PO4 has a relatively minor impact on agglomerate morphology and size. At low shear rates, the flocs are larger and more uniformly distributed, resulting in a more stable process. In contrast, although high shear rates enhance initial flocculation efficiency, they reducefloc size. Furthermore, the modified Smoluchowski model is applied to evaluate the impact of different factors on flocculation kinetics. The findings suggest that the effects of these factors vary across different stages of flocculation. The combined influence of NaOL concentration, pH, and shear rate is crucial in determining the stability of the flocs, with these three factors being key determinants of floc morphology and stability.
Słowa kluczowe
Rocznik
Tom
Strony
art. no. 202595
Opis fizyczny
Bibliogr. 59 poz., rys., tab., wykr.
Twórcy
autor
- Mining College, Guizhou University, Guiyang 550025, China
autor
- Mining College, Guizhou University, Guiyang 550025, China
autor
- Mining College, Guizhou University, Guiyang 550025, China
autor
- Guizhou Academy of Sciences, Guiyang 550001, China
autor
- Guizhou Academy of Sciences, Guiyang 550001, China
autor
- Guizhou Academy of Sciences, Guiyang 550001, China
- Department of Materials Science and Engineering, Anhui University of Science and Technology, Huainan 232001, China
autor
- Guizhou Academy of Sciences, Guiyang 550001, China
- School of Mining and Coal Engineering, Inner Mongolia University of Science and Technology, Baotou 014010, China
Bibliografia
- BOXALL, J. A., KOH, C. A., SLOAN, E. D., SUM, A. K., WU, D. T., 2010. Measurement and calibration of droplet size distributions in water-in-oil emulsions by particle video microscope and a focused beam reflectance method. Ind. Eng. Chem. Res. 49, 1412-1418.
- CAI, Z., LUO, H., WU, J., LIU, X., 2019. Shearing flocculation flotation of low-grade collophanite in jinning. Multipurpose Util. Miner. Res. 49-54.
- CHEN, W., ZHANG, G., ZHU, Y., 2022. Rheological investigations of the improved fine scheelite flotation spiked with agitation medium. Int. J. Min. Sci. Technol. 32, 1379-1388.
- CHIMONYO, W., PENG, Y., 2022. Selective inhibition of kaolinite entrainment during chalcopyrite flotation in saline water. Miner. Eng. 184, 107637.
- DUAN, J., 2022, Cfd-pbm coupling simulation of coal escence crushing efficiency in flocculation process of fine coal slime, Taiyuan University of Technology, Taiyuan, China.
- GAO, R., ZHOU, K., ZHANG, J., GUO, H., REN, Q., 2019. Research on the dynamic characteristics in the flocculation process of mineral processing tailings. Ieee Access. 7, 129244-129259.
- GRABSCH, A. F., YAHYAEI, M., FAWELL, P. D., 2020. Number-sensitive particle size measurements for monitoring flocculation responses to different grinding conditions. Miner. Eng. 145.
- GREGORY, J., 2013. Flocculation fundamentals: encyclopedia of colloid and interface science, Springer Berlin Heidelberg, Berlin, Heidelberg.
- HAO, C., GUO, J., CHU, M., YANG, Y., WANG, L., GONG, Y., ZHAO, X., 2019. Analysis of models and factors of long flame coal flotation process by response surface methodology. J. Min. Sci. Technol. 4, 547-557.
- HE, G., ZHANG, Q., 2023. Study on mechanism of selective inhibition of fluorapatite and dolomite by amino trimethylene phosphonic acid. Industrial Minerals & Processing. 52, 12-17.
- HUANG, X., ZHANG, Q., 2023. Interaction behavior between coarse and fine particles in the reverse flotation of fluorapatite and dolomite. Langmuir. 39, 12931-12943.
- HUANG, X., ZHANG, Q., 2024. Depression mechanism of acid for flotation separation of fluorapatite and dolomite using tof-sims and xps. J. Mol. Liq. 394, 123584.
- JIN, S., 2022, Study on hydrophobic aggregation flotation of fine cassiterite using hydroxamic acids as collectors, Central South University, Hunan, China.
- LASENTEC, M., 2001. Product group. Fbrm® d600 hardware manual. Mettler-toledo autochem. Inc., Redmond, Wa.
- LI, D., YIN, W., LIU, Q., CAO, S., SUN, Q., ZHAO, C., YAO, J., 2017. Interactions between fine and coarse hematite particles in aqueous suspension and their implications for flotation. Miner. Eng. 114, 74-81.
- LI, D., YIN, W., SUN, C., YAO, J., 2020. Aggregation characteristics of fine hematite and siderite particles in aqueous suspension. Powder Technol. 368, 286-296.
