Voltammetric screen-printed carbon sensor modified with multiwalled carbon nanotubes and bismuth film for trace analysis of thallium(I)

• Autorzy: Kozak Jędrzej , Tyszczuk-Rotko Katarzyna , Rotko Marek

Identyfikatory

DOI

10.5277/ppmp19065

• Języki publikacji: EN

Abstrakty

EN

The paper investigates the possibility of using commercially available screen-printed sensors with carbon nanomaterials modified working electrodes to anodic stripping voltammetric determination of trace concentrations of Tl(I). Each working electrode was additionally plated in-situ with a bismuth film (BiF). The highest analytical signal of Tl(I) at potential of -0.65 V (vs. pseudo- reference silver electrode) was achieved at the screen-printed carbon sensor with multiwalled carbon nanotubes and bismuth film modified working electrode (SPCE/MWCNTs/BiF). The calibration curve was linear in the range of Tl(I) concentrations from 1·10^-8 to 1·10^-6 mol·dm^-3 (-0.9 V, 180 s). The developed procedure of Tl(I) determination at this sensor allowed to achieve the low limits of detection and quantification of Tl(I), 2.8·10^-9 and 9.3·10^-9 mol·dm^-3 respectively. The method was used to determine thallium in the spiked water samples from the Vistula river.

Słowa kluczowe

EN

screen-printed sensor; anodic stripping voltammetry; bismuth film; multiwalled carbon nanotubes; thallium(I)

• Wydawca: Oficyna Wydawnicza Politechniki Wrocławskiej
• Czasopismo: Physicochemical Problems of Mineral Processing
• Rocznik: 2019
• Tom: Vol. 55, iss. 6
• Strony: 1422--1428
• Opis fizyczny: Bibliogr. 23 poz., tab., wykr.

Twórcy

autor

Kozak Jędrzej

• Maria Curie-Skłodowska University, Faculty of Chemistry, Department of Analytical Chemistry and Instrumental Analysis, Lublin, Poland

autor

Tyszczuk-Rotko Katarzyna

• Maria Curie-Skłodowska University, Faculty of Chemistry, Department of Analytical Chemistry and Instrumental Analysis, Lublin, Poland

autor

Rotko Marek

• Maria Curie-Skłodowska University, Faculty of Chemistry, Department of Chemical Technology, Lublin, Poland

Bibliografia

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Uwagi

Opracowanie rekordu ze środków MNiSW, umowa Nr 461252 w ramach programu "Społeczna odpowiedzialność nauki" - moduł: Popularyzacja nauki i promocja sportu (2020).