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Study of Microstructure of Oriented Eutectic Fe-C Alloy

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Warianty tytułu
Języki publikacji
EN
Abstrakty
EN
Fe - 4,25% C alloy was directionally solidified with a constant temperature gradient of G = 33,5 K/mm and growth rate of v = 83,3 μm/s (300 mm/h) using a vacuum Bridgman-type crystal growing facility with liquid metal cooling technique. To reveal more detailed microstructure, the deep etching was made. This was obtained in the process of electrolytic dissolution. The microstructure of the sample was examined on the longitudinal and transverse sections using an Optical Microscope and Scanning Electron Microscope. Using the Electron Backscattered Diffraction technique, phase map and analysis of phase were made. In this paper the analysis of Fe-C alloy eutectic microstructure is presented. Regular eutectic structure was obtained. The fracture surfaces show lamellar structure. Microscopic observation after electrolytic extraction indicates that the grains of longitudinal shape of eutectic cementite have been obtained. These grains are characterized by layered construction with many rounded discontinuities.
Rocznik
Strony
123--128
Opis fizyczny
Bibliogr. 17 poz., rys.
Twórcy
  • UTP University of Science and Technology, Mechanical Engineering Faculty, Bydgoszcz, Poland
Bibliografia
  • [1] Kurz, W., Fisher, D.J. (1986). Fundamentals of solidification. v. 1. Trans Tech Publications.
  • [2] Stefanescu, D.M. (2009). Science and engineering of casting solidification. v. 2. Springer.
  • [3] Davies, G.J. (1973). Solidification and casting. Wiley.
  • [4] Utter, B. & Bodenschatz, E. (2002). Dynamics of low anisotropy morphologies in directional solidification. Physical Review E. 66:051604.
  • [5] Utter, B. (2001). Low anisotropy growth in directional solidification. PhD thesis, Cornell University.
  • [6] Ghosh, S. (2015). Effects of solid-solid boundary anisotropy on directional solidification microstructures. HAL Id.
  • [7] Brener, E.A. & Temkin, D.E. (1996). Cellular, dendritic, and doublon patterns in directional crystallization. JETP. 82(3).
  • [8] Wołczyński, W. (2000). in: Modelling of transport phenomena in crystal growth. J.S. Szmyd & K. Suzuki, Ashurst Lodge, Southampton, UK - Boston, USA. 19.
  • [9] Piątkowski, J. & Matuła, T. (2012). Estimation of the operational reliability determined with Weibull modulus based on the abrasive wear in a cylinder-piston ring system. J. of Achievements in Materials and Manu-facturing Engineering. 55(2), 416-420.
  • [10] Stefanescu, D.M. (2005). Solidification and modeling of cast Iron—A short history of the defining moments. Materials Science and Engineering A. 413-414, 322-333.
  • [11] Nastac, L. & Stefanescu, D.M. (1995). Prediction of gray to white transition in cast iron by solidification modelling. AFS Transactions. 103, 329-337.
  • [12] Schumann, H. (1983). Metallographic 11. Auflage, VEB Deutscher Verlag fur Grundstoffindustrie, Leipzig, 314.
  • [13] Kopyciński, D. (2013). The inoculation of white cast iron. TMS (The Minerals, Metals & Materials Society). Published by John Wiley&Sons, Inc., Hoboken, New Jersey. Supplemental Proceedings. 601-608.
  • [14] Trepczyńska-Łent, M. (2017). Directional solidification of Fe-Fe3C white eutectic alloy. Crystal Research and Technology. 52(7), Version of record online: 26 JUN 2017. DOI: 10.1002/crat.201600359.
  • [15] Trepczyńska-Łent, M. (2013). Possibilities of the materials properties improvement for the cementite eutectic by means of unidirectional solidification. Archives of Metallurgy and Material. 58(3), 987- 991.
  • [16] Kitagawa, H., Shibata, N. (1961). Electrolytic isolation of carbide, sulphide and phosphide in white cast iron. Transactions of the Jap. Inst. of Metals. 2(2), 130-133.
  • [17] Trepczyńska-Łent, M. (2016). XRD and EBSD measurements of directional solidification Fe-C eutectic alloy. Archives of Foundry Engineering. 16(4), 169-174.
Uwagi
PL
Opracowanie rekordu w ramach umowy 509/P-DUN/2018 ze środków MNiSW przeznaczonych na działalność upowszechniającą naukę (2018)
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-2a1e98e6-28cf-4c1a-a56b-8b1807a86be2
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