- LI, D., ZHONG, H., YIN, W., SUN, C., HU, Y., 2021. Particle aggregation characteristics of hematite-quartz mixture with addition of sodium oleate. Powder Technol. 393, 796-806.
- LI, L. I., SAI, Z., QIANG, H. E., XUE-BIN, H. U., 2015. Application of response surface methodology in experiment design and optimization. Res. Explor. Lab. 34, 41-45.
- LI, M., XIANG, Y., CHEN, T., GAO, X., LIU, Q., 2021. Separation of ultra-fine hematite and quartz particles using asynchronous flocculation flotation. Miner. Eng. 164, 106817.
- LI, S., GAO, L., CAO, Y., GUI, X., LI, Z., 2016. Effect of ph on the flocculation behaviors of kaolin using a ph-sensitive copolymer. Water Sci. Technol. 74, 729-737.
- LI, S., GAO, L., WANG, J., ZHOU, H., LIAO, Y., XING, Y., GUI, X., CAO, Y., 2021. Polyethylene oxide assisted separation of molybdenite from quartz by flotation. Miner. Eng. 162, 106765.
- LI, Y., XIA, W., WEN, B., XIE, G., 2019. Filtration and dewatering of the mixture of quartz and kaolinite in different proportions. J. Colloid. Interface. Sci. 555, 731-739.
- LIANG, L., TIAN, F., WANG, M., 2022. Enhancement of selective flocculation of quartz in coal flotation based on shear rate adjustment. J. China Univ. Min. Technol. 51, 988-997.
- LUO, H., ZHAO, Z., CAI, Z., ZHANG, Z., YAN, Y., GUO, Y., 2021. Recovery of medium to low grade phosphate rock stockpiled in jinning phosphate mine by shear flocculation flotation. Industrial Minerals & Processing. 50, 26-30.
- NEELAKANTAN, R., VAEZI G., F., SANDERS, R. S., 2018. Effect of shear on the yield stress and aggregate structure of flocculant-dosed, concentrated kaolinite suspensions. Miner. Eng. 123, 95-103.
- NEGRO, C, FUENTE, E, BLANCO, A, TIJERO, J, 2005. Flocculation mechanism induced by phenolic resin/peo and floc properties. Aiche J. 51, 1022-1031.
- NIU, F., CHEN, Y., ZHANG, J., LIU, F., WANG, Z., 2024. Selective flocculation-flotation of ultrafine hematite from clay minerals under asynchronous flocculation regulation. Int. J. Min. Sci. Technol. 34, 1563-1574.
- NIU, F., LI, Z., ZHANG, J., 2017. Study on flocculation kinetics of fine hematite in stirring flow field. Conserv. Util. Miner. Resour. 58-63.
- NOGUEIRA, F., RODRIGUES, K., PEREIRA, C., SILVA, A. C., SILVA, E. M. S., AZIZI, A., HASSANZADEH, A., 2023. Quartz fine particle processing: hydrophobic aggregation by shear flocculation. Minerals. 13, 1208.
- PASCOE, R. D., DOHERTY, E., 1997. Shear flocculation and flotation of hematite using sodium oleate. Int. J. Miner. Process. 51, 269-282.
- RUAN, Y., HE, D., CHI, R., 2019. Review on beneficiation techniques and reagents used for phosphate ores. Minerals. 9, 253.
- RUAN, Y., ZHANG, Z., LUO, H., XIAO, C., ZHOU, F., CHI, R., 2018. Effects of metal ions on the flotation of apatite, dolomite and quartz. Minerals. 8, 141.
- SHI, J., 2017, Research on behaviors and mechanism of dispersion of the fine collophane and dolomite, Guizhou University, Guiyang, in China.
- SUN, C., SHI, S., HAN, D., 2022. Zoning model of flotation kinetics process in air-forced mechanical agitator flotation machine. J. China Univ. Min. Technol. 51, 411-418.
- WANG, C., SUN, C., LIU, Q., 2020. Formation, breakage, and re-growth of quartz flocs generated by non-ionic high molecular weight polyacrylamide. Miner. Eng. 157, 106546.
- WANG, H., DU, H., WANG, J., ZHANG, F., CAO, S., 2024. Unconfined compressive strength of composite improved expansive soil based on response surface method. Sci. Technol. Eng. 24, 6854-6861.
- WANG, X., 2020, Surface wettability regulation of minerals in flotation of calcium-magnesium phosphate ore, Guizhou University, Guiyang, in China.
- WANG, X., ZHOU, S., BU, X., NI, C., XIE, G., PENG, Y., 2021. Investigation on interaction behavior between coarse and fine particles in the coal flotation using focused beam reflectance measurement (fbrm) and particle video microscope (pvm). Sep. Sci. Technol. 56, 1418-1430.
