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Abstrakty
Well-controlled fine MgTi2O5 &ensppowders, with pseudobrookite-type structure, are desired toward various industrial applications, however, commercial powders are hardly available to date. In this study, we focused the processing and characterization of well-controlled MgTi22O5 &ensppowders with/without LiF additive. MgCO3 &ensp(basic) and TiO2&ensp anatase powders with/without 0.5 wt. % LiF additive were calcined in air at 1100 °C for 2 h to obtain the MgTi2O5 &ensppowders. SEM observation revealed that the non-doped MgTi2O5 &ensppowder consisted of equiaxed particles with the diameter of 0.51.5 μm, whereas, the LiF-doped MgTi2O5 &ensppowder consisted of elongated particles with the length of ~ 5-10 μm and the diameter of ~1.0-1.5 μm. The smooth surface of elongated MgTi2O5 &enspparticles demonstrates the effect of LiF doping as a flux, i.e., liquid phase formation during the reaction.
Słowa kluczowe
Rocznik
Tom
Strony
37--41
Opis fizyczny
Bibliogr. 11 poz., rys., wykr., wz.
Twórcy
autor
- College of Engineering Sciences, School of Science and Engineering, University of Tsukuba, Ibaraki 305-8573, Japan
autor
- College of Engineering Sciences, School of Science and Engineering, University of Tsukuba, Ibaraki 305-8573, Japan
- Faculty of Pure and Applied Sciences, University of Tsukuba, Ibaraki 305-8573, Japan
Bibliografia
- [1] G. Bayer, J. Less-Common Metals 24 (1971) 129-138.
- [2] I. J. Kim, J. Ceram. Proc. Res. 11 (2010) 411-418.
- [3] E. Kato, K. Daimon, J. Takahashi, J. Am. Ceram. Soc. 63 (1980) 355-356.
- [4] T. S. Liu, D. S. Perera, J. Mater. Sci, 33 (1998) 995-1001.
- [5] S. M. Lang, C. L. Filmore, L. H. Maxwell, J. Res. Nat. Bur. Sta. 48 (1952) 298-312.
- [6] Y. Suzuki, M. Morimoto, J. Ceram. Soc. Jpn. 118 (2010) 819-822.
- [7] Y. Suzuki, M. Morimoto, J. Ceram. Soc. Jpn. 118 (2010) 1212-1216.
- [8] Y. Suzuki, Y. Shinoda, Sci. Tech. Adv. Mater. 12 (2011) no. 034301.
- [9] Y. Suzuki, T. S. Suzuki, Y. Shinoda, K. Yozhida, Adv. Eng. Mater. 14 (2012) 1134-1138.
- [10] NIMS AtomWork Database (http://crystdb.nims.go.jp/)
- [11] K. Momma and F. Izumi, J. Appl. Crystallography 44 (2011) 1272-1276.
Typ dokumentu
Bibliografia
Identyfikator YADDA
bwmeta1.element.baztech-29e95821-25ba-47d0-b698-e15c2170080a