Effect of the vapour phase on the separation of isoquinoline alkaloids by thin-layer chromatography

• Autorzy: Petruczynik A. , Śliwka K. , Waksmundzka-Hajnos M.
• Języki publikacji: EN

Abstrakty

EN

The effect of conditioning of the silica layer by mobile phase vapour, diethylamine vapour and its aqueous and methanolic solutions, and ammonia vapour on the retention of alkaloids eluted with multicomponent non-aqueous mobile phases was examined. Effect of conditioning time and vapour phase composition on system efficiency and peak symmetry was investigated, as also was the effect of vapour phase composition on separation selectivity. The most effective and selective systems were used for separation of the alkaloid fraction from Fumaria officinalis.

Słowa kluczowe

EN

isoquinoline alkaloids; TLC; conditioning; Fumaria officinalis

• Wydawca: University of Silesia in Katowice ; Akademiai Kiado
• Czasopismo: Acta Chromatographica
• Rocznik: 2010
• Tom: Vol. 22, no. 3
• Strony: 391--404
• Opis fizyczny: Bibliogr. 29 poz., rys., tab.

Twórcy

autor

Petruczynik A.

• Medical University Department of Inorganic Chemistry 20-081 Lublin Poland

autor

Śliwka K.

• Medical University Department of Inorganic Chemistry 20-081 Lublin Poland

autor

Waksmundzka-Hajnos M.

• Medical University Department of Inorganic Chemistry 20-081 Lublin Poland

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