- WANG, Z., WU, A., RUAN, Z., BURGER, R., WANG, S., MO, Y., 2024. Flocculation behavior, mechanics, and optimization of tailings based on multi-objective: insight into the concentration and time-dependent floc size. Powder Technol. 439.
- WEI, H., GAO, B., REN, J., LI, A., YANG, H., 2018. Coagulation/flocculation in dewatering of sludge: a review. Water Res. 143, 608-631.
- WU, D., TAN, F., WANG, X., XIU, C., ZHANG, H., 2000. Study of kinetics mechanism of flocculation and controlling index. Environ. Eng. 22-25.
- WU, Y., ZHANG, Y., LI, X., GUAN, Z., HE, Q., 2024. Advancements in studying the flocculation flotation of fine minerals. Conserv. Util. Miner. Res. 44, 16-26.
- XIE, J., 2024. Selective removal of dolomite from rare earth element-bearing phosphorite by flotation and leaching and the adsorption mechanism of agents on mineral surfaces. Surf. Interface Anal. 56, 82-98.
- YAN, X., WANG, W., ZHANG, H., LI, D., SUN, Z., YANG, H., 2022. Enhancement of liquid-solid mixing and particle hydrophobization by an impeller-less flotation pulp conditioning device. Miner. Eng. 190, 107933.
- YANG, B., HUANG, P., SONG, S., LUO, H., ZHANG, Y., 2018. Hydrophobic agglomeration of apatite fines induced by sodium oleate in aqueous solutions. Results Phys. 9, 970-977.
- YANG, J., 2020, Formation mechanism of hydrophobic agglomerates of fine-grained scheelite and its application in alkali leaching slag of scheelite, Beijing University of Science and Technology, Beijing, China.
- YANG, P., HU, X., ZI, F., YANG, B., WANG, Q., CHEN, Y., CHEN, S., 2020. Synergistic enhancement of fine-kaoliniteparticle hydrophobic agglomeration by combining dodecylamine with octanoic acid. Miner. Eng. 155, 106444.
- YE, J., 2019, Study on interfacial regulation of fine apatite flotation, Guizhou University, Guiyang, in China.
- YE, J., WANG, X., LL, X., CHL, X., ZHANG, Q., 2017. Effects of acid on adsorption of collector on collophane and dolomite surface. J. Wuhan Inst. Technol. 39, 565-570.
- YE, J., ZHANG, Q., LL, X., WANG, X., SHEN, Z., MAO, S., 2020. In-situ investigation of hydrophobic agglomeration of fine dolomite. Min. Metall. Eng. 40, 39-42.
- ZHANG, F., LI, G., PEI, J., WANG, C., WANG, H., WANG, Q., 2013. Study on the dynamic flocculation process of kaolin suspensions induced by cationic polyacrylamide by using fbrm. China Pulp & Paper. 32, 15-20.
- ZHANG, G., YAN, D., YANG-GE, Z., QI-MING, F., WEI-QING, W., 2011. Influence of ph on adsorption of sodium oleate on surface of ilmenite and titanaugite. J. Cent. South Univ. 42, 2898-2904.
- ZHANG, L., CHEN, Y., ZHAO, B., 2024. Numerical simulation of the optimization for the inlet structure of the furnace in the phosphogypsum reduction process by sulfur vapor. Powder Technol. 438.
- ZHANG, Q., LI, X., MAO, S., ZHANG, T., 2023. Application progress of molecular simulation in phosphate ore flotation. J. Min. Sci. Technol. 8, 102-114.
- ZHANG, Q., MAO, S., HUANG, X., CHEN, A., ZHANG, W., 2024. Research progress in surface chemistry of flotation for apatite and gangue minerals in phosphate ore. Conserv. Util. Miner. Res. 44, 1-15.
- ZHANG, Y., 2023, Study on flocculation and sedimentation characteristics of two types of iron tailings in liaoning region, Liaoning Technical University, Liaoning, China.
- ZHAO, L., CHEN, A., ZHANG, Q., GAO, G., 2022. Study on mineral hydrophobic agglomeration behavior and slurry rheology in microfine apatite-dolomite flotation system. Conserv. Util. Miner. Res. 42, 104-111.
- ZHAO, L., ZHANG, Q., 2024. Study of oleic acid-induced hydrophobic agglomeration of apatite fines through rheology. Miner. Eng. 218, 108911.
- ZHE, L., WENGANG, Z., 2021. Flocculation process of coal slime water based on flocculation kinetics and its research methods: a critical review. China Min. Mag. 30, 160-167.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-2b8e4871-8f23-4628-be48-ed76a4038417
JavaScript jest wyłączony w Twojej przeglądarce internetowej. Włącz go, a następnie odśwież stronę, aby móc w pełni z niej korzystać.